ME 330 Engineering Materials Lectures 2-3 Tensile Properties • • • • • • • Elastic properties Yield-point behavior Plastic deformation True vs. Engineering stress Stress-strain curves Fracture surfaces Hardness Testing Please read chapters 1 (Lecture 1) & 6 (Lecture 2) Where We Are Going... • Engineers design products to carry loads, transmit forces, etc. • Characterize a material’s behavior through properties – Measure properties in lab test … extrapolate behavior to different scenario – Alternative is proof testing everything! • Basic mechanical testing – Look for response to applied forces • Apply load, measure deformation • Indent surface, measure hardness – Quantify words like “strong”, “ductile”, “hard”, etc Basic Mechanical Tests Tension Most common mechanical test Gage section reduced to ensure deflection here Load cell measures applied load Extensometer ensures l measured from gage region Compression Similar to tensile test Good for brittle specimens … hard to grip Often much different properties in compression Torsion Test of pure shear Member twisted by angle , calculate shear strain Measure applied torque, calculate shear stress Bending In all cases, a displacement is applied and you measure load Calculate stress from measured load Calculate strain from change in gage length Tension Test Measure load and displacement Compute stress and strain Review of Stress and Strain Often interested in measuring force and deformation in a size independent manner • Stress: force per unit area • Ao Force Area F Engineering : Ao True : T F A L Lo Engineering : Lo L True : T ln Lo Lo A From dT=dL/L L • • Traditional units: MPa or ksi Ao is original area • A is instantaneous area Strain: “relative” change in length Length Length • • • Dimensionless quantity Lo is original length (“gage length”) L is instantaneous length Relation Between Stress & Strain Tension (+) Compression (-) Typical Stress-Strain Curves Yield Elastic Plastic (MPa) Strength ceramics Today, we’ll talk about the different: Regions in stress-strain space Properties important to design metals Energy Absorption Stiffness polymers 0.1 10 100 Ductility (%) Elastic Region & Properties Elastic region: proportional stress and strain Stiffness = Modulus of Elasticity ductility Elastic (MPa) ceramics metals Stiffness polymers ~0.1 10 100 (%) Elastic Material Behavior Elastic region: strain returns to zero when stress removed Elastic Modulus (E) - measure of stiffness Non-linear E Strain (%) Stress (MPa) Stress (MPa) Linear 2 tangent modulus @ 2 1 secant modulus @ 1 Strain (%) Elastic Behavior linear non-linear E Strain (%) Stress (MPa) Stress (MPa) Tangent Modulus Secant Modulus Strain (%) Atomic Level Effects on Modulus • Strength of interatomic bonds: stiffness of springs • Atomic packing: springs per unit area F Many metals Most ceramics F Most polymers F F Atomistic Origins of Elasticity Force d F( r ) dr ro Energy (r) Atomic separation, r Force d dF E 2 dr r ro dr r r o 2 Strong bonding, stiff Weak bonding, compliant r Final Notes on Stiffness (MPa) • Interatomic bonding – Ceramics - Ionic & Covalent – Metals - Metallic & Covalent – Polymers - Covalent & Secondary Ceramics Metals E Polymers • Packing – Ceramics & Metals (%) • Highly ordered crystals • Dense packing – Polymers • Randomly oriented chains • Loosely packed • Temperature effects – Effect depends on types of bonds – As temperature increases, modulus decreases Ceramics Metals Polymers Material E (GPa) Silicon Carbide 475 Alumina 375 Glass 70 Steel Brass 210 97 Aluminum 69 PVC 3.3 Epoxy 2.4 LDPE 0.23 Elastic Constitutive Relation for 1-D Tensile Loading (linear materials) • Hooke’s Law: Stress and strain are directly related by modulus