CHEM 3270 Forensic Chemistry (2 Cr) University of Wisconsin- Platteville Fall 2013 Class Meets: Dr. Charles R. Cornett Department of Chemistry and Engineering Physics OTT 214 342-1658 cornettc@uwplatt.edu T,Th 10:00 -11:52 am Otts 122 Office hours MF 8:30-11:30, TTh 8:30-10, F 1-2 or by appointment Required Text Bell, Forensic Chemistry, 2nd edition, Pearson, 2013 Reading List Skoog et al, Fundamentals of Analytical Chemistry, any edition Christian, Analytical Chemistry, 5th edition, Wiley, 1994 Harris, Quantitative Chemical Analysis, 5th edition, Freeman, 1998 Harvey, Modern Analytical Chemistry, 1st edition, McGraw Hill, 2000 Willard, Merritt, Dean, and Settle, Instrumental Methods of Analysis, 7th edition, Wadsworth, 1988 Necessary Materials Scientific Calculator Course Description An in-depth examination of forensic applications of chemistry related to chemical analysis: presumptive and confirmatory drug identification, microscopic techniques in trace evidence analysis, quality assurance and quality control (QA-QC) issues for the crime lab analyst, the toxicology of illicit compounds, and modern methods of DNA analysis related to criminalistics. Prerequisite: A grade of AC@ or better in CHEM 2150 and CHEM 3540 or instructor permission. Teaching Methodology Because the course focuses Socratic discussion AND quantitative applications, students are strongly encouraged to take accurate notes and review these notes on a regular basis and participate fully in discussions. A comparison of notes and continuation of dialogue out of class with classmates is suggested to optimize your learning. Students are expected to remain current with reading assignments as well as suggested problems. Quizzes will be administered announced and unannounced and problem-solving assignments will be an integral part of a successful study. The ultimate responsibility of learning lies with the student, and all students are highly encouraged to make use of posted office hours for questions, clarification, or further discussion. Laboratory workshops will also be used to augment topics. CHEM 3270 Fall 2013 (2) Grading Examinations (2) 100 pts x 2 Best ≤ 10 quizzes/assignments 10 pts x ≤10 Term Paper Comprehensive Final Examination 200 pts 100 pts 200 pts 200 pts 700 pts A> B> C> D> F< 90 % pts 80 % 70 % 60 % 60 % Examinations Lecture notes, assigned reading, and discussion topics are the primary resources for study. Questions may include, but are not limited to, short-answer, multiple-choice, quantitative problemsolving, and short-essay formats. Conceptual integration should be anticipated. The instructor reserves the right to curve the final class averages. Individual exams will not be curved. Non-linear methods may be applied where statistically appropriate. Quizzes and Assignments There are at least 10 assigned quizzes and assignments, at least one per day, throughout the Winterim period. These quizzes are multiple choice and short answer questions focusing on the major points of the unit. While quiz questions provide an opportunity to assess student progress, these general questions do not exclusively represent the level or types of questions in the one hour examinations. These quizzes are intended to provide a basic assessment of how well each student is keeping current with the major concepts of the course. In the event that more than 10 quizzes and assignments are administered, the >highest-marked= 10 exercises will be retained. Unexcused absences will not be dropped; therefore quiz grades of >zero= for these absences will be retained. Term Paper Students will draw term paper topics at random on Sept 20. The term papers are due Dec 1, 2013 and should include eight peer-reviewed references. Formatting should comply with the Journal of Forensic Science. CHEM 3270 Fall 2013 (2) Participation In-class participation is an essential part of a successful study. This includes content-based discussion with fellow students outside of the classroom. Plan on spending two hours outside of the classroom for each hour in-class for best results. Another aspect of participation is seeking additional assistance if necessary. Please refer to posted office hours and feel free to schedule an appointment if you are unable to see me during these hours. In addition, feel free to email questions. A good measure of daily progress is available by working the assigned homework problems and assignments. Trouble with completing these problems DOES indicate the need for extra help. PLEASE see me during my posted hours or schedule an appointment. While an occasional appointment or illness may call me away, I reserve these hours solely for your questions and discussion. Assessment Philosophy A An excellent understanding of the material and an outstanding ability to quantitatively employ the concepts in solving related problems B An above average understanding of the material and the ability needed to quantitatively employ the concepts in further studies or applications C An average understanding of the material and its quantitative applicability Attendance Policy and General Expectations * Students are expected to attend all sessions. With consideration for others, do not attend class if you are ill. Please inform the instructor if you are to be absent, otherwise all absences will be treated as Aunexcused@ absences. It is the responsibility of the student to acquire the notes from the missed classes. The instructor reserves the right to refuse all assignments late as a result of an unexcused absence. Instructor notification of absence does not necessarily constitute an excused absence. * (Winterim) Commuting students, please check your e-mail prior to class in inclement weather and use appropriate judgment before traveling should the University remain open. * Habitual tardiness will not be tolerated. Occasional delays are a fact of life; however, when arriving late, please minimize disruption when entering the classroom. * If co-curricular activities necessitate an absence from class, please inform the instructor as soon as these events are scheduled so that these absences may be excused. CHEM 3270 Fall 2013 (4) * There are NO make-up examinations. In the event of an excused absence, the corresponding section of the final examination will substitute for the missed grade. * If you have a specific physical, psychological, or learning disability and require accommodations; please let me know as early as possible so that your learning needs may be appropriately met. * Cell phones are to be turned off prior to class. * Come to class prepared; bring along your scientific calculator as well as the textbook. Academic Integrity Academic dishonesty will not be tolerated and will be dealt with in the manner outlined in the University of Wisconsin-Platteville Student Handbook. Academic dishonesty includes the party(ies) knowingly supplying restricted work to another individual. Academic dishonesty is viewed as a very serious action and will be dealt with to the fullest extent provided under University guidelines. Tentative Schedule of Topics Introduction, Statistics, and Calibration QA-QC in the Forensic Chemistry Laboratory Sampling and Preparation of Samples Chromatographic Applications in the Forensic Laboratory Mid-term 1 = Oct 10 Spectroscopic Applications in the Forensic Laboratory Drugs of Abuse: Pharmacology Drugs of Abuse: Analysis Microscopy in Trace Evidence Analysis Combustion: Arson, Explosives, and Gun Shot Residue Inks, Dyes, and Documents Analytical Instruments and DNA Analysis Mid-term 2 = Dec 10