DOC:CB/CL/QR/5.8/IL-1
Issue No.: 04
Revision No. :01
Issue Date : 19.02.2014
Sample Reg. No. : ______________________
CENTRAL POLLUTION CONTROL BOARD
Parivesh Bhawan, East Arjun Nagar, Delhi-110032
INSTRUMENTATION LABORATORY
Requisition for Analysis of Trace Metals
:
1.
Division
2.
Project
:
3.
Sampling Location
:
4.
Sample Collected by
:
5.
Sample Matrix
: Water/Soil/Sludge
6.
7.
Date & Time of sampling
:
Samples Details
:
(i)
Sample nature
: Grab/ Composite: Preservation
(ii) Sample Pre-treated / Untreated
:__________________________
(iii)
Sample Digested by
:__________________________
(iv) Digested Sample Volume
(15 ml x no.of metals to be analyzed):_________________________
(v) Blank code no./nos
: _________________________
(vi) Sample Code no/nos
:__________________________
(vii) Total No. of Samples
:__________________________
(viii) Metals to be analysed
: Please tick or encircle
As
Cd
Cr
Cu
Fe
Pb
Mn
Hg
Ni
Zn
Sb
Co
Se
V
Any Other Information :
Indentor
Incharge
(Indenting Division)
Incharge
(Instrumentation Lab)
Incharge
(Sample receiving section)
Sample Reg. No. : ______________________
ACKNOWLEDGEMENT
Received__________Samples
from
No.___________to______on_____at_____a.m./p.m.
from_______________ Division/Zonal Office/SPCB for Physico-chemical/Biological ______ Testing
Remarks :
Date :
Signature
Sampling and preservation Requirement for Heavy Metal Samples:
Parameter
Heavy Metals (
As, Cd, Cr, Cu,
Fe, Mn, Ni, Pb,
Zn, Sb, Co, Se,
V)
Mercury
( Hg )
Container to be used
Narrow mouth
Polyethylene Bottle
Volume/Weight of samples
be provided
Water/ Waste Water-minimum
500 ml
Narrow mouth
Polyethylene Bottle
Soil/Sludge/Sediments/Solid
waste-Minimum 250 gm
Glass Bottle or
Polyethylene Bottle
Water/ Waste Water-minimum
1 litre
Wide mouth
Polyethylene Bottle
Soil/Sludge/Sediments/Solid
Waste - Minimum 250 gm
Preservation
Sample pH adjusted to <
2.0 with Conc. Nitric AcidAR Grade
-
Conc. Nitric Acid- (AR
Grade) + K2Cr2O7 (20% in
1:1 HNO3)
Ice preserved
Ice preserved
DOC:CB/CL/QR/5.8/IL-2
Issue No.: 04
Revision No. :01
Issue Date : 19.02.2014
Sample Reg. No. : ______________________
CENTRAL POLLUTION CONTROL BOARD
Parivesh Bhawan, East Arjun Nagar, Delhi-110032
INSTRUMENTATION LABORATORY
Requisition for Analysis of Trace Organic Carbons/ Adsorbable Organic Halide Samples
1.
Division
:
2.
Project
:
3.
Sampling Source
:
4.
Sample Matrix
:
5.
Sample Collected By
:
6.
Date & Time of sampling
:
7.
Samples Details
(i)
Sample preservation condition
:__________________________
(ii)
Sample Code no./nos
:__________________________
(iii)
Total No. of samples
:_________________________
(iv)
Parameter to be analysed
: Please tick or encircle
TC
Indentor
TOC
Incharge
(Indenting Division)
DOC
Incharge
(Instrumentation Lab)
TIC
AOX
Incharge
(Sample receiving section)
Sample Reg. No. : ______________________
ACKNOWLEDGEMENT
Received__________Samples
from
No.___________to______on_____at_____a.m./p.m.
from_______________ Division/Zonal Office/SPCB for Physico-chemical/Biological ______ Testing
Remarks :
Date :
Signature
Sampling Protocol to be followed :
(i)
Amber coloured glass bottles (preferably new) should be used for sample
collection for TOC/AOX analysis. To prepare sample bottles (500 ml capacity) give
acid wash, detergent wash, rinse with tap water then deionised water twice and
dry at 1500C in a drying chamber.
(ii)
For TOC analysis, sample must be collected in a 500 ml glass bottle by rinsing
with sample twice. The sample bottles of 500 ml capacity should be filled up to top
free of air bubbles and transported to laboratory in ice preserved condition or in
refrigerated condition.
(iii)
For AOX analysis, pH of the sample should be adjusted immediately after sampling
within 1.5 to 2.0 pH with Nitric Acid AR Grade. Fill the bottles of 500ml capacity up
to top, free of air bubbles. Remove active chlorine if present by adding Na2SO3
solution (less than 1ml/l) or crystals (Minimum 5mg/l) and preserve samples by
refrigeration at 40C and transfer to laboratory.