Supplementary materials for “Quantitative measurement of in-plane cantilever torsion for calibrating lateral piezoresponse force microscopy” Hyunwoo Choi1,2, Seungbum Hong2,a) and Kwangsoo No1,a) 1 Materials Science Division, Argonne National Laboratory, Lemont, Illinois 60439, USA 2 Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology, Daejeon 305-701, Korea a) Corresponding authors : hong@anl.gov and ksno@kaist.ac.kr 1 Figure S1. Trace and retrace lateral signal images of BaTiO3 single crystal at the scan size of (a) 20, (b) 80 and (c) 400 nm. Effects of the increase in the lateral force on the increases in the absolute values of the lateral torsion signal In order to examine the effects in the increase of the lateral force on the increases in the absolute values of the lateral torsion signals, we scanned BaTiO3 (BTO) single crystal with fixed scan distance of 200 nm under various scan speed (in case of the experiment in the manuscript, scan rate is maintained with 10 Hz, and the scan distance changes). Figure S2 shows the root mean square (RMS) lateral signals of the trace and the retrace scan images as a function of the scan speed (from 400 to 2000 nm/s, with the step of 200 nm/s). One can see that the lateral signal linearly increases as the scan speed increases. 2 Figure S2. RMS lateral torsion signal of the trace and the retrace scan images as a function of the scan speed. Sample is BTO single crystal, and the scan distance is 200 nm. Table SI. Previously reported d31 values of BaTiO3. d31 (pm/V = pC/N) -58a -72b -75c -82d a Reference 1. Reference 2. c Reference 3. d Reference 4. e Reference 5. f Reference 6. b 3 -78e -97.5e -103.3f References 1 Dale Ensminger, Ultrasonics: fundamentals, technology, applications (CRC Press, 1988) 2 D. Liu and J. Li, Appl. Phys. Lett. 83, 1193 (2003) 3 C. B. Cater and M. G. Norton, Ceramic materials: science and engineering (Springer, 2007) 4 R. Tazaki, D. Fu, M. Itoh, M. Daimon and S. Koshihara, J. Phys.: Condens. Matter. 21, 215903 (2009) 5 D. Berlincourt and H. H. A. Krueger, Phys. Rev. 105, 56 (1957) 6 W. L. Bond, W. P. Mason and H. J. McSkimin, Phys. Rev. 82, 442 (1951) 4