Curse Title: Project (Thesis) Curse Code: TE-407 Report on Industrial Attachment at Sinha Textile Group Academic Supervisor Dr. S. M. Mahbub-ul-Haque Majumder Professor of Textile Engineering & Dean Faculty of Science and Information Technology Daffodil International University Prepared by Farhana Islam Arifa ID: 091-23-1379 Date of Submission: 20-04-2013 1|Page Declaration We hereby declare that, this project has been done by me under the supervision of Dr. S. M Mahbub-ul-Haque Majumder Professor of Textile Engineering & Dean Department of Textile Engineering, Daffodil International University, Dhaka. I also declare that neither this project nor any part of this project has been submitted elsewhere for achieving award of any degree or diploma. Supervised By: Dr. S. M. Mahbub-ul-Haque Majumder Professor of Textile Engineering & Dean Department of TE Daffodil International University Submitted by Farhana Islam Arifa ID: 091-23-1379 Department of TE Daffodil International University 2|Page ACKNOWLEDGEMENT My first gratefulness goes to Almighty Allah to give me the strength and ability to complete the industrial training and this report. Who has made our life more beautiful, glorious and honored. A number of people have made significant contributions to the preparation of this report. Their insights, advice and suggestions helped us a lot. Firstly, I am very much thankful to Professor Dr. S. M. Mahbub-ul Haque Majumder,Dean, FSIT, DIU, for his encouragement and valuable suggestions for continual improvement of the report. My Internship Supervisor who offered me to do internship in the number one industry in Bangladesh Named Sinha Textile Group. I got tremendous support and guidance throughout the internship period. Working with him I have earned not only valuable knowledge but also inspired by innovativeness which helped to enrich my experience to a greater extent. His ideas and way of working is truly remarkable. I would also like to thank Prof. Dr. Md. Mahbubul Haque, Head, Dept. of TE, DIU for all necessary information delivery as well as for many technical help. I am very thankful to Prof, Dr. Zulhash Uddin, Advisor DIU for his support. I learned many things from him that can’t be expressed in a single of line. I would like to thank the Chairman, Managing Director, General Manager, Deputy General Manager, Manager, Assistant Manager, Senior Production Officer, Production Officer, Assistant Technical Officer, Technical Officer who gave us scope & helped for doing industrial attachment in the factory as well as for giving scope to work in their respective section. Being involved with them we have not only earned valuable knowledge but was also inspired by their innovativeness which helped to enrich our experience to a greater extent. I believe this report could not be finished if they did not help us continuously. I am also very much grateful to Sinha Textile Group authority for giving us opportunity to do our internship work in their factory. Finally I want to give thanks for all the workers, supervisors who have assisted, helped & inspired us to complete this report. 3|Page SL. NO Topics Page No. INTRODUCTION 5 1.2 BASIC DESCRIPTION OF TEXTILE 5 1.3 GENERAL INFORMATION ABOUT FACTORY MANAGEMENT ORGANOGRAM 6 8 2.2 SINHA DYEING & FINISHING LIMITED (SDFL) PRETREATMENT 11 2.3 DYEING 26 2.4 FINISHING 31 2.5. QUALITY ASSURANCE LAB 37 2.6 DYEING LAB 40 3. KNIT DYEING 42 3.1 DYEING LAB 50 4. YARN DYEING 51 5. EFFLUENT TREATMENT PLANT 54 6. WATER TREATMENT PLANT 59 7. CONCLUSION 61 1. 1.4 2.1 7 4|Page 1. INTRODUCTION Textile technology education is based on industrial ground. Theoretical background is not sufficient so, industrial training is an essential part of study to make a technologist technically sound in this field. Industrial training provides us that opportunity to gather practical knowledge. Sinha Textile Group is a truly integrated undertaking. The textile division has the capability to offer a complete product range for the export & domestic textile markets. The goal of the textile division is to become the preferred partner for sourcing high quality fabrics & clothing from Bangladesh. With high advanced technology & an emphasis on developing local human resources, the textile division has the potential to make an important contribution to the nation’s growing readymade garments export sector. The rationale behind the existing structure & future expansion of the textile division is to capture value added at each stage of the textile manufacturing process. Despite Bangladesh’s lack of indigenous cotton production capability, STG has leveraged Bangladesh’s labor cost advantage & export competitiveness to maximum level. 1.2 BASIC DESCRIPTION OF TEXTILE The term ‘Textile’ means originally a woven fabric, but textile & the plural textiles are now also applied to fibre, filament & yarn. Natural & manufactured & most products for which these are a particular raw material. This definition embraces, for example fibre- based products in the following categories: threads, cords, ropes & braids; woven, knitted & non woven fabrics, lace, nets & embroidery; hosiery knitwear & made up apparels; household textiles, soft furnishing & upholstery; carpets & other floor coverings; technical, industrial & engineering textiles include geo textiles & medical textiles. Some necessary terms in textile processing & production are given belowFibre: Textile raw materials generally characterized by fineness, Flexibility & high ratio of length to thickness. Yarn: A product of substantial length & relatively small cross section consisting of fibre(s) and/or filament(s) with or without twist. 5|Page Fabric: A manufactured assembly of fibres and/or yarns that has substantial surface area in relation to its thickness & sufficient cohesion to give the assembly useful mechanical strength. Common processes of fabric manufacturing are weaving, knitting & non woven. 1. Weaving: The action of producing fabric by interlacing of warp & weft threads. 2. Knitting: The process of manufacturing of fabric by the intermeshing of loops of yarn. 3. Non-woven: The process of producing of fabrics by chemical bonding of fibres. 