SOLITAIRE PHARMACIA PVT. LTD.
RESTRICTED CIRCULATION
AUTHORISED PERSONS ONLY
STANDARD OPERATING PROCEDURE
Title: Operation & Calibration of UV- Cabinet
Prepared By
Concerned Dept
1.
Checked By
Concerned Dept
Reviewed By
QA
Approved By
QA-Head
SOP. No.
:
SPL/ SOP/QC/029
Page No.
:
1 of 3
Supersedes
:
New
Revision No.
:
00
Effective Date
Review Date
Objective
To define the procedure for Operating and Calibration procedure of UV Cabinet.
2.
Scope
This procedure is applicable to Quality Control department at Solitaire Pharmacia Pvt. Ltd.,
Baddi.
3.
Responsibility
Executive Quality Control
4.
Accountability
Head Quality Control
5.
Procedure
5.1.
Instrument Detail:
Name
UV-CABINET
Make
Model
Sr. No.
Sarthak
STK-312
100303
Instrument ID.
QCD/UVC/009
5.2.
5.2.1.
Location
Instrument Lab.
Operation Procedure:
Before operation check the UV cabinet and observation glass window for the cleanliness. If
found unclean, clean it using dry cloth.
5.2.2.
Connect the UV cabinet to the Mains and switch “ON” the mains.
5.2.3.
Place the TLC plate / sample in the UV cabinet hood by opening the front door. Then close
the door.
Format No.SPL/QA/001
SOLITAIRE PHARMACIA PVT. LTD.
RESTRICTED CIRCULATION
AUTHORISED PERSONS ONLY
STANDARD OPERATING PROCEDURE
Title: Operation & Calibration of UV- Cabinet
Prepared By
Concerned Dept
5.2.4.
Checked By
Concerned Dept
Reviewed By
QA
Approved By
QA-Head
SOP. No.
:
SPL/ SOP/QC/029
Page No.
:
2 of 3
Supersedes
:
New
Revision No.
:
00
Effective Date
Review Date
Set the required wavelength (at which sample is to be observed) by pressing”254nm''
switch, which corresponds to UV short region or ``365 nm '' switch which corresponds to
UV long region and allowed to stabilized for 10 minutes.
5.2.5.
Observe the TLC plate / sample through glass window situated on the top of the instrument
.Note the observations in the analytical work report.
5.2.6.
Put off the wavelength switch. Remove the TLC plate/sample and Switch off the “MAIN”.
5.2.7.
Take proper entry in the log book.
5.3.
Calibration of UV - Cabinet:
Weight
6.
7.
Records/Formats:
SPL/QC/046
-
Log book for UV-Cabinet
SPL/QC/047
-
Calibration of UV-Cabinet
Annexure:
NA
8.
Reference:
Nil
9.
Abbreviations:
SPL
-
Solitaire Pharmacia Pvt. Ltd., Baddi
QC
-
Quality Control
SOP
-
Standard Operating Procedure
Format No.SPL/QA/001
SOLITAIRE PHARMACIA PVT. LTD.
RESTRICTED CIRCULATION
AUTHORISED PERSONS ONLY
STANDARD OPERATING PROCEDURE
Title: Operation & Calibration of UV- Cabinet
Prepared By
Concerned Dept
10.
Checked By
Concerned Dept
Reviewed By
QA
Approved By
QA-Head
SOP. No.
:
SPL/ SOP/QC/029
Page No.
:
3 of 3
Supersedes
:
New
Revision No.
:
00
Effective Date
Revision History:
Revision No
00
Format No.SPL/QA/001
Effective date
Reason for Revision
New Document
Review Date
SOLITAIRE PHARMACIA PVT. LTD.
RESTRICTED CIRCULATION
AUTHORISED PERSONS ONLY
STANDARD OPERATING PROCEDURE
Title: Operation & Calibration of UV- Cabinet
SOP. No.
Prepared By
Concerned Dept
Checked By
Concerned Dept
Reviewed By
QA
:
SPL/ SOP/QC/029
Approved By
QA-Head
Log book for UV-Cabinet
Format No : SPL/QC/046
Sr. No.
Format No.SPL/QA/001
Date
Name of Material
A.R. No.
Done By
Checked By
SOLITAIRE PHARMACIA PVT. LTD.
RESTRICTED CIRCULATION
AUTHORISED PERSONS ONLY
STANDARD OPERATING PROCEDURE
Title: Operation & Calibration of UV- Cabinet
SOP. No.
Prepared By
Concerned Dept
Checked By
Concerned Dept
Reviewed By
QA
:
SPL/ SOP/QC/029
Approved By
QA-Head
Calibration of UV-Cabinet
Format No : SPL/QC/047
Date of Calibration
:
Next Due Date:
Name of Instrument
:
UV-Cabinet
Make
:
Sarthak
User Department
:
Quality Control
Instrument Code
:
AVL/QC/047
Calibration Schedule
:
Monthly
Procedure:
Weight of Sodium salicylate :
mg
Weight of Sodium salicylate :
mg
Apply to the plate 5 ul of a 0.04 % W/V solution of Sodium Salicylate in alcohol for lamp o
maximum output at 254 nm and 5 ul of 0.2 % W/V Solution in alcohol for lamp of maximum
output at 365 nm.
Acceptance Criteria: The lamps should be capable of revealing without doubt the spots of
Sodium Silicate.
Remark: The instrument is working/ not working under satisfactory condition.
Analyzed By:
Checked By:
Approved By:
Date
Date
Date
:
Format No.SPL/QA/001
:
: