CHEMISTRY 201L
Organic Chemistry I Lab
Fall 2014
URL http://www.southalabama.edu/chemistry/laboratories.html
Session
Date
Exp. #
Topic
Analysis
1
Aug 18-22
2
Aug 25-29
Online
Determination of Melting Points
Sept 1
No Lab
LABOR DAY
3
Sept 2-8
3A & B
Recrystallization: Purification of Sulfanilamide
4
Sept 9-15
6D, then 6A
Chromatography: Separation of
Fluorene / Fluorenone
5
Sept 16-22
Online
Part 1: Extraction of a Three Component Mixture
MP
6
Sept 23-29
Online
Part 2: Extraction of a Three Component Mixture
MP
7
Sept 30- Oct 3
& 13
13A
Isolation of Caffeine from Tea (PAIRS)
MP/IR
Oct 6-7
Oct 8-10
No Labs
No Labs
FALL BREAK
8
Oct 14-20
7B & Online
Simple Distillation (PAIRS) (Note: For prelab,
2-methylpentane and heptane will be separated)
9
Oct 21-27
23D
Synthesis of t-Pentyl Chloride
Oct 24
NOTE
Last Day to Drop
10
Oct 28-Nov 3
24A
Synthesis of 4-methylcyclohexene
11
Nov 4-10
21
Reactivities of Some Alkyl Halides: Part 1
(Note: For prelab, use NaI as reagent (SN2))
12
Nov 11-17
21
Reactivities of Some Alkyl Halides: Part 2
(Note: For prelab, use AgNO3 as reagent (SN1))
13
Nov 18-24
Nov 26-28
14
Orientation/Check-in/Safety*
MP
MP
MP/TLC
GC
IR/NMR
PRACTICUM
No Labs
Dec 1-4 (Friday sections TBA)
THANKSGIVING
**Check-out of Laboratory
**RETURN YOUR CHECK-OUT SHEET TO THE STOCKROOM AND GET YOUR LAB
RECORD CLEARED OR YOU WILL BE CHARGED A $50.00 PENALTY FEE.
NOTES: *1. YOU MUST ATTEND THE SAFETY ORIENTATION SESSION TO BE ALLOWED TO
WORK IN THE LABORATORY.
2. Payment of fees must be completed BEFORE 5:00 PM, Thursday, December 4, 2014.
** 3. The last opportunity to complete Check-Out WITHOUT PENALTY is the DAY and START TIME
of your LAST regular scheduled lab session → See Schedule.
Rev 7/21/14/dr
IR