SNC 2D Name: ___________________ (develop a title for this experiment) Introduction Water in its natural form is almost never pure H2O. In fact, most water contains many other dissolved substances. When an ionic compound is added to water, it will separate into its ions. For example, when sodium chloride (NaCl) is added to water it will separate into Na1+ and Cl1- ions. Well water that comes from the ground will contain many of the dissolved ionic compounds that are found in the ground. These ions include positive ions like calcium (Ca2+), magnesium (Mg2+), and iron (Fe3+), and negative ions such as chloride (Cl1-), nitrate ((NO3)1-) and sulphate ((SO4)2-). Since ions are not usually visible, chemical tests are used to detect and identify ions in water. Most chemical tests involve mixing two solutions that produce an insoluble solid (precipitate). A positive test is one that clearly indicates the presence of the ion. A positive test may produce a precipitate, colour change or both. In this investigation, you test for the iron ion(Fe3+), chloride ion (Cl-), and sulphate ion(SO4)2-) ions dissolved in three different water samples and one unknown sample solution. Purpose:____________________________________________________________________ ____________________________________________________________________________ ____________________________________________________________________________ Hypothesis: It was believed that the: Materials: Procedure Part 1 1. Complete the title, impersonal purpose, hypothesis (what ions do you expect in the distilled water, tap water, and well water and unknown sample?), and materials section for your report. 2. Examine the three sample solutions and the three testing solutions. Write down three physical properties for each and fill in observation table 1. 3. Add two drops of tester solutions to two drops of each of the sample solutions. Record your observations particularly any changes in colour or formation of precipitate in table 2. Part 2 1. Place two drops of each water sample into three different spots on your tray. Observe the sample of water and record observations in table 2. 2. Add 1 drop of tester solution to each of the water samples. Record your results table 3. 3. Repeat for other two tester solutions in new water samples. Record your results in the provided table. Observations Part 1: (Complete the following tables including observations of all reactants and products) Table 1: Physical Properties of the Solutions Sample 3 Physical Properties Table 2: Identifying Positive Tests for Ions Silver (I) nitrate Testers and formulas Barium chloride → Positive Samples Potassium thiocyanate RESULTS Potassium Chloride Sodium sulphate Iron (III) nitrate Conclusion part 1: 1) Silver nitrate tests for ________________________________ ions. 2) Barium chloride test for _______________________________ ions. 3) Potassium thiocyanate tests for ________________________ ions. Observations Part 2 Table 3: Testing for Ions in Water Samples Testers ---> Samples Silver nitrate Barium chloride Potassium thiocyanate Distilled Water Well Water Tap Water Unknown Conclusion: answer the following questions with complete sentences on your own paper. 1. What is meant by a “positive” test for an ion? 2. Write the chemical formulas for silver nitrate, sodium sulphate, barium chloride and iron (III) nitrate. 3. How could you tell how much sulphate was present in two different solutions by adding barium chloride? 4. List any problems that you had when following the procedure or doing the experiment. Suggest what could be done to improve the experiment. 5. State which ions were found in each of the 3 water samples and the unknown sample. What was your proof for each sample? 6. Where might your unknown sample come from (read introduction)? Explain your answer.