Fine Welding with Lasers Michael Müller Table of contents Lasers and Systems Welding principle Weld types and tolerances Material selection Influencing factors / Advanced process approaches ISO – Standards 2 Laser Working Station Notation according EN ISO 1145 : 1994 Beam guiding system Beam forming Laser source Process gas supply Work piece Laser Supply cabinet (power, cooling) Handling system (positioning, movement, clamping, gas supply) 3 Pulsed Nd:YAG lasers StarPulse 40 / 90 /150 Starfiber OEM StarPulse 500 Starfiber 400 - 600 Starfiber 100 - 300 4 Class 1 Systems Performance Integral MPS Select MPS 3D 5 Fix Optics 6 Galvo head Advantages fast positioning flexible in terms of part geometry easy to use software Suitable for fiber and direct beam delivery Vision system through the lense 7 Welding with Galvo Head - Principle 8 Laser – As a Thermal Tool Laser material interaction Absorption t0 Laser beam Laser beam In a thin surface layer (optical penetration depth depends on material , <10 nm) Generation of heat By transition of the energy of the light (photons) to the electrons of the material within the optical penetration depth Heat transport Laser beam Laser beam By heat conduction from the optical penetration depth into bulk material (temperature gradient) Materials reaction Solid state-, liquid state-, vapour phase processes (e. g. recristallisation, anealing, hardening, melting,...) depending on power density and interaction time t1 Isotherme 9 Laser Beam Absorption Absorption 30 Absorption in % Cu CO2 10,6 µm 25 20 Au 15 Ag Al Nd: YAG 1,06 µm St Fe 10 Mo 5 0.1 0.2 0.4 0.8 1 2 4 6 8 10 Wave length in µm 20 The absorbtivity of materials at room temperature and perpendicular incidence angle of low intensity laser radiation is strongly depending on the wave length 10 Process types – conduction welding Heat conduction welding 1) 2) Molten material Weld depth The material is heated above melting temperature but there is no vaporization. aspect ratio approx. 1 1) 4) max. penetration approx. 0.5 mm Very smooth surface Applications: Welding of thin workpieces, cosmetic welding of enclosures 11 Process types – keyhole welding Deep / Keyhole welding 1) 1) 2) 3) 4) Plasma cloud Molten material Keyhole Weld depth Heating of the material above vaporization temperature and formation of a keyhole aspect ratio approx. >> 1 Keyhole diameter approx. spot 3) 2) diameter Cw: max. penetration depending on laser power Pw: max penetration approx. 3 mm 4) 12 Depth [mm] Conduction mode 105 Critical intensity PROCESS TYPES 106 Plasma shielding Keyhole mode power 107 Power density [W/cm²] Example: Spot diameter 0.04 mm, Power 200 W -> I = 1.6 x 107 W/cm² Spot diameter 0.2 mm, Power 200 W -> I = 6.3 x 105 W/cm² 108 Laser Parameters - pulsed Power P PPK E process threshold PPuls PAV τ 1. Peak power 2. Pulse power 3. Pulse width 4. Pulse energy 5. Frequency 6. Average power 7. Pulse shape Time t T = 1/υ PPK PPuls τ E υ PAV P(t) E = PPuls· τ PAV = E · υ PPulse Spot welding Energy too high Energy too low τ 14 Effect of Parameter Changes Pulsed Laser 1) Increase of peak power (W) 1000 W-2 ms-Focus 0,4 mm 2000 W-2 ms-Fokus 0,4 mm 3000 W-2 ms-Fokus 0,4 mm 2) Increase of pulse duration (ms) 1000 W-10ms-Fokus 0,4 mm 1000 W-2ms-Fokus 0,4 mm 1000 W-50 ms-Fokus 0,4 mm 3) Increase of spot size (mm) 1000 W-2 ms-Fokus 0,4 mm 1000 W-2 ms-Fokus 0,8 mm 1000 W-2 ms-Fokus 1,2 mm 15 Pulsed Welding - Overlap The overlap indicates which percentage of a pulse is covered by the following pulse. From overlap, spot diameter and velocity the necessary frequency can be calculated. ø 100% overlap 70% Cross section 70 % 50 % The overlap in pulsed laserwelding is usually in the range of 50 to 90 %. To achieve good strentgh a little more than 50 % are sufficient. If hermetic sealing is requiered the overlap needs to be 75 % or more. 16 Laser parameters - cw cw - Laser Power P E process threshold PAV = PPK Time t Peak power = average power in cw mode, peak power of a modulated puls is as maximum the