1.3 GENERAL INFORMATION ABOUT FACTORY Name of the factory: Sinha Textile Group Owner of the mi: Mr. Anisur Rahman Sinha Location of the mill: Kanchpur, Sonargaon, Narayanganj Head office : House No.363 Road No.02 New DOHS, Mohakhali Dhaka-1206 Commercial production: 1997 Total production: 50000-70000 m/day (woven) 15 ton/day (knit). Business line: Manufacturing & Marketing of high quality yarn & fabric. 6|Page Total turnover: Vision: Building a true marketing led enterprise with motivated workforce, innovative vision, and strong revenue based product portfolio, customer satisfaction & understanding of global market. Mission: Each of the activities must benefit & add value to the common wealth of our society. We firmly believe that, in the final analysis we are accountable to each of the constituents with whom we interact; namely our employees, our customers, our business associates, our fellow, citizens & our shareholders. 1.4 MANAGEMENT ORGANOGRAM Manpower of Sinha Textile Group Sinha Textile Group is running with strong manpower in total. At present about 65,000 people involved here. Every section of STG has sufficient manpower to ensure its smooth running of production in every shift. As I completed my industrial training on Sinha Dyeing & finishing sector so here I am giving the sectionwise manpower of that sectionTotal manpower of Sinha Dyeing & Finishing sector is 301. Manpower of SDFL: Section Manpower Pretreatment 66 Dyeing 63 Finishing 57 Printing 27 Inspection & rolling 22 Quality control 14 Testing laboratory 12 Maintenance 32 Accounts 06 Store 08 7|Page 2.1 SINHA DYEING & FINISHING LIMITED (SDFL) Layout of Sinha Dyeing & Finishing Limited SINHA DYEING & FINISHING LIMITED Here, A- Singeing & Desizing Machine B- Continuous Scouring & Bleaching Machine C- Mercerizing Machine D1- Thermosol Dyeing Machine D2- Pad Steam Machine E1- Electrolyte Control Dyeing Machine E2- Washing Machine P- Screen Printing Machine K- Color Kitchen L- Loop Steamer S- Stenter Machine F- Sanforising Machine I- Brush Machine H- Peach Machine R- Calendaring Machine T- Inspection & Rolling Machine FFS – Finished Fabric Store MR – Mechanical Room ER - Electrical Room RFS – R&D Fabric Store GFS – Grey Fabric Store PS - Printing Section DR – Design Room 8|Page QC – Quality Control Section TL – Textile Testing Laboratory CR – Conference Room DT – Director (Technical) Room Pr.M- Printing Manager’s Room DM – Dyeing Manager’s Room Ad.M- Administration Manager SPZ – Spare Parts Zone – Emergency Exit Way - Fire Extinguisher ST - Staff Toilet Daily production of Sinha Dyeing & Finishing Limited: Woven Dyed Fabric-- 45000m/day Yarn Dyed Fabric-- 10000m/day Printed Fabric-- 20000m/day Process Flowchart Though Sinha Textile Group is a composite mill. For that reason grey fabrics are come from four weaving unit (Somet1, Somet2, Toyota & Picanol) in SDFL (Sinha dyeing & finishing limited). Fabrics are inspected in weaving section & 2nd time inspection is not held. In Sinha Dyeing & Finishing Ltd. scouring-bleaching is done in one machine. Process flow chart in wet processing are given below- For solid dyed fabric………………………………. Desizing Scouring Bleaching Mercerizing Heat setting (for TC/CVC fabric only) Dyeing 9|Page Stenter finishing Sanforizing Inspection & rolling Packing Delivery For white fabric………………………….. Singeing Desizing Scouring Bleaching Re-bleaching Mercerization Stenter finishing Sanforizing Inepection & rolling Packing Delivery For yarn dyed fabric………………………….. Inspection Singeing Desizing Washing Finishing Inspection & Rolling Packing Delivery 10 | P a g e 2.2 PRETREATMENT 2.2.1Theory of Pretreatment The term “Pretreatment” covers all operations of preparing textile material for subsequent dyeing, printing & finishing processes. Objective: The preparation of goods for dyeing & printing is a far important process then the production of white goods. Textile material to be dyed or printed must have the following properties- High & uniform dye uptake & absorptivity. Completely free from husks. High degree of polymerization of the cellulose. Adequate degree of whiteness to permit faultless dyeing of pale shades. Degree of whiteness: In the past, it was customary to regard the degree of whiteness as the most reliable criterion for judging the quality of the pretreatment. But now there are other factors governing the results obtained in subsequent operations. Today, therefore, the object of pretreatment is not full bleach, but only a partial bleach as necessary to ensure good purity & brilliance of shade in subsequent dyeing or printing. Hydrophilic properties: High & uniform absorptivity of the goods is essential. It is the hydrophilic properties that govern the evenness of uptake of the dyes & chemicals, particularly in cases where these are applied continuously. Swelling state: Swelling changes the inner surface of the cotton fibre & consequently its sorption behavior. Maximum, uniform swelling of the cellulose is therefore, essential for complete & level uptake of dye. This can be ensured by Removing the hydrophobic impurities from the fibre. Treatment with alkali in scouring, bleaching, mercerizing etc. Full-width, tight-strand passage of the goods during the swelling process. 11 | P a g e Solubilizing & washing out of impurities: The purer the cellulosic fibre, the greater the assurance that the desired quality & uniformity of the pretreatment effect will be obtained. When the impurities of the cotton fibre have been solubilized, only the chemical problem has been solved. The next step is to remove by washing large amount of various substances in as short a time as possible. Following processes are held in pre-treatment sectionSingeing Desizing Scouring Bleaching Mercerizing 2.2.2 Singeing Singeing is the process by which protruding fibres are removing from the surface of a fabric. Since spinning of yarn from short lengths of fibres essentially involves making a bundle of fibres parallel to each other followed by drawing & twisting, the ends of some of the fibres are likely to protrude from the surface of yarn while those of the bulk of the fibres may be considered as trapped inside the yarn. When such yarn is used in weaving, these free fibre ends along with vary short fibre lengths, protrude from the surface of the fabric, giving it a fuzzy appearance. They destroy the smooth & lustrous character of the fabric surface. Fabric like satin, sateen’s poplin twill etc, are valued for their smooth appearance. Therefore, in most of the cases, the