of elasticity, E • z Poisson’s ratio: Strain perpendicular to applied load is related to the axial strain, y x z x z – Maximum (constant volume) : = 0.50 – Minimum: = 0 – Look at change in volume in a cube of side length, L LxLxL {L0 (1 xx )}x{L0 (1 yy )}x{L0 (1 zz )} {L0 (1 zz )}x{L0 (1 zz )}x{L0 (1 zz )} {L0 (1 zz )}x{L0 (1 zz )}2 L30{1 (1 2 ) zz ( 2) zz2 2 zz3 } L30{1 (1 2 ) zz } – Volume increases during tensile, elastic deformation (if 0.50) Elastic Behavior 1 Elastic E 2 Modulus 2 1 Axial E Shear G Poisson’s Ratio Elastic Modulus transverse longitudinal E 2G1 dF E dr r r 0 x z y z for isotropic material Elastic +Plastic Properties Yield Elastic Plastic (MPa) Strength ceramics metals Energy Absorption Stiffness polymers 0.1 10 100 Ductility (%) Elastic Unloading total strain = elastic + plastic Stress (MPa) Stress – always elastic, no concept of plastic stress E E e p p E Strain (%) plastic elastic Review Stress and Strain Engineering F Ao Stress Engineering L Lo L Lo Lo Strain Constant Volume F Lo ~ AL A0 L0 F True Stress 1 A L A True Strain T ln ln o ln 1 L A o Ao do A L ~ d Modeling Plastic Deformation: True Stress and Strain • • True stress-strain values for plasticity … takes into account large area changes during plastic deformation Can relate true values to engineering values – Valid only for constant plastic deformation – Assuming constant volume, T Ao * Lo A * L P P Ao A A Ao , A L / Lo 1 * * L / Lo A Ao L / Lo AA** LL o o L L * L / Lo * o Lo T *(1 ) T ln( L / Lo ) ln( 1 ) L Ao Lo Elastic Constitutive Relation for Simple Shear Ao F F F F Shear stress: Ao Shear strain: tan( ) Again, stress and strain are directly related, by shear modulus, G: G For isotropic materials, shear and elastic modulus are related by: E 2G 1 Stress & Strain in 3-Dimensions z z zx xz x xy zy yz yx y y x x y z xy xz yx yz zx zy x y z xy xz yx yz zx zy Need to relate stress to strain ij Cijkl kl Originally 9 independent components Cijkl has 81 constants!! Equilibrium indicates ij = ji 6 components 36 constants (most general anisotropic matl) Elastic strain is reversible, so Ci j= Cji 21 constants Based on crystal symmetry, for cubic crystals 3 constants For an isotropic crystal, need only 2 constants to describe 3-D response Relate 1-D tests to complex loading 3-Dimensional Elastic Stress State 1 E x E y z E xy 0 yz xz 0 0 E 1 E E 0 0 0 0 0 0 0 E E 1 E 0 0 2(1 ) E 0 0 0 2(1 ) E 0 0 0 0 0 x y 0 z xy 0 yz 0 xz 2(1 ) E 0 Orthotropic Material Isotropic Material 1 E x x yx y Ex z zx xy E x yz 0 xz 0 0 xy xz 0 0 0 0 Ey 1 Ez 0 0 0 0 0 0 0 0 Gxy 0 0 0 G yz 0 Ey 1 Ey zy Ez yz Ez 0 x 0 y z 0 xy yz 0 xz 0 Gxz Yield Point Yield Yield point marks the transition from elastic to plastic deformation Elastic (MPa) ceramics metals Stiffness polymers ~0.1 10 100 (%) Yield Point Behavior uy 0.2%y ly (%) 0.1 (MPa) (MPa) (MPa) y 0.2 (%) • Proportional limit marks the end of linearity • Yield point marks the beginning of plastic deformation (%) – Some materials show an obvious transition, y – Often need to define 0.2% offset yield, 0.2%y – Sometime see an upper (uy) and lower (ly) yield stresses occur • Caused by significant dislocation-solute interaction • Common in BCC iron based alloys Plastic Region Yield Elastic Plastic Stress is no longer proportional to strain Plastic deformation is permanent, non-recoverable (MPa) ceramics metals Stiffness polymers ~0.1 10 100 (%) Plastic Phenomena (MPa) Uniform deformation Localized deformation Necking begins: E E d 0 d y2 Upon unloading, strain is partitioned between recovered and permanent. y1 e p E p No concept of “plastic stress” (%) plastic elastic (MPa) Plastic Phenomena Upon reloading, stress-strain curve follows the same path to