The Glass Bead Lab: Report Tutorial Palko (1-29-04) Each report should begin with a heading that includes the title of the experiment, the name of the person who is submitting the report and the date it was turned in. To complete this, fill in the blanks above. Purpose: This section is usually just a few sentences. The idea is to succinctly state the reasons for doing the lab. This can include learning goals (practice measurement techniques) and specific experimental goals (determine the density of glass beads). DO NOT repeat the purpose written in the lab handout, you should distill this section down and write it in your own words. This has already been done for you as an example for future reports and a future tutorial will explain in detail how these are to be written. Procedure: Formation of Groups For this part of the report, list members of your group and describe the exact roles they played during the experiment. In other words, in all lab reports, you should describe briefly what each person did to help the group to carry out the procedure. This should already be recorded in your lab notebook on the day of the experiment so you only need to rewrite it in the final report. Part I: Determining the Density of a Single Glass Bead In this part or the report you should briefly summarize the experimental procedure your group agreed on to measure the volume of a single glass bead. The rest of the procedure was explicitly described in the lab handout and does not need to be repeated. This is true of all future lab reports. You should only include an explanation of the procedures that the group decided to use that was not specifically described in the lab manual. A summary of the procedure should have been recorded in your notebook during the lab and only needs to be rewritten in your final report. Data and Results For Part II: Determination of the Density of a Glass Bead Mass Diameter Radius Volume Density Deviation from (g) (cm) (cm) (cm3 or (g/mL) Avg. mL)* Bead #1 Bead #2 Bead #3 Average 1 cm3 = 1 mL 1. Example calculation of radius and volume for one of the beads in the Table for Part II. 2. Example calculation of density (mass/volume) for one of the beads in the Table for Part II. 3. Example calculation of the deviation between the density for one sample and the average in the Table for part II. Data and results should always be tabulated with the quantities being measured or calculated as column headings and the identity of each sample as row headings. There should also be a title for the table that describes what data is shown by the table. In the heading of each column and row the units of measurement are included so that you do NOT need to record the units after each number. All numbers should be recorded in the table with the correct number of significant figures based on the stated precision of each measuring device. Even if the measured value is zero, it should be recorded with the same precision as all the other nonzero measurements made with the same device. In some cases as in the table above, both data and results are combined into a single table. In some experiments it will be more convenient to separate them. Also notice that an average value is placed on a separate line below the table since it is not related to one particular sample. Other footnotes explaining the data and results can be included, such as example calculations. You should provide a set of sample calculations for each column of results included in the table and you should use the correct number of significant figures for each calculated value. Data and Results For Part II: Determination of the Density of a Set of Glass Beads Mass (g) Initial Final Net Density Deviation Volume Volume Volume (g/mL) from Avg. (mL) (mL) (mL) Sample #1 Sample #2 Sample #3 Average 1. Example calculation of volume for one sample in the Table for Part II: 2. Example calculation of density (mass/volume) for one sample in the Table for Part II: 3. Example calculation of the average deviation between the density for one sample and the average density in the Table for part II: Conclusions First you should always have a simple conclusion statement that summarizes or restates the final results and explains how the results obtained fulfills the purpose of the experiment. Notice that a purpose of this experiment was to determine the density of glass beads. Were you successful in determining the density of the glass beads? Explain your answer. As a second part of the conclusion section you will need to use the precision of the data to determine how much variability there is within each set of data and results. One final note: how do you know if your results are accurate? In order to determine accuracy, you need a reference value for the density of glass. This can be obtained from a reference book such as the CRC Handbook of Chemistry and Physics; Lange’s Handbook of Chemistry, the Merck Index, your textbook or may be provided by your instructor. If you are provided with a reference value for the density of the glass beads this experiment, restate the two average densities you obtained and compare the reference value to your averages from Part I and II. To make this comparison determine, in each case, if your average value is higher or lower and by how much it differs from the reference value. You could also calculate the percent difference, which is defined as: % Difference = [(calculated or measured value - reference value)/reference value]*100 The sign of the percent difference indicates whether the calculated or measured value is larger (positive) or smaller (negative) than the reference value. If you are not provided with a reference value all you should do is restate the final calculated results. Compare the data you collected with another group that used a different size bead. What effect did using larger beads have? The Determination of the Density of Glass Beads Background: Physical properties such as density can be used to characterize a specific type of matter, in this case, glass beads. The determination of density involves making measurements that will provide mass and volume data regarding the beads. It is possible to collect this data in a number of ways. You will use two methods of collecting the necessary data and then compare those methods in terms of precision and accuracy. Precision describes the degree of certainty in your results. It can be looked at two ways. For an individual measurement, precision is represented by the degree of guessing used to make that measurement. For example, if you were to measure the width of this page, you might obtain a result of 21.50 cm. The last digit of this measurement is a guess because the ruler used was marked every 0.1 cm. We guess the last digit as it represents a value that is not marked on the ruler, but can be estimated. We could represent the “degree of guessing in this measurement as +0.01 cm. We can calculate the relative “degree of guessing” by comparing the guess amount to the actual measurement. Relative guess = degree of guessing/measurement value x 100 In this case, +0.01/21.50 x 100 = 0.05 % If the actual measured value were smaller, then the relative guess would become larger. In other words, our guessing becomes a more significant factor as the size of the object being measured becomes smaller. Accuracy is a comparison of the experimental result to some “accepted” or “real” value. The conclusion section of the report tutorial details a calculation that allows for a numerical comparison. In general, if there is a value available for comparison, it is prudent to compare experimental results to this and discuss any possible reasons for differences. Purpose: 1. Measure mass and volume of a single glass bead and calculate its density. 2. Measure the mass and volume of a set of glass beads and calculate density of the beads. 3. Devise a method to determine volume of a glass bead. 4. Evaluate your results. Procedure: Work in a group of three or four. Part One: Meet as a team and determine a method to determine the volume of a single glass bead. Each team member should then obtain a bead and use that method to determine the beads volume. Additionally, each team member needs to obtain the mass of his or her bead. Share all individual data and record it in the table on the report sheet for part I. Part Two: In this part, you will work as a team to determine the volume and mass of a set of beads. Obtain a beaker of beads. Divide this sample into three parts of varying size. Obtain the mass of each part. Use water displacement to determine the volume of each part. To do this, obtain a graduated cylinder and half fill it with water. After recording this volume, add the beads and record the new volume. Calculate the bead’s volume by taking the difference of the two volume measurements. Calculations: Complete all calculations as directed on the report sheet. Important relationships: Diameter = 2 x (radius) Volume of a sphere = 4/3 x () x (radius)3 Density = mass / volume Deviation from average = Average value of all trials – value from single trial Note: = 3.1415 or can be obtained from a button on your calculator.