protruding fibre has to be removed & this is done by a process called singeing. There are three types of singeing machines1. Gas singeing machine 2. Plate singeing machine 3. Roller singeing machine Gas singeing machine is used in Sinha Dyeing & Finishing sector. There are two gas singeing machines in Sinha Dyeing & Finishinig sector. Machines areMachine no.1 Name of machine: Parex-mather Manufacture: 1995 Origin: Manchester, England 12 | P a g e Air pressure at cabinet/injector: 410mm WG Gas pressure at inlet to controller: 100-150mm WG No of burner: 2 Capacity of singeing: Both of face side and face & back side Flame height: 2-3 inch Speed of the machine: 70-75m/min Distance burner to product: 6mm Process sequence of “Parex-mather” machine: Pre-heating Brush Singeing Desizing Batching Picture of “Parex-mather” machine: Machine no.2 Name of machine: Carbomatic Origin: Belgium Number of burner: 2 Number of beater: 2 Capacity of singeing: Only face side singeing Flame height: 5-7 inch 13 | P a g e Speed of machine: 120m/min (generally used) Speed of machine: 150m/min (maximum) Distance burner to product: 6mm Padder pressure: 2-2.5 bar Dozing system: Automatic Process sequence of “Carbomatic” machine: Preheater Brush Singeing Beating Desizing Batching Picture of “Carbomatic” machine: 14 | P a g e 2.2.3 Theory of Gas Singeing Machine The machine essentially consists of two burners giving continuous flat flames, produced by a mixture of compressed air & gas. The flame issues from a narrow slit, which is adjustable with to width & thickness. When the cloth is drawn over the flame at a high speed, the flame impinges on its surface & burns the protruding fibres without damaging the cloth to any appreciable extent. The speed of transmission of the cloth through the singeing machine has to be adjusted to suit the amount of the singeing required, without the risk of burning the cloth. When the flame impinges on the cloth surface, the fibre ends present in the interstices of the warp & weft are also singed. Then the singed cloth passed through the desizing bath. So that all the sparks are extinguished. In order to remove the burns fibres & exhaust gases, a fan is providing over the machine. Control of the burning is very important in singeing. The burner be a iron pipe with suitable perforations along its length. This burner is of the slot type with an arrangement for varying the width of the slot so that gases of different calorific value can be used in the machine. As the fabric passes between two slot burner & the exhaust chamber, the flame is drawn directly into the directly into the fabric. The singeing takes place at this stage & the products of combustion are led into the exhaust chamber & taken away from the machine. The slot length can be adjusted according to the width of the cloth being singed. In case of synthetic fibre fabrics, especially those made from thermoplastic fibres such as polyester, nylon etc problem arise in singeing. During singeing such fabrics, the protruding fibres melt & recede from the flame form minute beads. These being disoriented, absorb the dye-faster than the rest of the fabric resulting in specky dyeing. In order to avoid this differential dyeing character of the singed fabric, singeing operation is carried out after dyeing, In case of polyester/cellulose fibre blend, singeing is the best method of controlling piling. It is a critical operation, since an otherwise satisfactory piece of the blend can be rendered useless by uneven/over singeing. The polyester fibre ends melt during singeing. If the machine runs too slowly the flame may become too hot for certain area of the fabric being singed, which then becomes plasticize. Improper singeing may lead to as much as 75% tensile strength loss in the warp direction. 15 | P a g e 2.2.4 Desizing After singeing fabrics comes for desizing unit. It is necessary to remove the size (i.e. to desize) from the cloth; other the hydrofobicity of the wax & the fallow hinder the subsequent dyeing & printing processes. Wax & tallow are removed in the later process (scouring), while the starch is removed during desizing. Thus desizing is the term usually restricted to the process of removal of starch (of the size) from the cloth. Chemically starch is poly-alpha-glucopyranose in which straight chain (amylose) & branched chain (amylopectin) polymers are present. Both the constituents of starch are insoluble in water, but they can be solubilised by hydrolysis of these long chain compounds to shorter ones. Thus under suitable conditions starch can be progressively hydrolyzed to yhe following stagesStarch (insoluble) Dextrin (insoluble) Soluble dextrin (soluble) Maltose (soluble) Alpha-glucose (soluble) In desizing, the hydrolysis reaction is carried out up to the stage of soluble dextrin only & no further to alpha-glucose. Desizing is a chemical process & the rate of this process i.e. the rate of hydrolysis of starch can be controlled. For example, if the desizing liquor is stronger, the process can be completed in a short time in a short time so that the process can be made a continuous one. If weaker solutions are used, the process is bound to be a batch one. Classification of desizing methods: Desizing Methods Hydrolytic Methods Rot steep Enzyme steep Acid steep Oxidative Methods Chlorine Chlorite Bromite 16 | P a g e Another methods of desizing Solvent desizing Low temperature plasma treatment Desizing by thermochemic alextraction & coronization (glass). In Sinha Dyeing & Finishing sector “Rot Steep” & “Acid Steep” desizing method is used. Recipe for rot steep desizing: Water: 1000 liter Wetting agent (Felosan RGN): 1gm/ liter Temperature: 60-800C When only finfix & wax are used as sizing chemical then in desizing process only wetting agent is used in rot steep method. But when starch, fat are used as sizing chemical then to remove these chemicals acid steep method is used. In case of acid steep method “Heptol EMG” (mild acid) is used as a desizing chemical. Process control in desizing: Nature of size: Starch Wet pick up during desizing: 100 %( adjusted by pressure) Concentration of desizing agent: 0.8% Batching time: 6-8 hours Desizing efficiency: Should be 80% 2.2.5 Scouring Scouring is almost invariably the first wet process applied to textile materials. The object is remove oils, fats, waxes, soluble