failure. (%) (MPa) True vs. Engineering - Curve True Engineering (%) • Decreasing area in plastic regime higher “true” stresses • Once a neck forms, – Equations are invalid – True curve overpredicts actual stress due to triaxial stress state True vs. Engineering - Curve Compression Plastic Constitutive Response • Can approximate relation between true stress-strain curve in constant plastic deformation region by: (MPa) T K T n – K is the strength parameter – n is the strain-hardening exponent • • • • 0 n1 if n = 0, elastic-perfectly plastic response if n = 1, ideally elastic material as n increases, achieve more strain hardening – Typically valid only for some metals and alloys – Termed “power law hardening” (%) Measures of Energy Absorption: Toughness vs. Resilience Resilience: Ability to absorb energy without permanent deformation - (elastic only) (MPa) Toughness: Total energy absorption capability of a material - (elastic + plastic) (%) •Units: Energy per unit volume •Define: Energy stored during deformation •Graphically: Area under - curve Stress-Strain Properties (cont.) y Modulus of Resilience 1 U r d y y 2 0 1 y y U r y 2 E 2E 2 Stress vs. Strain Eq. T K Tn for y T u Measures of Strength f Fracture stress, f UTS 0.2%y (MPa) Ultimate Tensile Stress, UTS 0.2% offset yield strength, 0.2%y Fracture strain, f (~Ductility) 0.2% (%) f Measures of Ductility Lo Ao L Percent Elongation: % EL L Lo * 100 Lo Area Reduction: % AR Ao A * 100 Ao A Sensitive to gage length Does not account for necking Insensitive to gage length Does account for necking Sensitive to cross-section Stress-Strain Properties Proportional limit Yield Strength UTS % Elongation % Reduction in Area = highest linear stress y 0.2% offset or lower yield point u Highest stress on curve L Lo % EL x 100 Lo % RA Ao A x 100 Ao Material Deformation & Fracture From Callister, p.126 Fracture Surfaces Brittle Ductile Brittle •Cleavage failure •Flat,rough fracture surface •No necking •Failure in tension •Ductile From Callister, p.187 •Completely ductile failure necks to a point •Cup-cone fracture surface •Necking prior fracture •Cavities initiate in neck •Voids coalesce to form crack •Final failure in shear •Discuss more completely in fracture Shear in Tension Test? ’ ’ 2-D Mohr’s Circle (’/2, ’/2) ’ ’ ’ ’ ’ ’ ’ ’ ’ All stress states on a diameter of this circle are equivalent, just rotation of axes Mohr’s Circle y Generalized 2-D Loading • x Stress state (tensor) depends on coordinate frame chosen Mathematical construct to ease coordinate transform Rotation of in material space is equivalent to 2* in Mohr space – Example: pure shear • • • • rotate 45º on material unit rotate 90º on Mohr’s circle /2 -/2 xy C 2 R C x y 2 2 2 R x xy 2 2 Mohr’s Circle Examples (y ,yx) y yx xy x min max ~ 35º ~ 10º y max max =0 ~ 70º ~ 20º y y max 45º (y ,0) (x ,0) x= -y y (x ,xy) (y ,0) 45º x Failure mode - simple models Brittle failure- Ductile failure - Maximum normal stress criteria Tresca criteria f f f f More complex failure theory - Von Mises (energy based) 2 2 1 2 3 1 2 3 2 2 e 2 1 2 Hardness Testing • Scratch Test - very qualitative – Mohs • Penetration Tests – – – – Brinell Rockwell Knoop Vickers Microhardness • Hardness testing measures ability to resist plastic deformation – Need to eliminate effect of elastic deformation • Brinell - load applied for 30 sec • Rockwell - initial preload and differential depth measurement • To measure individual grain hardness, use Knoop or Vickers (lab #8) Brinell Hardness F D d BHN D 2 D F D2 d 2 • Large, hard spherical indentor • Relatively large loads (500-3000 kg) • Hold load for 30 sec. • Leaves large indent in specimen • Manually measure indentation with calibrated microscope • Single