Quantitative Analysis of Iron Ore Hand-In, Chem 150L, Fall 2015 Name: Partner: See the attached rubric for more detailed information about grading. 1. (2 points) For the iron-phenanthroline complex that you measured the absorbance of, what color light does the wavelength of maximum absorbance correspond to? Is this color consistent with the color you observe? Explain using concepts developed in the introduction to spectroscopy experiment. {Type answer here} 2. (4 points) a) Beer’s Law states the absorbance of a substance in solution is proportional to its concentration in the solution. Absorbance Concentration describes a straight line whose y-intercept is zero. {Paste absorbance vs. concentration graph here} b) How well does your data fit Beer’s Law? {Type answer here} c) What effect does this have on your confidence in your results reported below? Explain. {Type answer here} 3. (10 points) a) What is your unknown number? ___________ b) (4 points: accuracy) What is the percent iron (± error) in your sample? _____________________ c) (6 points) Show all calculations below. This includes the calculations for the concentration of the standard solutions made during week 1 of this experiment. It also includes all calculations needed to determine the %Fe2+ in the ore and the error during week 2. Use Equation editor. Show units. Be aware of significant figures. {Show calculations here} 4. (4 points) What specific steps in procedure or choice of equipment were taken to minimize the error in this experiment? There were many. List and briefly discuss as many as you can. {Type answer here} See the attached rubric for more detailed information about grading. Q#1 Explain color Q#2 Discuss graph Q#3b. Accuracy Q#3c. Calcs. Unsatisfactory Illogical answer or no answer 0 points No graph and no answer. 0 points Answer within about 30% of the correct answer. 1 point Equation editor not used. 0-1 points Q#4 Discussion of minimization of error Borderline Graph present but poor discussion of quality of data. 1-2 points Answer within about 20% of the correct answer. 2 points 2-3 points Only 1 or 2 examples with reasonable discussion. 2 points Satisfactory 3 points Answer within about 14% of the correct answer. 3 points 4-5 points Excellent Reasonable explanation of observed color 2 points Reasonable discussion of the quality of your data and implications for your results. 4 points Answer within about 7% of the correct answer. 4 points Calculations for standards 1 pt., %Fe2+ 2pts, error 1 pt., Units, 1 pt., sig figs 1pt. 6 points At least 3 good examples with reasonable discussion. Pts. 2 pts 4 pts 4 pts 6 pts 4 pts 4 points 20 pts