impurities and any particulate or solid dirt adhering to the fibers. The process consists essentially of treatment with a detergent with, or without, the addition of an alkali. When soap is used a 17 | P a g e good supply of soft water is essential but this is of less importance with the synthetic detergents, which, now occupy such a prominent position After the cloth still contains fats and waxes (both natural and added), due to the presence of which the cloth becomes non-absorbent. These are removed from the cloth by scouring, also called kiering, kierboiling, boiling out etc. Objective of scouring: To remove the natural as well as added impurities as completely as possible to from textile material. To produce hydrolytic characteristics. To produce a clean material by adding alkali. To make the fabric suitable for the next process. To leave the materials in a highly absorptive condition without undergoing physical and chemical damage. The main purpose of scouring cotton fabrics is to remove natural as well as added chemicals of essentially hydrophobic character as completely as possible and leave the fabric in a high absorptive condition without undergoing chemical or physical damage significantly and also to make the goods suitable for removing the natural coloring matter of cotton during the subsequent process. The main processes occurring during scouring are Saponification of fats into water-soluble soap and water-miscible glycerin under alkaline condition, Hydrolysis of proteins into water-soluble degradation products, Dissolution of hydrolysis to ammonic of simpler amino compounds, Conversion of pectin and into their solution salts, Dissolution of mineral matter, Emulsification of unsaponificable oils and waxes, and Removal of dirt particles from the kier liquor by the detergent present therein. Scouring process: 1. Batch or Discontinuous process (e.g. Kier boiling process) 2. Continuous process( e.g. Scouring in J-box) 3. Semi- continuous process (e.g. Pad-roller process) 18 | P a g e In Sinha Dyeing & Finishing sector “Continuous Method” is used. Process sequence of scouring-bleaching: Washing Chemical padding Steamer Washing Drying In Sinha Dyeing & Finishing sector two machines are used for scouring-bleaching purpose. Machines areMachine No.1 Name of machine: Benninger Manufacture: 1995 Origin: Switzerland Speed of machine: 120-130m/min (generally used) Speed of machine: 150m/min (maximum) Number of washing bath: 2 (at first stage) Number of washing bath: 4 (at last stage) Number of dry cylinder: 24 Name of chemical padding bath: Impacta Number of chemical tank: 2 Some details about this machine Number of roller in first washing bath: 24 Number of supporting roller in first washing bath: 6 Number of roller in second washing bath: 18 Number of supporting roller in second washing bath: 6 Number of roller in third washing bath: 17 19 | P a g e Number of supporting roller in third washing bath: 5 Number of roller in fourth washing bath: 17 Number of supporting roller in fourth washing bath: 5 Number of roller in fifth washing bath: 17 Number of supporting roller in fifth washing bath: 5 Number of roller in sixth washing bath: 18 Number of supporting roller in sixth washing bath: 6 Number of dry cylinder in first stage: 12 Number of dry cylinder in second stage: 12 Number of padder: 2 Number of squeezer: 6 Number of winder: 1 Temperature in first washing bath---- 500-700C Temperature in last four washing baths: Bath No.1---- 950C Bath No.2---- 950C Bath No.3---- 850C Bath No.4---- 400C Temperature in steamer---- 1000C Temperature in dry cylinder---- 1400C Vapor pressure in steamer---- 650C Reaction time in steamer---- 20 min Fabric stored in steamer at a time---- 100 meter Production capacity per day---- 80,000-1, 00000 meter 20 | P a g e Function of supporting roller: To maintain tension. To maintain fabric width. Function of squeezer: To squeeze & wash out extra water. Picture of “Benninger” machine: Machine No.2 Name of machine: Kuster Manufacture: 2004 Origin: Germany Speed of machine: 70m/min (generally used) Speed of machine: 100m/min (maximum) Number of washing bath: 2 (at first stage) Number of washing bath: 5 (in last stage) Number of dry cylinder: 22 Name of chemical padding bath: Flexnip Number of chemical tank: 6 21 | P a g e Some details about this machine Number of roller in first washing bath: 12 Number of roller in second washing bath: 12 Number of roller in third washing bath: 13 Number of roller in fourth washing bath: 22 Number of roller in fifth washing bath: 22 Number of roller in sixth washing bath: 12 Number of roller in seventh washing bath: 6 Temperature in first washing bath---- 450-550C Temperature in last four washing baths: Bath No.1---- 950C Bath No.2---- 950C Bath No.3---- 950C Bath No.4---- 800C Bath No.5---- 400C Temperature in steamer---- 1000C Vapor pressure in steamer---- 650C Fabric stored in steamer at a time---- 80 meter Temperature in dry cylinder---- 1400C Reaction time in steamer---- 20 min Factors involved in scouring: When cleaning solid surfaces, five variables become involved that interact during scouring and they are as follows: 1. 2. 3. 4. 5. The nature of the surface to be c leaned. The nature of the dirt or soil. The chemicals to be used. The nature of the water or solvent. The nature of the detergent or soap. 22 | P a g e Chemical Use Caustic(NaOH) Neutralize acidic materials, saponify glycerides (Waxes and Oils,) and solubilize silicate. Penetrate and break down lignins in motes. Reduces surface tension and minimize interfacial tensions. Emulsify oils, fats, and waxes; remove oil borne stains; suspend materials after they have been removed. Deactivate metal ions. Cause detergents to become increasingly effective. 