Oral Presentation

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Sources and Beam Lines of
Canadian Light Source
Emil Hallin
Canadian Light Source
(material organized and presented by D.T. Jiang)
First Phase CLS Beamlines
7 beam lines are funded and approved by the
CLS Facility Advisory Committee
• (Facility Diagnostic Line #1: BM, visible
light)
• Far IR (BM)
• Mid IR Spectromicroscopy (BM)
• Soft X-ray Spectromicroscopy (Elliptical
Undulator)
• SGM (Undulator)
• VLS-PGM (Undulator)
• Protein Crystallography (Small Gap invacuum U)
• Hard X-ray microXAFS (Wiggler,
Ec=10.7keV)
Main Hall Floor plan
Mezzanine Level
Expansion Zone - Beamlines
Offices & Labs
Shielding Roof
Floor Elevation
103.650 (+3.650m)
Office
Reserve
Lab Reserve
Canadian Light Source
Mezzanine Floor Elevation
106.00 (+6.000m)
High Resolution Far IR
Spectroscopy
• PI: Bob McKellar: Robert.Mckellar@nrc.ca
• Wavelength range: 10-200 mm, 0.006-0.13 eV,
50-1000 cm-1
• Resolution: < 0.001 cm-1
• Endstation:
– High resolution Fourier Transform
spectrometer
– Sensitive FIR detectors; liquid He cooled
– Gas Phase work:
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Coolable long-path cell
Multi-pass electric discharge cell
High temperature absorption cell
Supersonic jet expansion chamber
– High pressure: diamond anvil cell, focusing
optics, bench & alignment tools
– Surface & interface studies: UHV chamber,
sample preparation and manipulation, 100 mm
spot size
Mid IR Spectromicroscopy
• Mike Jackson: mike.jackson@nrc.ca
• Wavelength: 1.5-15 mm, 0.08-0.8 eV, 700-6000
cm-1
• Spatial resolution: < 5 mm
IR Beamlines
First Mirror Concept
02B1.1 Mid IR Schematic
02B1.1 Mid IR Floor Layout
01B1.1 Far IR Schematic
01B1.1 Far IR Floor Layout
2
Brightness Photon/s-0.1%bw-100mA-mm
-sr
Brightness 100 mA
17
10
16
10
15
10
14
10
13
10
BB 1475'K
CLS 58 mrad
ALS 10 mrad
NSLS 40 mrad
SRC 15 mrad
12
10
11
10
1
10
100
Wavelength (micrometer)
1000
Soft X-ray Spectromicroscopy
• PI Adam Hitchcock: aph@mcmaster.ca
• Wavelength: 6-60 Angstrom, 250-1900 eV
• Insertion device: EPU (AppleII, ESRF
termination)
• Infinity corrected entrance slitless PGM with
vertical dispersion plane
• Optics: grating (SX700 style) & zone plate
• Resolution: 3000 or better
• Endstation: STXM + PEEM
SM Optical Layout
Feature XES
M1 177o 6o
PGM 177o
M2 G(1-3)
EPU *16.2 (15.0)
M3 STXM exit slit
1.5
6
3
STXM
5
1.5
M3 PEEM
6o
exit slit
M4 PEEM
177o
3
3
02B2-2
02B2-1
02B1-2
02ID-1
03ID-1
03B1-1
03B2-1
04ID-1
04B1-1
1
PEEM
04B2-1
05ID-1 / 05ID-2
05B1-1
02B1-1
01B2-1
05B2-1
12B2-1
06ID-1 / 06ID-2
11B1-1
11ID-1
06B1-1
06B2-1
11ID-2
10B2-1
07ID-1 / 07ID-2
10B1-1
~131 deg
10ID-1 / 10ID-2
09B2-1
~22.7m
09B1-1
09ID-1 / 09ID-2
12m
07B1-1
08B2-1
08B1-1
07B2-1
08ID-1 / 08ID-2
SM Optical Description
Variable polarization: arbitrary linear
150-2000eV, circular- 100-1000eV
Infinity corrected PGM: STXM at long
arm branch (preserved brightness),
PEEM (exchangeable) on short
(preserve flux)
Nominal energy resolving power 3000,
may be increased till 7000
Intensity on sample: STXM-108ph/s at
40nm, PEEM-1012ph/s in f40m
Stable operation even for CLS 2005 ebeam parameters
SGM and VLS PGM
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PI T.K. Sham: sham@uwo.ca
SGM Wavelengths: 200 – 1900 eV
PGM Wavelengths: 5.5 – 250 eV
SGM Resolution: 3000
PGM Resolution: 10000
Optics: grating monochromator
Endstations: UHV
Capabilities: photoemission, XAFS
Both preliminary design reports are complete
Insertion Devices
•SGM- 44 mm PPM device ~1.2 m long
•PGM- 185 mm PPM device ~1.8 m long
•1.25 mrad total canting between devices
•Preliminary designs for both devices complete
Protein Crystallography
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PI Louis Delbaere: Louis.Delbaere@usask.ca
Wavelengths: 1.9 – 0.68 Angstrom, 6.5 – 18 keV
Resolution: 1.6 x 104 using Si(220)
Typical Crystal size: 20 – 50 mm
Design goal: flux of 1013 photons/sec into a 50 x
100 mm area
• Design will be modeled after beamlines at SBCCAT and SER-CAT (APS). Preliminary design is
almost complete.
Protein Crystallography
Beamline Layout
(Based on the Design of SER-CAT/APS)
Small Gap Undulator Brilliance
Per =4.5 cm, N=26 (L=1.19m), B0=0.843T, Kmax=3.54
Micro-XAFS
PI De-Tong Jiang: jiang@usask.ca
Superconducting Wiggler Parameters:
lm= 0.033 m
Magnet Period Length
N = 35.5
Number of Periods
B = 1.9 T
Magnetic Field
K = 5.91
K Parameter
Front End Aperture: 1 mrad (H) x 0.24 mrad (V)
Ray-tracing shows that the XAFS focus is ~1050 m
horizontal (FWHM) x ~257 m vertical (FWHM) in
size. The Kirkpatrick-Baez mirror pair reduces this
down to ~[14-19] m
horizontal (FWHM) x [6-9] m vertical (FWHM), using
bent elliptical cylinders.
Wiggler Brilliance
DTJ Note: This is from the first hybrid design concept, total power
SR there would have been 23 kW. Gave up and switched to
Superconducting design. The new design is at least another factor
of 2 better yet half the total SR power. Smaller SR horizontal fan of
course.
Flux at Sample (Shadow tracing)
Photon Energy
(keV)
Photon Flux (photons/second) @ m-probe
Focus:
[14-19] m horizontal (FWHM) x [6-9] m
vertical (FWHM)
5
1.21 x 1013
10
1.94 x 1013
15
1.61 x 1013
20
9.12 x 1012
30
2.36 x 1011
40
1.02 x 107
Micro-XAFS photon flux
m-probe photon flux into 5 m x 5 m spot
at focus
Photon Flux (photons/second)
1.E+13
1.E+12
1.E+11
1.E+10
1.E+09
1.E+08
1.E+07
1.E+06
1.E+05
0
10000
20000
30000
Photon Energy (eV)
40000
Summary of CLS BL Status
•First 7 lines scheduled operation time: Jan.
2004
•Preliminary designs for most of the first 7 lines
are complete
•Tendering process has been started on
beamline and endstation
Instrumentation
•Phase I Insertion device preliminary designs
are completed
•Front ends conceptual design completed
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