max. average power Pulse width: 0.004 ms - 100 ms or cw mode Frequency: cw (up to 170 kHz in modulated mode) Power density (P/(π/4*D²)) has to be above process threshold 17 Effects of Temperature Cycle Laser welding has the following characteristics: Very high gradients and heating- (>10000 K/s) and cooling rates (100 .. Some 1000 K/s). Result: high state of stress. Material areas close to the molten zone are heated up close to the solidus temperature. The formation of balanced microstructures is nearly impossible. Typically we find coarse grained, hard and brittle microstructures in the HAZ. 18 Weld joint types Butt weld Lap joint Thin material should be on top Fillet weld Incidence angle of the laserbeam as much in joint direction as possible 19 Joint types – Butt Weld Butt weld Advantages: • optimum distribution of forces • optimum solution for light weight structures • no problems at welding coated material Disadvantages: • high requirements on tolerances • high requirements on clamping and positioning 20 Joint types – Lap Joint Lap joint Advantages: • low requirements in tolerances and positioning accuracy • low distortion indistribution of forces • more than 2 layers possible Disadvantages: • risc of crevice corrosion • difficult degassification Please note: Thin material should be on top. 21 Joint types – Fillet Weld Fillet weld Advantages: • easy to clamp • good distribution of forces 15° - 30° Disadvantages: • high requirements on clamping and positioning Please note: Angle of weld follows incidence angle of laserbeam 22 Tolerances Butt weld < 0,15 • d d < 0,1 • d Lap joint d < 0,1 • d d = 0.75 mm 23 Spot sizes 600 µm 30 µm 24 Spot diameter – pulsed lasers max. weld depth = 1-2 · spot diameter Max. gap < 0.1 · weld depth The spot diameter should be in the range of 50 – 100 % of the requiered weld depth and 10 times the maximum gap. The spot diameter results from the beam expansion rate and the focal length of the focussing lens when using direct beam delivery. Using fiber delivery the spot diameter depends on fiber diameter, upcollimation and focal length of the focussing lens. 25 Protection Gas Goal: Prevent oxidation Improve seam quality Solution: Use protection gas Nitrogen → cheap Argon → better seam quality Helium → difficult to handle Without gas Nitrogen Important: Laminar flow At 6 mm nozzle diameter 10 l/min are reasonable Argon 26 Weldability of Materials Weldability of a material is given, if in production due to the chemical, metallurgical and physical properties a weld according to the requirements can be done. from: DIN 8528 Teil 1 Possible requirements: • static strength • dynamic strength • heremtical sealing • electrical conductivity • reproducability • process stability Weldability is no material specific value. Due to this most often tests need to be done. 27 Material Selection Material Comment Carbon steel Welds well. If carbon content > 0.2 % brittle welds. Stainless steel 300 series welds well except alloys with S > 0.05 % 400 series welds brittle Copper High refectivity requires high peak power Cu-Be Welds well but particles hazardous Bronze (Cu/Sn) Reasonable welds Brass (Cu/Zn) Outgasing of zinc prevents good welds Aluminium Pure Al (1xxx) welds well, only a few alloys weld crack free (2219, 3003). Filler material 4047 or combination of alloys may improve result (e. g. 6061 with 4047), Titanium Welds well. Very good shielding with inert gas necessary Gold, Silver, Platinum High reflectivity requires high peak power Nickel Welds well Ni based super alloys Welds well if Ti + Al content < 4 % Kovar Welds well Tantal Welds well. Very good shielding with inert gas necessary Molybdenum Usually welds brittle – may be acceptable where high strength is not required Plating may cause cracks e.g. electroless nickel plating due to its phosphorous content 28 Material Selection - Combinations Weldability of metal combinations poor; good; excellent 29 Plating Issues Zinc coating • Boiling issues have to be considered • May cause