1. Assist emulsification by dissolving oily materials. Sodium Silicate Surfactant Detergent Chelating(Sequestering) agent Builder(Salt) Solvent Table: chemicals and their purposes 2.2.6 Bleaching Bleaching is a process, which is designed to produce white fabrics and must be accomplished with a minimum of damage to the cotton being bleaching. Bleaching is not a cleaning process in the sense of scouring; bleaching does not remove dirt. Bleaching is an oxidation process whereby coloring matter is destroyed (not removed) and cotton invariably is degraded. Production personnel must be aware that degradation is part of the process and must be regulated in a way so that satisfactory whiteness is obtained while fabric properties are maintained within customer specification. The removal of cotton wax, natural fats and added fatty matter (of the size) and others components from the desired fabric during the scouring process carried out in a kier leaves the material in a more absorbent condition than the fabric. But the natural coloring matter of the cotton is still present in the cloth. In order to obtain white cloth (so that pure or pale shades are produced on it either by dyeing or printing), the normal is to decolorize the natural coloring matter present in the cloth. Bleaching in different ways does this. An effective bleaching process must ensure pure and permanent white level dyeing properties (overbleaching and under-bleaching adversely affect the dye absorption properties of the fabric) and the fabric too should not undergo not chemical damage or degradation during bleaching. A control over the bleaching agent, the pH, and temperature of the solution, the duration of bleaching, the presence of catalysts like rust etc. On the cloth during bleaching should be in order to minimize or prevent any chemical damage of the cloth being bleaching or wastage of the bleaching agent by self-decomposition. 23 | P a g e Types of bleaching agents: There are different types of bleaching agents are used- Reducing bleaching agents 1. Sulphur dioxide 2. Sodium dithionite 3. Sulphoxylates Oxidizing bleaching agents 1. 2. 3. 4. 5. 6. 7. Sodium hypochlorite Hydrogen peroxide Sodium peroxide Sodium perborate Sodium percarbonate Peracetic acid Sodium chloride PH effect in bleaching: In Sinha Dyeing & Finishing sector PH used in bleaching---10.5-11.8 Perfect PH for bleaching--- 10.5 Fabric in steamer: Fabric stays in steamer---- 20 min Maximum time to fabric stay in steamer--- 30 min In case of rebleach fabric stay in steamer--- 8 min 2.2.7 Mercerizing Mercerizing require cotton to be treated with concentrated solutions of sodium hydroxide (caustic soda). Mercerization requires higher concentration of caustic soda (120Be-240Be). Caustic soda solution swells cotton fibres breaking hydrogen bonds & weak vander wall forces between cellulose chains. The expanded, free chain rearranges & re-orient & en the caustic soda is removed the chain form new bonds in the reorganized state. When done tensionless, the cotton fibre swells, the cross-section becomes thicker & the length is shortened. Because of fibre thickening the fibre becomes denser, stronger & more elastic. Held under tension, the coiled shape of the fibre is straightened & characteristic lumen almost disappears. 24 | P a g e Object of mercerizing: To fix dimensional stability of the fabric. To improve dye uptake of the fabric. To increase strength of the fabric. To increase smoothness of the fabric. To increase luster effect of the fabric. To remove crease from the fabric. Process sequence of ‘mercerizing’: NaOH penetration Reaction time Stabilization Wash out There are two machines in Sinha Dyeing & Finishing sectorName of machine: Farmer Norton Origin: England Speed of the machine: 35-40m/min Number of chemical bath: 2 (NaOH padding) Number of wash bath: 9 Number of acid wash bath: 1 Number of timing cane: 12 Number of dry cylinder: 16 Number of padder: 6 Number of dancing roller: 18 Number of band roller: 23 Temperature of dry cylinder: 1200-1400C Temperature of NaOH padding bath: 150C Temperature of acid wash bath: 900-950C 25 | P a g e Picture of ‘mercerizing’ machine 2.3 DYEING Dyeing can be defined as that process in course of which a textile fibre, placed in contact with the solution/dispersion of a dye absorbs said dye in such a way that the dyed material opposes a certain resistance to releasing the dye to the bath from which it has been absorbed. Such resistance to release the dye is a consequence of its bonding energy, which in its turn, depends on the relationship between the molecular structures of the two substances & the way in which the dyeing was carried out. Dyestuffs give color to the material onto which they have been anchored by selectively retaining some of the wavelengths out of the light falling upon the surface. In Sinha Dyeing & Finishing sector reactive dyes are used maximum. There are three machines in dyeing sector. Two dyeing machines & one washing machine. There are two types of dyeing machines here. Machines are Pad-dry-pad-steam Pad-dry-thermofix Machine Details Type of machine: Pad-dry-pad-steam Padding zone Name of machine: Kusters Origin: Germany Mnufacture: 1996 Model No: E.u.A Kombi Drying zone Name of machine: Monforts Origin: Germany Manufacture: 1995 Pad steam zone Name of machine: Benninger Origin: Switzerland 26 | P a g e Manufacture: 1995 Model: CH-9240 uzwill Process sequence of pad-dry-pad-steam Padding IR Dryer with gas burner Padding Fixation Wash out Dry in dry cylinder Chemical used in pad-dry-pad-steam In first time padding: Dyes Wetting agent In second time padding: Anti-migrating agent Acetic acid NaOH Salt Wetting agent Temperature of different zone First padding bath -- 35-400C Second padding bath -- 35-400C Dryer -- 170-1800C Steamer -- 1000C Dry cylinder -- 1400C First wash bath -- 950C 27 | P a g e Second wash bath -- 950C Third wash bath -- 950C Fourth wash bath -- 950C Fifth wash bath -- 950C Sixth wash bath -- 950C Seventh wash bath -- 400C Others information about pad-dry-pad-steam Speed of machine: 30 m/min (for lycra) & 25 m/min (without lycra ) Speed of IR: 40 m/min Water removed by IR: 40% Number of dry cylinder—15 Number of steaming roller in steamer—48 Reaction time in steamer—1 min Type of machine: Pad-dry-thermofix Name of machine: Monforts Origin: Germany Manufacture: 2005 This machine is also called “E-control” i.e. electrolyte control. Because of dyeing without electrolyte it is saying that “E-control”. Process sequence of pad-dry-pad-steam Padding IR Dryer with gas burner Fixation Wash out Dry in dry cylinder 28 | P a g e Chemical used in pad-dry-pad-steam NaOH Na 2CO3 Wetting agent Anti-migrating agent Information about pad-dry-thermofix Number of padding bath: 1 Number of gas burner: 2 Temperature of dryer: 1000C (maximum) Tempaerature of dryer: 1200C (minimum) Percentage of steam used: 30% Liquor concentration of pad-dry steam: 