Ben- Gurion University of the Negev Materials Engineering Name of the module: Materials Characterization Number of module: 36513471 BGU Credits: 4 Aims of the module: The module will provide an introduction to modern materials ECTS credits: number of credits in the characterization techniques and their principles of operation. European Credit Transfer System Objectives of the module: The module will provide students with basic concepts in interaction Academic year: of radiation with matter, and will present a variety of techniques for the characterization of bulk Semester: spring semester material as well as surfaces. Classification to microscopy, scattering and spectroscopy techniques will Hours of instruction: provide the students with effective means for assigning the proper characterization tools for a given problem in materials characterization. Location of instruction: Learning outcomes of the module: On successful completion of the course, the Language of instruction: Hebrew student should be able to: Cycle: 1. Position: Advanced obligatory core class for and x-rays) with solid matter. Attributes such as interaction cross-section third year materials engineering students Field of Education: Materials Science and mean free path will be emphasized. 2. and Engineering sensitivity and detection limits. 3. be familiar with transmission electron microscopy and its principles of operation; be able to carry out basic analysis of an electron diffractogram. General prerequisites: Introduction to Materials 1,2,3; Physics 1,2,3. understand basic principles in materials characterization, such as quantitative and semi-quantitative analysis, bulk vs. surface analysis, Responsible department: Materials Engineering be familiar with basic concepts in interaction of radiation (e.g., electrons 4. be familiar with scanning electron microscopy and its principles of operation. Grading scale: metric 0-100 5. understand x-ray microanalysis (EDS) and the fundamental differences between EDS coupled with scanning vs. transmission electron microscopy. 6. be able to describe scanning tunneling and scanning force microscopies and their principles of operation. 7. understand surface analysis techniques such as x-ray photoelectron and Auger spectroscopies and their principle of operation; be able to explain the origin of surface sensitivity in these techniques. 8. be familiar with secondary ion mass spectrometry and its principles of operation. 9. be able to describe various surface diffraction techniques and the origin of surface sensitivity in each of them. 10. be familiar with the main materials characterization tools available at the university. Attendance regulation: No attendance requirements Teaching arrangement and method of instruction: Lectures and exercises in class, homework, tour of the characterization laboratories. 1 Ben- Gurion University of the Negev Materials Engineering Lecturer: Professor Yuval Golan Assessment: Contact details: Building 51 Office 308 how the students will be assessed in the module Office phone: 61474 1. Homework 5% Email: ygolan@bgu.ac.il 2. Report in preparation for lab tour 5% Office hours: 3. Midterm exam 10% 4. Final exam 80% (must pass exam in order to pass course) Module evaluation: at the end of the semester the students will evaluate the module, 100% in order to draw conclusions, and for the university's Work and assignments: internal needs. 1. Submission of 3-5 sets of homework. Submission deadline will be announced for each set. After the deadline a solution will be uploaded to the course website. Confirmation: the syllabus was confirmed by the faculty academic 2. Midterm exam will be held after circa 7 weeks of lectures. 3. Lab tour will be carried out during the last two weeks of the semester. Preparation report will be submitted up to 24 hours before the tour. advisory committee to be valid on 2012-2013. 4. Final exam will be held during exam period. Time required for individual work: in addition to attendance in class, the students Last update: September 2013 are expected to do their assignment and individual work: 1. Homework: 2-3 hours per week 2. Midterm exam: 10-12 hours 3. Preparation for lab tour: 6 hours 4. Final exam: 24-30 hours 2 Ben- Gurion University of the Negev Materials Engineering Module Content\ schedule and outlines: Lectures: Hours Introduction to materials characterization 3 Basic principles in materials characterization 6 Scanning electron microscopy 3 Transmission electron microscopy and electron diffraction 3 Micro and nanoanalysis using characteristic x-rays 3 Scanning probe microscopy techniques 3 X-ray photoelectron spectroscopy 3 Auger spectroscopy 3 Secondary ion mass spectroscopy 3 Surface sensitive scattering techniques 3 Lab tour 2 Summary: assignment of techniques to problems 4 Recommended reading: 1. Fundamentals of surface and thin film analysis (Feldman & Mayer). 2. Scanning electron microscopy and x-ray microanalysis (Goldstein et al.). 3. Materials science and technology, Vol. 2A-2B (Cahn, Haasen & Kramer). 4. Structural and chemical analysis of materials (Eberhart). 5. Microstructural Characterization of Materials (Brandon & Kaplan). 6. Low energy electrons and surface chemistry (Ertl & Kuppers). 7. Physical methods of materials characterization (Flevitt & Wild). 8. Transmission Electron Microscopy (Williams & Carter). 9. Practical surface analysis (Seah & Briggs). * All learning material will be available to the students on the module's website (high-learn)/ library/ electronic documents available to BGU students. 3