brittle intermetallic phases with Cu Tin Nickel • • Electroless -> leads to cracking due to P in plating process Electrolytic -> to be preferred Gold • • Often with Ni underplating , avoid electroless Ni plating „Shiny“ Au more difficult than „dull“ Au Silver • Tends to spatter 30 Steel - Basics The weldabilty of steel depends strongly on the following material characteristics: chemical composition metallurgical processes at melting and solidification physical properties Material composition limits: C- content < 0,2 % S- and P-content as small as posible ( usually 0.035% S and 0.045 % P). (S often used to improve material suitability for milling, e. g.: 303 = 304 with high S content, 0.15 %) A prediction about the resulting microstructure and possible imperfections for highly alloyed steel grades can be obtained by using the Schäffler diagram. Please note: Diagram only valid for < 0,2 % C, < 1,0 % Si, < 4 % Mn, < 3 % Mo, < 1,5 % Nb. Schäffler diagram was created for non laser welding processes with lower cooling rates, use with great care. 31 Steel Weldability – Low alloyed Steel non- and low alloyed steel General structural steel: • hardening in HAZ possible. Tough at subzero steel and heat resisting structural steel: • Weldabilty good besides martensitic heat resisting structural steel . Case hardening-, nitriding heat treatable steel: • good weldability for CE = C+Mn/20+Mo/15+Ni/40+Cr/10+V/10+Cu/20+Si/25 < 0,35, limited weldability for 0,35< CE < 0,5. 32 Steel Weldability – Stainless steel Stainless steel Ferritic chrome steel (12 % < Cr < 17%, C < 0,1 %): • weldability has to be proved. Martensitic chrome steel (10 % < Cr < 14%, 0,1 % < C < 1,2 %): • • • Danger of cold cracking, increase of hardness and brittleness. weldability has to be proved. weldability for martensitic chrome nickel steel with 1 % < Ni < 6% and C < 0,05 % is better. Austenitic chrome – nickel (-molybdenum)-steel: • mainly good weldabilty. Austenitic ferritic steel (duplex steel): • Cool down time not sufficient for complete change of microstructure. 33 Suutala diagram S+P+B [mass %] 0.1 Arc welding Laser welding Crack No crack 0.05 0 1.4 1.6 1.8 Cr/Ni equivalent J.C. Lippold, Weld. J., 73-6 (1994)129s – 139s 34 Aluminium Welding - Basics Weldability of aluminium depends strongly on the composition of the alloy. Pure aluminium is for example well weldable. When using Al alloys containing Si, Mg and Cu care should be taken to avoid the peak of hot crack sensitivity. Solution: Filler wire, increase flexibilty in material selection but difficult handling Choose the material of one of the parts to weld in a way that the resulting microstructure in the weld seam is not critical. (e. g.: 5052 and 4047) 35 Aluminium Welding – Hot Cracking Al-Mg Relative Crack Sensitivity Al-Cu Al-Li Al-Mg2-Si Al-Si 1 2 3 4 5 6 7 Percentage Alloying Element [Weight %] 36 Aluminium – Alloy series Series Alloying elements Weldability Comment Non-heat-treatable alloys 1xxx pure Al (> 99%) generally weldable soft material 3xxx Al-Mn often weldable without filler soft , good corrosion resistance 4xxx Al-Si weldable, Si > 3 % to avoid hot cracking soft and ductile, mainly used as filler material 5xxx Al-Mg weldable using filler (Mg > 4 %) often rough surface higher strength due to Mg content Heat-treatable-alloys 2xxx Al-Cu / Al-Cu-Mg / Al-Cu-Li difficult to weld, exception 2219, high strength, low corrosion 2519 resistance 6xxx Al-Mg-Si weldable using filler (e. g.4047) good strength, well formable and relatively good corrosion resistance 7xxx Al-Zn, Al-Zn-Mg-Cu difficult due to Zn content, filler requiered strongest Al alloy 37 Weld Depth – Pulsed Laser 3,5 Stainless steel Aluminum 3 depth in mm 2,5 2 1,5 1 0,5 0 0 5 10 15 20 25 30 35 40 45 50 Pulseenergy in J Protection gas: Argon 38 Depth in mm Weld depth – cw Fiber Laser 2,4 2,2 2 1,8 1,6 1,4 1,2 1 0,8 0,6 0,4 0,2 0 100 W 200 W 400 W 600 W 0 2 4 6 8 3 speed in m/min 10 Depth stainless steel stainless steel: aluminum: 0.5 mm/100 W 0.3 mm/200 W Depth