Fall 2009
CHML212
Thursday Sections
COURSE WEBSITE: http://www.uncw.edu/chem/courses/chmL212/
REQUIRED TEXTS:
Organic Chemistry: Chemistry 211-212 Laboratory Manual (Fall 2008 Edition)
 Organic Chemistry Laboratory Notebook
PREREQUISITE: CHML102
Day:
EXP. #
8/20
13
8/27
Introduction, Safety,
14
9/3
15
9/10
16
9/17
17
9/24
17 (cont.)
10/1
10/8
10/15
10/22
18
19
20
21
10/29
11/5
11/12
11/19
22
23
24
25
TENTATIVE SCHEDULE
EXPERIMENT TITLE
Calculation, Chromatographic, and Spectral Applications
IR and NMR Identification of an Unknown
Substituent Effects on the Rate of Electrophilic Aromatic Substitution
Synthesis of p-methylacetanilide
Nitration of p-methylacetanilide (Synthesis and Purification)
Nitration of p-methylacetanilide (Product Analysis)
(QUIZ 1: Exp. 13, 14, 15, and 16)
The Grignard Reaction
Oxidation of 9-Fluorenol
Reduction of 9-Fluorenone
Ester Synthesis: Flavors and Fragrances
(QUIZ 2: Exp. 17, 18, 19, and 20)
The Solventless Aldol-Type Condensation
Theory of Color in Organic Compounds: Preparation of Organic Dyes
Synthesis and GC Analysis of Fatty Acid Methyl Esters
Polymers: Synthesis of Nylon
(QUIZ 3: Exp. 21, 22, 23, and 24)
Attendance and Safety:
 No one is admitted to lab after the first 10 minutes or without closed toe shoes, lab manual or
safety glasses.
 You are expected to attend every laboratory session. There are NO make-up labs. You will receive a 0
for every lab you do not attend, regardless of the reason for the absence.
 If you miss three or more labs (including those for which you were more than 10 minutes late) you will
receive a grade of “F” for the entire course.
 Any student who does has not taken and received a passing grade for CHML102 will be administratively
withdrawn from the course.
Course Grading and Policies
93-100 = A, 90-92 = A-, 87-89 = B+, 83-86 = B, 80-82 = B-, 77-79 = C+, 73-76 = C, 70-72 = C-, 67-69 = D+, 63-66 = D, 60-62 = D-, <60 = F.
Lab Exams (50%):
 3 lab tests will be given, testing on 3-5 experiments each. Test dates are given on syllabus.
 Study guides will be provided on the course website.
 There will be NO make-up exams.
Laboratory Notebook (20%)
 Your notebook will consist of pre-lab and in-lab entries as described in class and in Appendix C in the lab
manual.
 A list of notebook requirements for each experiment is provided on the course website.
 Each student will submit yellow carbon pages containing pre-lab notebook entries at the beginning of the
lab period.
 Each student will submit yellow carbon pages containing in-lab entries at the end of the lab period.
Laboratory Reports (20%)
 Unless otherwise instructed, final lab reports are due at the beginning of lab one week after the
completion of the experiment.
 Late lab reports will receive a penalty of 5% of total grade per day. Unless previously arranged with
instructor, once graded lab reports are returned to students, no more lab reports will be accepted.
Lab Technique (10%)
 Up to 10% of the final grade for each experiment will be based on technique. In order to receive the
maximum score on the technique portion of your grade, you must do the following:
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Keep up with the glassware from your lab drawer. Return it to the lab drawer clean and dry, as well as to the drawer
from which it came.
Keep your work area clean and clean up after yourself. Equipment cords must be unplugged, wrapped, and the
equipment pushed to the back of the hood before leaving.
Bring your own safety goggles and wear them at all times while in the lab.
Come to lab prepared to do an experiment, having prelab completed, and ready to participate in the experiment.
Write things down in your lab notebook as you do the experiment.
Be sure to submit samples to instructor when required. This applies to samples for instrumental analysis and samples
for storage. If you throw out your samples too early, you will not have all of the results needed to complete an
assignment.
Turn in materials on time.
Be safe! Be familiar with the hazards of the chemicals to be used during an experiment.
Obey your safety contract at all times!
*** At the end of the semester, each student will be responsible for the contents and cleanliness of their lab
drawers. Any student leaving their assigned lab drawer missing glassware, or with dirty glassware, will be
penalized on their technique grade, resulting in a lower lab grade. ***
Use of Personal Electronics
 Cell phone use will not be tolerated in this class. Turn off your cell phones prior to class. If your cell
phone rings, you will be asked to leave the class. Refusal to identify the source of the ringing will result in
dismissal for the entire class, with the entire class receiving a zero for the lab.
 Laptops and desktop computer use is allowed for lab related materials ONLY. Any student seen engaging
in non-laboratory related activity will be asked to leave the class, and will receive a zero for the lab.
Learning Outcomes
 A student taking this course in the Department of Chemistry and Biochemistry at UNCW will demonstrate
the ability to perform laboratory-based experiments, utilizing appropriate equipment, applying proper
procedures and adhering to safety guidelines
Academic Integrity
 All members of UNCW’s community are expected to follow the academic Honor Code. Please read the
UNCW Honor Code carefully (as covered in the UNCW Student Handbook). Academic dishonesty in any
form will not be tolerated in this class.
 Please be especially familiar with UNCW’s position on plagiarism as outlined in the UNCW Student
Handbook. Plagiarism is a form of academic dishonesty in which you take someone else’s ideas and
represent them as your own.
Students with Disabilities
 Students with diagnosed disabilities should contact the Office of Disability Services (962-7555). Please
submit a copy of the letter you receive from Office of Disability Services detailing class accommodations
you may need. If you require accommodation for test-taking, please be sure to have referral letter
submitted no less than 3 days before the test.
Violence and Harassment
 UNCW practices a zero tolerance policy for any kind of violent or harassing behavior. If you are
experiencing an emergency of this type contact the police at 911 or UNCW CARE at 962-2273. Resources
for individuals concerned with a violent or harassing situation can be located at
http://www.uncw.edu/wsrc/crisis.html.