DEPARTMENTOFMATERIALSSCIENCEANDENGINEERING Mat E 453/MSE 553 Physical and Mechanical Properties of Polymers Course Policies and Procedures - Fall 2012* Course Timing Location Instructor TA Office Hours : Lecture – T & Th 8:00 a.m. - 8:50 a.m. Lab – assigned on the first week of class : 1246 Howe Hall (Lecture) : Dr. Michael Kessler, 3053B Gilman Hall / 2220X Hoover Ph. (515) 294-3101 E-mail: mkessler@iastate.edu : Yuzhan Li E-mail: yuzhanli@iastate.edu : Open door policy and by appointment. Course Description: Overview of polymer chemical composition, microstructure, thermal and mechanical properties, rheology, and principles of polymer materials selection. Intensive laboratory experiments include chemical composition studies, microstructural characterization, thermal analysis, and mechanical testing. Prerequisites: Mat E 351. Recommended Text Book: 1. Brazel, C. S., Rosen, S. L. Fundamental Principles of Polymeric Materials, 3rd Ed., John Wiley and Sons, New York, 2012. References: 2. Fried, J. R. Polymer Science and Technology, 2nd Ed., Prentice Hall, Upper Saddle River, NJ, 2003. 3. Kumar, A., and Gupta, R. K., Fundamentals of Polymer Engineering. 2nd ed., Marcel Dekker, Inc., New York, 2003. Blackboard Learn and Website: Additional resources, including lab instructions, will be posted on the course website at http://polycomp.mse.iastate.edu/ Grades, will be posted on the course Blackboard Learn site (http://bb.its.iastate.edu/). * Schedule and assignments are subject to change. Desired Outcomes: The student will: Understand major types of polymeric materials and their primary applications Measure and interpret major physical and mechanical properties of polymers and understand their origin Select and understand major polymer characterization and mechanical testing techniques and their strengths and limitations Search, analyze and compare data on physical and mechanical properties Show improved report-writing skills, communication skills, ability to work in small groups, and delivery of clear oral presentation Grading Policy: Formal Lab Reports (4) Memo Lab Reports (4) Presentation Lab Reports (2) Webpage Report (2) Final Exam Attendance and Participation - 20 % - 20 % - 10 % - 10 % - 35 % - 5% A– (90.1-93.0), A (93.1-100), B– (80.1-83.0), B (83.1-87.0), B+ (87.1-90.0) C– (70.1-73.0), C (73.1-77.0), C+ (77.1-80.0) D– (60.1-63.0), D (63.1-67.0), D+ (67.1-70.0) F (Below 60.0%) Note: There will be 12 laboratory reports by each group. Four reports will require a “Formal Lab Report” format, four will require a “Memo Lab Report” format, two will be in the form of a PowerPoint presentation, and two will be webpage reports. Each person will rate the effort of their group mates on each laboratory report for all members of the group. Ideally, for a group of four students, each student should have a 25% effort. The score given to a particular student will be calculated as follows Student grade = 75% of the report score + (25% of the report score * n), where n is the average reported effort divided by the expected effort. For example, if a report score is 80% and the average effort rating for a student on a team of 4 is 20%, then the students score is 0.75 80 0.25 80 20 / 25 76% . However, if the student’s effort in the same example were 30%, the students score is 0.75 80 0.25 80 30 / 25 84% The final exam is scheduled for Friday, Dec 14, 7:30– 9:30 a.m Academic Misconduct: All students are expected to practice and display a high level of personal and professional integrity. During examinations each student should conduct himself in a way that avoids even the appearance of cheating. Any academic misconduct will be dealt with under the policies of the College of Engineering. The result could be a failing grade and/or dismissal. Note: Students are encouraged to ask questions and participate in lectures, labs, and discussions to make the learning process lively and enriching. Please leave all cell phones and electronic communication devices turned off and put away during class and lab. If you have a disability and require accommodations, please contact the instructor early in the semester so that your learning needs may be appropriately met. You will need to provide documentation of your disability to the Disability Resources (DR) office, located on the main floor of the Student Services Building, Room 1076, 515-294-7220 . The policy of the University regarding withdrawals and incomplete will be adhered to strictly. The instructor may be consulted for any clarifications regarding this course and related academic matters. Lab Schedule Week Experiment Instructor/Supervisor Location Aug. 20 No lab – lab group and time determined first week Aug. 27 Sep. 3 Lab 1: Synthesis of PS and Nylon 6,6 Tom Garrison 3344 Hoover Lab 2: Gel Permeation Chromatography Ying Xia 3311 Gilman Sep. 10 Lab 3: Fourier Transform Infrared Spectroscopy Eliseo De Leon 3344 Hoover Sep. 17 Lab 4: DSC Yuzhan Li 3113 Gilman Sep. 24 Lab 5: Wide Angle X-Ray Diffraction Peter Hondred 3365 Hoover Oct. 1 Lab 6: Polarized Optical Microscopy Yuzhan Li 3311 Gilman Oct. 8 No lab – MS&T Oct. 15 Lab 7: Injection Molding Mahendra Thunga 0124 Davidson Oct. 22 Lab 8: Tensile Testing Amy Bauer 3305 Gilman Oct. 29 Lab 9: DMA Mitch Rock 3113 Gilman Nov. 5 Lab 10: TGA Danny Vennerberg 3113 Gilman Nov. 12 Lab 11: Rheology Samy Madbouly 3113 Gilman Nov. 26 Lab 12: Film Blowing Yuzhan Li 0124 Davidson Dec. 3 Make-up Labs Write-up Assignment Lab # Group 1 Group 2 Group 3 Group 4 Group 5 Group 6 1 Formal Memo Presentation Formal Memo Web 2 Web Formal Memo Presentation Formal Memo 3 Memo Web Formal Memo Presentation Formal 4 Formal Memo Web Formal Memo Presentation 5 Presentation Formal Memo Web Formal Memo 6 Memo Presentation Formal Memo Web Formal 7 Formal Memo Presentation Formal Memo Web 8 Web Formal Memo Presentation Formal Memo 9 Memo Web Formal Memo Presentation Formal 10 Formal Memo Web Formal Memo Presentation 11 Presentation Formal Memo Web Formal Memo 12 Memo Presentation Formal Memo Web Formal