Lab 4B – Putting Bubbles to the Test Answers 1. Tube # Material & Amount 1 3 ml of ammonia solution 2 ml of lead nitrate solution 1 small piece of chalk 1 pinch of baking soda 1 small piece of zinc 2 3 4 5 Appearance Before Adding HCl Clear colorless liquid Observable Changes Clear colorless liquid Yellow cylindrical solid White powder Cloudy white Gray solid, rough surface, irregular shape Slow bubbling Got warmer Tiny bubbles Rapid bubbling 2. Chalk, baking soda and zinc (all bubbled) produced a gas when HCl was added. 3. Ammonia solution nor lead nitrate solution behaved the same way when HCl was added to them. 4. Chalk, baking soda and zinc all had a gas bubble from them when HCl was added to them. Operationally defined, you know a gas is carbon dioxide if turns limewater cloudy, phenol red to yellow, and quickly puts out a burning match. Chalk + HCl → Carbon dioxide and Soda + HCl → Carbon dioxide