Sources and Beam Lines of Canadian Light Source Emil Hallin Canadian Light Source (material organized and presented by D.T. Jiang) First Phase CLS Beamlines 7 beam lines are funded and approved by the CLS Facility Advisory Committee • (Facility Diagnostic Line #1: BM, visible light) • Far IR (BM) • Mid IR Spectromicroscopy (BM) • Soft X-ray Spectromicroscopy (Elliptical Undulator) • SGM (Undulator) • VLS-PGM (Undulator) • Protein Crystallography (Small Gap invacuum U) • Hard X-ray microXAFS (Wiggler, Ec=10.7keV) Main Hall Floor plan Mezzanine Level Expansion Zone - Beamlines Offices & Labs Shielding Roof Floor Elevation 103.650 (+3.650m) Office Reserve Lab Reserve Canadian Light Source Mezzanine Floor Elevation 106.00 (+6.000m) High Resolution Far IR Spectroscopy • PI: Bob McKellar: Robert.Mckellar@nrc.ca • Wavelength range: 10-200 mm, 0.006-0.13 eV, 50-1000 cm-1 • Resolution: < 0.001 cm-1 • Endstation: – High resolution Fourier Transform spectrometer – Sensitive FIR detectors; liquid He cooled – Gas Phase work: • • • • Coolable long-path cell Multi-pass electric discharge cell High temperature absorption cell Supersonic jet expansion chamber – High pressure: diamond anvil cell, focusing optics, bench & alignment tools – Surface & interface studies: UHV chamber, sample preparation and manipulation, 100 mm spot size Mid IR Spectromicroscopy • Mike Jackson: mike.jackson@nrc.ca • Wavelength: 1.5-15 mm, 0.08-0.8 eV, 700-6000 cm-1 • Spatial resolution: < 5 mm IR Beamlines First Mirror Concept 02B1.1 Mid IR Schematic 02B1.1 Mid IR Floor Layout 01B1.1 Far IR Schematic 01B1.1 Far IR Floor Layout 2 Brightness Photon/s-0.1%bw-100mA-mm -sr Brightness 100 mA 17 10 16 10 15 10 14 10 13 10 BB 1475'K CLS 58 mrad ALS 10 mrad NSLS 40 mrad SRC 15 mrad 12 10 11 10 1 10 100 Wavelength (micrometer) 1000 Soft X-ray Spectromicroscopy • PI Adam Hitchcock: aph@mcmaster.ca • Wavelength: 6-60 Angstrom, 250-1900 eV • Insertion device: EPU (AppleII, ESRF termination) • Infinity corrected entrance slitless PGM with vertical dispersion plane • Optics: grating (SX700 style) & zone plate • Resolution: 3000 or better • Endstation: STXM + PEEM SM Optical Layout Feature XES M1 177o 6o PGM 177o M2 G(1-3) EPU *16.2 (15.0) M3 STXM exit slit 1.5 6 3 STXM 5 1.5 M3 PEEM 6o exit slit M4 PEEM 177o 3 3 02B2-2 02B2-1 02B1-2 02ID-1 03ID-1 03B1-1 03B2-1 04ID-1 04B1-1 1 PEEM 04B2-1 05ID-1 / 05ID-2 05B1-1 02B1-1 01B2-1 05B2-1 12B2-1 06ID-1 / 06ID-2 11B1-1 11ID-1 06B1-1 06B2-1 11ID-2 10B2-1 07ID-1 / 07ID-2 10B1-1 ~131 deg 10ID-1 / 10ID-2 09B2-1 ~22.7m 09B1-1 09ID-1 / 09ID-2 12m 07B1-1 08B2-1 08B1-1 07B2-1 08ID-1 / 08ID-2 SM Optical Description Variable polarization: arbitrary linear 150-2000eV, circular- 100-1000eV Infinity corrected PGM: STXM at long arm branch (preserved brightness), PEEM (exchangeable) on short (preserve flux) Nominal energy resolving power 3000, may be increased till 7000 Intensity on sample: STXM-108ph/s at 40nm, PEEM-1012ph/s in f40m Stable operation even for CLS 2005 ebeam parameters SGM and VLS PGM • • • • • • • • • PI T.K. Sham: sham@uwo.ca SGM Wavelengths: 200 – 1900 eV PGM Wavelengths: 5.5 – 250 eV SGM Resolution: 3000 PGM Resolution: 10000 Optics: grating monochromator Endstations: UHV Capabilities: photoemission, XAFS Both preliminary design reports are complete Insertion Devices •SGM- 44 mm PPM device ~1.2 m long •PGM- 185 mm PPM device ~1.8 m long •1.25 mrad total canting between devices •Preliminary designs for both devices complete Protein Crystallography • • • • • PI Louis Delbaere: Louis.Delbaere@usask.ca Wavelengths: 1.9 – 0.68 Angstrom, 6.5 – 18 keV Resolution: 1.6 x 104 using Si(220) Typical Crystal size: 20 – 50 mm Design goal: flux of 1013 photons/sec into a 50 x 100 mm area • Design will be modeled after beamlines at SBCCAT and SER-CAT (APS). Preliminary design is almost complete. Protein Crystallography Beamline Layout (Based on the Design of SER-CAT/APS) Small Gap Undulator Brilliance Per =4.5 cm, N=26 (L=1.19m), B0=0.843T, Kmax=3.54 Micro-XAFS PI De-Tong Jiang: jiang@usask.ca Superconducting Wiggler Parameters: lm= 0.033 m Magnet Period Length N = 35.5 Number of Periods B = 1.9 T Magnetic Field K = 5.91 K Parameter Front End Aperture: 1 mrad (H) x 0.24 mrad (V) Ray-tracing shows that the XAFS focus is ~1050 m horizontal (FWHM) x ~257 m vertical (FWHM) in size. The Kirkpatrick-Baez mirror pair reduces this down to ~[14-19] m horizontal (FWHM) x [6-9] m vertical (FWHM), using bent elliptical cylinders. Wiggler Brilliance DTJ Note: This is from the first hybrid design concept, total power SR there would have been 23 kW. Gave up and switched to Superconducting design. The new design is at least another factor of 2 better yet half the total SR power. Smaller SR horizontal fan of course. Flux at Sample (Shadow tracing) Photon Energy (keV) Photon Flux (photons/second) @ m-probe Focus: [14-19] m horizontal (FWHM) x [6-9] m vertical (FWHM) 5 1.21 x 1013 10 1.94 x 1013 15 1.61 x 1013 20 9.12 x 1012 30 2.36 x 1011 40 1.02 x 107 Micro-XAFS photon flux m-probe photon flux into 5 m x 5 m spot at focus Photon Flux (photons/second) 1.E+13 1.E+12 1.E+11 1.E+10 1.E+09 1.E+08 1.E+07 1.E+06 1.E+05 0 10000 20000 30000 Photon Energy (eV) 40000 Summary of CLS BL Status •First 7 lines scheduled operation time: Jan. 2004 •Preliminary designs for most of the first 7 lines are complete •Tendering process has been started on beamline and endstation Instrumentation •Phase I Insertion device preliminary designs are completed •Front ends conceptual design completed