Organic Chemistry I Lab (CH-201) Spring 2015 URL http://www.southalabama.edu/chemistry/laboratories.html Session 1 Date Exp. # Jan 12-15 Topic Analysis Orientation/Check-in/Safety* Jan 19 Holiday Martin Luther King Birthday 2 Jan 20-26 Online Determination of Melting Points MP 3 Jan 27-Feb 2 3A & B Recrystallization: Purification of Sulfanilamide MP 4 Feb 3- 9 6D, then 6A Chromatography: Fluorene / Fluorenone 5 Feb 10-16 Online Part 1: Extraction of a Three Component Mixture Feb 17 Holiday Mardi Gras Day 6 Feb 18-24 Online Part 2: Extraction of a Three Component Mixture 7 Feb 25-26 & Mar 9-10 13A Isolation of Caffeine from Tea (PAIRS) Mar 2-6 Holiday Spring Break Week 8 Mar 11-17 7B & Online Simple Distillation (PAIRS) (Note: For prelab, 2-methylpentane and heptane will be separated) 9 Mar 18-24 23D Synthesis of t-Pentyl Chloride 10 Mar 25-31 24A Synthesis of 4-methylcyclohexene Apr 3 Note Last Day to Drop 11 Apr 1-7 21 Reactivities of Some Alkyl Halides: Part 1 (Note: For prelab, use NaI as reagent (SN2)) 12 Apr 8-14 21 Reactivities of Some Alkyl Halides: Part 2 (Note: For prelab, use AgNO3 as reagent (SN1)) April 15 NO LABS 13 Apr 16-22 PRACTICUM 14 Apr 23-29 ** Check-out of Laboratory MP/TLC MP MP MP/IR GC IR/NMR **RETURN YOUR CHECK-OUT SHEET TO THE STOCKROOM AND GET YOUR LAB RECORD CLEARED OR YOU WILL BE CHARGED A $50.00 PENALTY FEE. NOTES: *1. YOU MUST ATTEND THE SAFETY ORIENTATION SESSION TO BE ALLOWED TO WORK IN THE LABORATORY. 2. Payment of fees must be completed BEFORE 5:00 PM, Thursday, April 30, 2015. ** 3. Check-out is to be completed on the last day that YOUR lab section meets. Return Check-out Sheet to the stockroom to complete check-out. REV 1/5/15/DR IR