4:1 Type of machine: Washing machine Name of machine: Kusters Origin: Germany Number of washing bath: 10 Speed of washing bath: 80 m/min (maximum), normally used 45-60 m/min. Temperature of every washing bath First washing bath -- 400C Second washing bath -- 500C Third washing bath --600C Fourth washing bath --600C Fifth washing bath --900C 29 | P a g e Sixth washing bath --950C Seventh washing bath --950C Eighth washing bath --800C Ninth washing bath --700C Tenth washing bath -- 400C Without hot water no other thing used in washing bath. Type of machine: Jigger dyeing Name of machine: Jig-Matic Origin: U.S.A Speed of machine: 900 m/min (maximum), normally 100 m/min is used. Chemical used in jigger dyeing Dyestuff Salt Soda Detergent (for soaping) Temperature of dyeing -- 650C Temperature of soaping -- 980C 30 | P a g e 2.4 FINISHING Various types of finishing areStiff finish Regular finish Resin finish Water repellent finish Wrinkle free finish Stentaring Purpose of stentaring: To control width of fabric. To increase smoothness on fabric surface. For heat setting in case of lycra fabric. Sometimes topping is also done. To control moisture of fabric. Machine Details Number of machine: 3 Machine No. 1 Name of machine: Monforts Origin: Germany Manufacture: 1996 Model: E.u.A Kombi Used fabric type: Woven Number of drying chamber: 6 31 | P a g e Number of gas burner: 12 One special roller is used in this machine for removing crease in case of yarn dyed fabric. Machine No. 2 Name of machine: Monforts Origin: Germany Manufacture: 1994 Model: E+A Komb Used fabric type: Woven & knit Number of drying chamber: 6 Number of gas burner: 12 Two special rollers are used for removing crease of knit fabric. Machine No. 3 Name of machine: Icomatex Origin: Spain Manufacture: 2007 Model: Terassa Used fabric type: Woven Number of drying chamber: 4 Number of gas burner: 8 Temperature of every chamberFirst -- 800C Second -- 1000C Third -- 1200 C Fourth -- 1800C Fifth -- 1800C Soxth -- 1800C 32 | P a g e Seventh -- 1800C Eighth -- 1400 Chemical used in finishing: Persoftal BD -- Cationic softener Adasil SM -- Anionic softener SBN -- Non-ionic softener Softener is used On the basis of buyer requirement. On the basis shade. Speed of machine: 120 m/min maximum & normally 65-70 m/min is used. Topping is also done by stentaring machine. Topping temperature is 800C, 1000C, 1200C. Sanforozing Purpose of sanforizing: To control GSM. To control shrinkage. Machine Details Number of machine: 3 Machine No. 1 & 2 Name of machine: Monforts Origin: Germany Manufacture: 1996 Model: Monfortex Machine No. 3 33 | P a g e Name of machine: Morrison Origin: U.S.A Manufacture: 2005 Speed of machine: 40 m/min Pressure & temperature is used for control shrinkage. Peach Finish There are 4 types of peach finish areLight peach Microsand peach Normal peach Heavy brush peach Features of peach finish areLight peach: Smoothness or peach effect is low. Microsand peach: Smoothness effect is greater than light peach & lower than normal peach. Normal peach: By using this type of peach fabric can be smooth much. Heavy brush peach: Smoothness effect is more than any other type of peach. “Sand paper” takes a major part in peach finish. Varieties grade sand paper is used in peach finish Name of peach Sand paper in grade 34 | P a g e Light peach 220, 400, 600 Normal peach 220, 400, 600, 320 (2 times used) Microsand peach 220, 320, 400, 600 Heavy brush peach 80, 120, 320 “Sand papers” are rapped on sand roller. Machine Details Number of machine: 3 (5 peach machines & 1 calendaring machine) Machine No. 1 Name of machine: Gessner Origin: U.S.A Manufacture: 2003 Model: Sander Speed of machine: 20-25 m/min for both of peach. Number of sand roller: 4 Number of brush roller: 1 Machine used for: Normal peach, heavy brush peach. Machine No. 2 Name of machine: Gessner Origin: U.S.A Manufacture: 2003 Model: Sander Speed of machine: 20-25 m/min for normal & heavy brush peach, 20-35 m/min for microsand peach. Number of sand roller: 4 Number of brush roller: 1 Machine used for: Normal peach, microsand peach, heavy brush peach. 35 | P a g e Machine No. 3 Name of machine: Santex Origin: U.S.A Manufacture: 2005 Model: Plurima Speed of machine: 20-25 m/min for normal peach, 20-35 m/min for microsand peach & 35-40 m/min for light peach. Number of sand roller: 4 Speed of sand roller: 1100 m/min Number of brush roller: 1 Machine used for: Light peach, normal peach & microsand peach. Both dry & wet peach are held here. Machine No. 4 Name of machine: Danti paolo Origin: Italy Manufacture: 2007 Model: S1000 Number of sand roller: 2 Number of brush roller: 4 Number of dancing roller: 2 (it is used for maintain fabric tension) Machine No. 5 Name of machine: Lamperti Origin: Italy Manufacture: 1998 It is a calendaring machine. 36 | P a g e 2.5 QUALITY ASSURANCE LAB Machines are- Picture: Wash Fastness Tester & Quick Wash Plus Machine (one type of wash fastness tester) Picture: Wash Fastness Tester & Washing Machine Picture: Light Fastness Tester & Tensile Strength Tester 37 | P a g e Picture: Dryer Picture: Color Assessment Cabinet & Hygrometer Picture: Picture: Tearing Tester & Crease Recovery Tester 38 | P a g e Picture: Abrasion & Pilling tester, Flammability Tester Picture: Bursting Tester & Rubbing Fastness Tester Picture: TPI tester & Perspiration tester Picture: Stretch & growth tester 39 | P a g e 2.6 DYEING LAB Machines are- Picture: Dryer & Padder Picture: Dryer & Padder Picture: Steamer & Jigger Dyeing Machine Picture: Mixture of Salt & Soda for padding 40 | P a g e Picture: Stock of dyes in dyeing lab Picture: Working elements for dyeing in lab Picture: Color Assesment Cabinet & Spectrophotometer 41 | P a g e 3. KNIT DYEING PRODUCT VARIATION The product, which are available in knit dyeing floor are given below: → Single jersey / Single jersey with lycra → Polo pique, Lacost (Single / Double) → Rib - (1x1), (2x2), (8x2), (9x2), (9x1) → Lycra rib, Drop needle fabric → Interlock → Grey mélange → Stripe (S/J, rib, interlock, grey mélange) Raw materials for knitting: Type of yarn Count Cotton 20S, 24S, 26S, 28S, 30S, 32S, 34S, 36S, 38S, 40S, 45S Polyester 70D, 100D, 150D Spandex yarn 20D, 40D, 70D Grey mélange 24S, 26S Ecru melange 24S, 26S, 28S Cotton mélange (100%) 24S, 26S, 28S PC (65% polyester, 35% cotton) 24S, 26S, 28S,30S 42 | P