CH-201: Organic Chemistry I Fall 2015 URL http://www.southalabama.edu/colleges/artsandsci/chemistry/laboratories.html Session Date Exp. # Topic 1 Aug 18-24 Check-in/Orientation/Safety * 2 Aug 25-31 Online Determination of Melting Points MP 3 Sept 1-4 & 14 3A & B Recrystallization: Purification of Sulfanilamide MP Sept 7 Sept 8-11 No Lab No Labs LABOR DAY 4 Sept 15-21 6D, 5 Sept 22-28 6 Chromatography: Fluorene / Fluorenone then 6A MP/TLC Online Part 1: Extraction of a Three Component Mixture MP Sept 29-Oct 5 Online Part 2: Extraction of a Three Component Mixture MP Oct 6-7 Oct 8-9 No Labs No Labs 7 Oct 12-16 13A 8 Oct 19-23 FALL BREAK Isolation of Caffeine from Tea (PAIRS) MP/IR 7B & Online Simple Distillation (PAIRS) (Note: For prelab, 2-methylpentane and heptane will be separated) GC Oct 23 NOTE Last Day to Drop 9 Oct 26-30 23D Synthesis of t-Pentyl Chloride IR/NMR 10 Nov 2-6 24A Synthesis of 4-methylcyclohexene IR 11 Nov 9-13 21 12 Nov 16-20 Nov 23-27 13 Nov 30-Dec 4 Reactivities of Some Alkyl Halides: Part 1 (Note: For prelab, use NaI as reagent (SN2)) Reactivities of Some Alkyl Halides: Part 2 (Note: For prelab, use AgNO3 as reagent (SN1)) AND **Check-out of Laboratory No Labs THANKSGIVING PRACTICUM **RETURN YOUR CHECK-OUT SHEET TO THE STOCKROOM AND GET YOUR LAB RECORD CLEARED OR YOU WILL BE CHARGED A $50.00 PENALTY FEE. NOTES: *1. YOU MUST ATTEND THE SCHEDULED SAFETY ORIENTATION SESSION TO BE ALLOWED TO WORK IN THE LABORATORY. 2. ALL monetary charges accrued through the Stockroom will be charged to your PAWS account. ** 3. Check-out is to be completed on the last day that YOUR lab section meets, prior to the Practicum. 4. Return Check-out Sheet to the stockroom to complete check-out. REV 7/26/15/DR