Supporting Information A microelectromechanical system for thermomechanical testing of nanostructures Tzu-Hsuan Chang and Yong Zhu Department of Mechanical and Aerospace Engineering, North Carolina State University, Raleigh, NC 27695, USA Fig. S1. SEM image showing the fabricated MEMS thermomechanical testing device that has a serpentine heating coil that can be resistively heated. Fig. S2. Calculated temperature distribution under 4 volt heating voltage in air. In contrast to Fig. 3(a), the air is included here. 1 Fig. S2 shows temperature distribution of the MEMS stage in air. Due to symmetry, only a quarter of the stage is shown. The temperature decreased rapidly along the shuttle due to the heat conduction to the nearby fixed combs through air gap, which provides additional route by which heat can be dissipated. Under vacuum environment, the only heat dissipation route is to the anchors of the comb drive through the support beams. In order to check if the temperature on the nanowire is the same as that on at point B and if the temperature is uniformly distributed along the SCS nanowire, we conducted Raman-based temperature measurement and ANSYS. As shown in Fig. S3(a), the nanowire is attached on the middle of the shuttle between actuator and force sensor. The diameter of NW was set to be 60 nm, and the length is 2 μm. Noticed that the thermal conductivity of SCS in nano scale (~15 W/mK)1,2 is different from that in micro and macro scale, so it should be treated as a different element type from our SCS based stage. The inset of Fig S3(a) shows that the temperature is uniformly distributed along the SCS nanowire. Temperature difference between the center of the nanowire (point C) and the edge of the device (point B, the same as that in Figure 2a) is only 0.2 K while the temperature of nanowire exceeds 500 K. Fig S3(b) shows the Stokes-shifted Raman spectra of points C and B. The difference of temperature between two points is 2 K. The peak position is a reflection of the temperature according to Eq. 3. The large difference in the spectra amplitude is due to the fact that the probe areas in point C is much smaller than that in point B. 2 Fig S3. (a) Temperature contour of MEMS device and mounted nanowire. (b) Raman spectra of point B and C under 8 V heating voltage in air. References: 1 D. Li, Y. Wu, P. Kim, L. Shi, P. Yong and A. Majumdar, Appl. Phys. Lett. 83, 2934 (2003) 2 J. Anaya, A. Torres, A. Martín-Martín, J. Souto, J. Jiménez, A. Rodríguez and T. Rodríguez, Appl. Phys. A 113, 167 (2013) 3