a g e CVC (60 % polyester, 40% cotton) 24S, 26S, 28S, 30S Source of yarn for knitting: Lycra: Sinha rotor spinning Ltd. Arif textile HK Spinning Padma Textile Prime Textile Kader Synthetic Shohagpur textile Jamuna spinning Shamim spinning Amber textile Yasmeen spinning Square textile CREORA Made in Korea, Type # H-100 (20D) Raw materials for dyeing: Raw materials used in the dyeing section are1. Grey fabrics 2. Dyes 3. Chemicals Grey fabrics: Following types of gray fabrics are dyed- 43 | P a g e Process sequence of knit dyeing Fabric receiving Fabric inspection Batching Scouring & Bleaching Dyeing After treatment & Softening Fixing Dewatering/ Squeezing Drying Compacting Final Inspection Machine Details Machine No.1 Brand Name: FONGS Model:-WINCH GN 18 2T (Atmospheric) Origin: Hong Kong Capacity: 600 Kg No. of Nozzle: 03 Max. Operating Temperature: 950 C Max. Operating Presser: .75 Bar Manufacturing Year: 1996 Fong’s Machine No. 02 44 | P a g e Brand Name: FONGS Model:-WINCH DW 2T (Atmospheric) Origin: Hong Kong Capacity: 300 Kg No. of Nozzle: 02 Max. Operating Temperature: 950 C Max. Operating Presser: .75 Bar Manufacturing Year: 1996 Fong’s Machine No. 03 Brand Name: FONGS Model:-WINCH DW 3T (Atmospheric) Origin: Hong Kong Capacity: 500 Kg No. of Nozzle: 03 Max. Operating Temperature: 950 C Max. Operating Presser: .75 Bar Manufacturing Year: 1996 Fong’s Machine No. 04 Brand Name: Tecninox Origin: Portugal Capacity: 1000 Kg No. of Nozzle: 05 Max. Operating Temperature: 1050 C Max. Operating Presser: 1.5 Bar Manufacturing Year: 1997 Machine No. 05 45 | P a g e Brand Name: Tecninox Origin: Portugal Capacity: 1000 Kg No. of Nozzle: 05 Max. Operating Temperature: 1050 C Max. Operating Presser: 1.5 Bar Manufacturing Year: 1997 Machine No. 06 Brand Name: Tecninox Origin: Portugal Capacity: 1200 Kg No. of Nozzle: 05 Max. Operating Temperature: 1050 C Max. Operating Presser: 1.5 Bar Manufacturing Year: 1997 Dyeing Machine No. 07 Brand Name: GATSON COUNTRY (high temperature high pressure) Origin: USA Capacity: 500 Kg No. of Nozzle: 02 Max. Operating Temperature: 1400 C Max. Operating Presser: 5 Bar Manufacturing Year: 1996 46 | P a g e Dyeing Machine No. 08 Brand Name: FONGS Model:-WINCH DW 3T (Atmospheric) Origin: Hong Kong Capacity: 500 Kg No. of Nozzle: 03 Max. Operating Temperature: 950 C Max. Operating Presser: .75 Bar Manufacturing Year: 1996 Fong’s Dyeing Machine No. 09 Brand Name: FONGS Model:-WINCH DW 3T (Atmospheric) Origin: Hong Kong Capacity: 500 Kg No. of Nozzle: 03 Max. Operating Temperature: 950 C Max. Operating Presser: .75 Bar Manufacturing Year: 1996 Fong’s Dyeing Machine No. 10 Brand Name: FONGS Model:-WINCH DW 3T (Atmospheric) Origin: Hong Kong Capacity: 500 Kg No. of Nozzle: 03 47 | P a g e Max. Operating Temperature: 950 C Max. Operating Presser: .75 Bar Manufacturing Year: 1996 Fong’s Dyeing Machine No. 11 Brand Name: FONGS Model:-WINCH DW 3T (Atmospheric) Origin: Hong Kong Capacity: 500 Kg No. of Nozzle: 03 Max. Operating Temperature: 950 C Max. Operating Presser: .75 Bar Manufacturing Year: 1996 Fong’s Dyeing Machine No. 12 Brand Name: FONGS Model:-WINCH DW 3T (Atmospheric) Origin: Hong Kong Capacity: 500 Kg No. of Nozzle: 03 Max. Operating Temperature: 950 C Max. Operating Presser: .75 Bar Manufacturing Year: 1996 Fong’s Dyeing Machine No. 13(sample) Brand Name: tecninox (HTHP) Origin: Portugal Capacity: 15 Kg No. of Nozzle: 01 48 | P a g e Max. Operating Temperature: 1000 C Max. Operating Presser: .1.5 Bar Manufacturing Year: 1996 Dyeing Machine No. 14(sample) Brand Name: tecninox (HTHP) Origin: Portugal Capacity: 15 Kg No. of Nozzle: 01 Max. Operating Temperature: 1000 C Max. Operating Presser: .1.5 Bar Manufacturing Year: 1996 Dyeing Machine No. 15(sample) Brand Name: FONGS Model: Winch GNS 1 T Origin: Hong Kong Capacity: 10 Kg No. of Nozzle: 01 Max. Operating Temperature: 950 C Max. Operating Presser: 0.75 Bar Manufacturing Year: 1996 Dyeing Machine No. 16(Washing) Origin: local Capacity: 15 Kg No. of Nozzle: 02 Max. Operating Temperature: 850 C 49 | P a g e Max. Operating Presser: 1bar Manufacturing Year: 1998 3.1 DYEING LAB Picture: Dyeing machine & Working zone Picture: Stock of bleached fabric & Stock of pipette Process sequence of lab dyeing Dyes+Water+Auxiliaries+Fabric+Salt (Continuous stirring for 30 min) After 30 min soda is added After 10 min temperature is raised up to 60-650C Dyeing in this temperature for 1 hour Temperature is fall down Wash off 50 | P a g e M:L=1:8 Fabric weight=5 gm 4. YARN DYEING Process sequence of yarn dyeing Grey Yarn Soft Winding Batch Preparation Scouring & Bleaching Washing Dyeing Soaping Neutralization Softening & Fixing Washing Hydro-extraction Drying Random Winding Packing Delivery Machine Details Type of machine Soft winding Origin Manufacturer Quantity SSM, Fadis Switzerland, Italy 09 51 | P a g e Batch preparation Scholl Switzerland 02 Dyeing Scholl, Galvanin Switzerland, Italy 21 Hydro-extractor Scholl Switzerland 02 Radio Frequency Dryer Stallam, Strayfeild England, Italy 02 Hard Winding Hard Winding Switzerland, Italy 09 Process sequence of dyeing in bulk Ladiquest+Glauber salt (300C in main tank 20 min circulation) 500C color dozing for 30 min 600C color dozing gradually for 30 min+migration 30 min+30 min soda dozing+30 min run Hot wash Rinse Acid wash for neutralization Wash with detergent Hot wash Rinse Acid wash Fixer finish Dyeing Procedure in lab Salt at 500C & run 20 min (Check pH & salt gravity) Color dozing at 500C for 10 min Color migration at 700C for 30 min 52 | P a g e Soda ash dozing at 600C for 20 min Temperature at 600C & run for 30 min Sample check if ok then wash Wash-off process in dyeing lab For light shades: Cold wash Hot wash at 500C Neutralize with acetic acid 0.5 g/l Soap wash with ladiquest 1 g/l at 950C Hot wash at 800C Rinse For medium shades: Cold wash Hot wash at 500C Neutralize with acetic acid 0.5 g/l Soap wash with ladiquest 1 g/l at 950C Hot wash at 800C Rinse For dark shades: Cold wash Hot wash Neutralize with acetic acid Soap wash with avolan 2 g/l at 950C Soap wash with avolan 2 g/l at 950C Hot wash at 800C 53 | P a g e Rinse 5. EFFLUENT TREATMENT PLANT There are 3 “Effluent Treatment Plant” in Sinha Textile Group”. This are ETP 1 ETP 2 ETP 3 Process sequence of ETP 1 (Capacity- 150m3/hour) “It’s a physiochemical plant” All kind of dyeing water