scale for all materials • Takes average hardness over many grains Rockwell Hardness • F1 Rockwell B F2 • Most common hardness test method Many scales: 2 important for us: – Rockwell B- soft materials • Spherical indentor • Low loads (~100 kg) • small indention d1 F1 Rockwell C – Rockwell C- hard materials d2 • Conical indentor • Slightly higher loads (~150 kg) • Very small indention F2 • • • d1 d2 Measures differential penetration depth (initial preload, 10 kg) Machines are fully automated Scale limits 20-100 (HRB, HRC, etc) – if exceeded, switch test Conversions & Correlations • • Can convert from one scale to the other approximately Brinell Hardness number (HB) is approximately related to tensile strength by: UTS 3.45 * HB ( MPa ) UTS 0.5 * HB ( ksi ) • From Callister, p.139 in steels only (empirical relation) Notes on Hardness Testing • Scales are designed for flat specimens – Need “curvature correction” for round specimens – Avoid specimen edges and other indents • Specimen thickness must be at least 10x indention depth Advantages Cheap Simple test “Relatively” nondestructive “Relatively” quantitative Correlates with tensile strength Disadvantages “Relatively” nondestructive “Relatively” quantitative Statistical Testing • • • • When conducting experimental testing, data will vary. Be aware of your sources of variability: – Specimen manufacture – Machine variations/malfunctions – Environmental changes – Improper procedure – Random variables In lab, report your statistical differences, don’t hide them. For more in-depth analysis, look into IE230. • Measure of average value: Mean Value n xi • x i 1 n Measure of scatter: Standard Deviation n s • xi x i 1 2 n 1 Relative measure of scatter: “Coefficient of variation” s Cv x Thermal Properties • Often design to utilize a material’s thermal properties – Energy storage – Insulative or Conductive – Use thermally activated switches (beam expands and closes switch) • Properties we care most about – Heat Capacity (C) – Conduction (q) – Thermal Expansion (T) Heat Capacity & Conduction • Heat (Q) and Temperature (T) are related by dQ CdT • • C dQ dT Property can be measured at: – Constant volume, Cv – Constant pressure, Cp – Condensed phases (solid in our case) are more often at constant pressure Heat always flows from high energy to low q x k dT dx – qx is heat flux, k is thermal conductivity – Metals are excellent conductors due to free electrons – Ceramics and polymers are usually considered insulators Thermal Expansion • Temperature change will induce a change in dimensions l l • T l T f To If a bar is heated while physically constrained, induce a thermal stress T e 0 l = lo • l T f To T E l T f To E Thermal expansion coefficient is strongly dependent on material (shape of force vs. atomic separation curve) – Polymers: ~100-200 x 10-6 C-1 – Metals: ~10-20 x 10-6 C-1 – Ceramics: ~1-10 x 10-6 C-1 New Concepts & Terms • • • • Elastic Properties – Elastic (Young’s) Modulus • Secant Modulus • Tangent Modulus – Poisson’s ratio – Linear vs. Nonlinear – Isotropic vs. orthotropic Yield-point behavior – Proportional limit – 0.2% offset yield strength – Upper & lower yield Plastic Deformation – Neck – Uniform vs. localized deformation – Mohr’s circle True vs. Engineering stress – Engineering: original area – True: instantaneous area • • • • • Stress-strain curves – Yield strength – Ultimate Tensile Strength – Fracture Strength – Fracture Strain – Toughness, Resilience – Ductility (%AR, %EL) Fracture Surfaces – Cleavage – Cup-cone Hardness Testing – Rockwell – Brinell Statistics (mean, standard deviation) Thermal Properties – Heat Capacity – Thermal Expansion – Conduction Next Lecture ... • Please read chapters 2 & 3