Which gas is produced when acids react with carbonates? A heaped spatulaful of magnesium carbonate was placed in a boiling tube and clamped. The end of the delivery tube was placed in a test tube of lime water as shown in the diagram opposite. 10 cm3 of sulphuric acid was measured and added to the carbonate. calcium carbonate and sulphuric acid lime water The experiment was repeated using calcium carbonate and nitric acid. Carbon dioxide gas was formed in this reaction. We knew this as it turned limewater milky. Which gas is produced when acids react with carbonates? A heaped spatulaful of magnesium carbonate was placed in a boiling tube and clamped. The end of the delivery tube was placed in a test tube of lime water as shown in the diagram opposite. 10 cm3 of sulphuric acid was measured and added to the carbonate. calcium carbonate and sulphuric acid lime water The experiment was repeated using calcium carbonate and nitric acid. Carbon dioxide gas was formed in this reaction. We knew this as it turned limewater milky.