came from different dyeing unit Rotary screen filter Equalization tank Chemical reactor Flotation unit Sludge Clean water To river Step discussions All kind of dyeing water comes from different dyeing section: In this segment water comes from different dyeing section. LikeWoven dyeing section Knit dyeing section Yarn dyeing section etc. 54 | P a g e Rotary screen filter: Suspended solid quartz material removed by using this step. Equalization tank: To equalize the effluent quantitatively & qualitatively. Material takes approximately 10 hours time to get clean. Its capacity is 1560 m3. Flotation unit: Chemical dozing (Fecl3, polyelectrolyte, decoloring agent). After flotation unit water goes two sides. One is sludge & another is clean water which is gone into river. Process sequence of ETP 2 (Capacity- 350m3/hour) “It’s a biological plant” Combined effluent from various units Mechanical bar screen Collection tank Pumping Equalization tank Flash mixing tank (by pumping) Flocculation tank Primary claritubesetteler tank PH correction channel FAB reactor 1 FAB reactor 2 Secondary claritubesettler tank 55 | P a g e Chlorine contact tank To river Step discussions Combined effluent from various units: In this segment water comes from different dyeing section. LikeWoven dyeing section Knit dyeing section Yarn dyeing section etc. Mechanical bar screen: To removing the coarse solids. Equalization tank: To equalize the effluent quantitatively & qualitatively. Material takes approximately 10 hours time to get clean. Its capacity is 1560 m3. Flash mixing tank: 2 nos for rapid or uniform mixing of dosing chemicals with the effluent. Flocculation tank: For coagulation & flocculation of solids. Polymer increases the size of dust particles. Primary claritubesetteler tank: To remove the inorganic flocs formed. PH correction channel: To correct inlet pH by HCl dosing. FAB reactor: Treatment of organic matter to reduce BOD/COD aerobically. Secondary claritubesettler tank: To remove the biological solid generated. Chlorine contact tank: 56 | P a g e For polishing & disinfections. Calcium or sodium hypochlorite dosing. Sludge sump: To collect the thickened sludge. Centrifuge: For mechanical dewatering of sludge. Process sequence of ETP 3 (Capacity- 150m3/hour) “It’s a biological plant” Rotary screen Effluent collection tank Chemical dosing Clarifier PH correction channel Biotower Aeration tank Lamela clarifier 1, 2 Chlorine contact tank Multigrade filter To river Step discussions Rotary screen filter: Suspended solid quartz material removed by using this step. Equalization tank: To equalize the effluent quantitatively & qualitatively. Material takes approximately 10 hours time to get clean. Its capacity is 1560 m3. Chemical dosing: Lime, Fe (SO4)3, polyelectrolyte are added in this stage. 57 | P a g e PH correction channel: To correct inlet pH by HCl dosing. Biotower: Atmospheric air is blown in this stage. Chlorine contact tank: For ploishing & disinfections. Calcium or sodium hypochlorite dosing. Process Description The effluent is first passed through a Manual Bar Screen Channel / Chamber to remove any floating debris. The effluent is then collected is a Equalization Tank where it is equalized with respect to its characteristics and flow. The content is kept in mixed conditions with the help of air blower. The equalized effluent is then pumped to flash mixing tank followed by a Flocculation Tank. Chemicals like lime and FeSO4 are dosed in the flash mixing tank to aid coagulation and color removal. Anionic Polly-electrolyte (type-1) is dosed in the Flocculation Tank to aid in the agglomeration of the particles. The flocs formed are removed in the downstream Primary Claritubesttler -1. The effluent will further flow by gravity to a PH correction tank where requisite quantity of acid will be dosed and PH will be adjusted as per the requirement. After the primary treatment effluent flows by gravity to the FAB Rector for reduction of BOD / COD aerobically. The air is supplied by means of fine bubble diffusion. The generated are removed in the Secondary Claritubesettler – 11. The clarified effluent polished and disinfected by dosing sodium hypochlorite in the Chlorine Contact Tank. The disinfected effluent is suitable for disposal. Chemicals are used in ETP-1: Ferric chloride Polyelectrolyte De-coloring agent As a preservativeNaOH H2SO4 Na2SO4 Chemicals are used in ETP-2 &3: 58 | P a g e Lime Ferrus Sulphate Polyelectrolyte HCl- 5% solution Sodium or Calcium hypochlorite- 5% solution. 6. WATER TREATMENT PLANT Process Sequence of WTP Water from river Flash mixer Clarifier Filter pack Clarified water tank Softening plant Soft water to various units Step discussions Water from river: Water comes from various rivers in water treatment plant. Flash mixer: In this segment Al2 (SO4)3, polymer etc are mixed in water. Softening plant: In this segment activated carbon are used as a softener. Soft water to various units: 59 | P a g e After softening of water it is supplied in various units for various purposes. There are two types of water are prepared in water treatment plant Clarified water for washing purpose. Soft water for dyeing purpose. Chemicals are used in WTP Aluminum Sulphate Polyelectrolyte Sodium Chloride Amount of chemical usedPolymer- .1% solution Al2 (SO4)3- 10% solution Lime- 10% solution 60 | P a g e 7. CONCLUSION For every person who is fresher in the field of textile, industrial training works is like a learning route. This course gave me the opportunity to move liberally in every section of the industry to learn the industrial work & follow the process sequence visually . I came to know practical knowledge not only dyeing section but also every section of textile industry. Sinha group contain A to Z function in textile sector . I learned how to work professionally in job field. I many gathered many technical knowledge working by my own hend. I worked hard with a great interest. Because I had Interest to learn every new things. In the production floor the commanding power of the officers, compliance, administration rules everything is appealing. I hope that this industrial training will help me a lot to work in the future period wherever I want to develop my career. Finally wishing the best prospect of both the industry & myself I want to conclude. Thank you. 61 | P a g e