in mm 2,5 Rules for Laser selection: stainless steel (3 mm thick), welds in thinner material might be faster. N2 protection gas, spot Ø 20 µm 2 Depth aluminum 1,5 1 0,5 0 0 200 400 Power in W 600 800 Weld Depth - cw Diode Laser 2,5 Material: SUS304 Gas: Argon 2 Depth in mm 1kW, 400µm fiber 500µm spot size 1,5 1 0,5 0 0 2 4 Speed [m/min] 1m/min 3m/min 6 8 Focus position -z z=0 +z Laser beam inclined plane 41 Pulse Shaping Freely programmable pulse shape Closed loop control for accurate pulse shaping Green: Set point Yellow: Actual values 42 Pulse Shape - Why Peak Power [W] Purpose of Pulse Shaping: 2 5 1 Pulse duration [ms] 1. Fast keyhole opening using steepest rising slope and high peak intensity 2. Option: Prevention of melt expulsion (depending on viscosity of melt) 3. Adjust penetration and volume of keyhole (deep penetration/‘keyhole welding‘) 4. Step down or ramp down intensity to avoid overheating of melt (spatter!) 5. Continuous absorption of radiation into still open or just closing keyhole (medium intensity, transition to ‘heat conduction welding‘) Smoothening effect. 43 Pulse Shape - Effects Welding of Aluminum From: Rofin - Lasag 44 Rofin Smart Weld Technology Workpiece Top View Galvo Field 1. Application: Fine seam welding 2. Laser: Fiberlaser with Scanner Optics 3. Technology: Galvo used to move small spot perpendicular (programmable) to the welding direction Oscylation-movement perpendicular to weld seam Influence oscillation width Oscillation width 700 µm Oscillation width 350 µm With increasing oscillation width the weld gets wider but less deep. Max process speed depends on oscillation width and frequency. 46 Quality Aspects Weld penetration • Easy to judge by cross section or through weld Weld strength • Determined by destructive testing (pull test ….) Cracking • Visual inspection, ultrasonic, dye pentration Porosity • Cross section, various causes Hermetical sealing • Determined by leak test Weld cosmetics • Smoothness, flatness of surface 47 Construction Notes Process related allow root fusion support heat removal allow degassing of the melt new joint geometries possible (e. g. welding of several layers, weld even if lower surfece is not accesible) Clamping related clamping device close to joint allow self centering system technology related least possible contour complexity consider accesability 48 ISO STANDARDS Test and inspection ISO 15614 – 11 Seam quality evaluation ISO 13919 part 1-2 Quality management ISO 9000 Welding coordination ISO 14731 Welding personnel ISO 14732 quality standards laser welding Welding system ISO 15616 part 1-3 Base material EN 10025 Filler material ISO 2560 Welding procedures and -instructions ISO 15607 ISO 15609 part 3-4 ISO STANDARDS ISO 4063:2009: Welding and allied processes -- Nomenclature of processes and reference numbers EN 10025: Steel Specifications ISO 2560:2009: Welding consumables -- Covered electrodes for manual metal arc welding of non-alloy and fine grain steels -- Classification ISO 14731:2006: Welding coordination -- Tasks and responsibilities ISO 14732:2013: Welding personnel -- Qualification testing of welding operators and weld setters for mechanized and automatic welding of metallic materials ISO 13919-1:1996: Welding -- Electron and laser-beam welded joints -Guidance on quality levels for imperfections -- Part 1: Steel, Part 2: Aluminium and its weldable alloys ISO STANDARDS ISO 15607:2003: Specification and qualification of welding procedures for metallic materials -- General rules ISO 15614-11:2002: Specification and qualification of welding procedures for metallic materials -- Welding procedure test -- Part 11: Electron and laser beam welding ISO 15616-1:2003: Acceptance tests for CO2-laser beam machines for high quality welding and cutting -- Part 1 – 4 Laser standards ANSI Z136.9 - Safe Use of Lasers in Manufacturing Environments ISO 11145;2006: Optics and photonics -- Lasers and laser-related equipment -- Vocabulary and symbols Thank you for your attention. www.rofin.com