An Experimental and Theoretical Study of the Cooling of a Thin Glass Fiber during the Formation Process By Daxi Xiong Submitted to the Department of Mechanical Engineering in Partial Fulfillment of the Requirements for the Degree of Doctor of Philosophy in Mechanical Engineering BARKER at the MASSACHUSETTS INSTITUTE OF TECHNOLOGY MASSACHUSETTS INUTITUTE OF TECHNOLOGY MAR 2 5 2002 February, 2002 LIBRARIES @Massachusetts Institute of Technology 2002. All rights reserved. Signature of Authors Departmeit of Meq ical Engineering January 3, 2002 Certified by Professor John H. Lienhard V Thesis Supervisor Accepted by Professor Ain A. Sonin Chairman, Department Committee on Graduate Studies An Experimental and Theoretical Study of the Cooling of a Thin Glass Fiber during the Formation Process By Daxi Xiong Submitted to the Department of Mechanical Engineering on January 3, 2002 in Partial Fulfillment of the Requirements for the Degree of Doctor of Philosophy in Mechanical Engineering Abstract The cooling of a thin, moving glass fiber was studied through both experiments and theoretical method in the present thesis. An experimental system was built at a laboratory scale, which included a glass fiber production subsystem, a temperature measurement subsystem, and a thermocouple temperature control subsystem. A heated thermocouple technique was adopted to measure the temperature distribution of the glass fiber along its drawing direction. Data were collected for diameters ranging from 20 to 50 micrometers and speeds from 1 meter per second to 6 meters per second. Experiments were performed both with and without water spray cooling of the fiber. A comprehensive analysis was performed to estimate the uncertainty in our experiments. The analysis shows that, without water spray, the 2a- uncertainty is 14.8%, and with water spray, it is 15.3%. The major uncertainty comes from the uncertainty of the thermocouple probe. For theoretical modeling, the von Karman-Pohlhausen boundary layer integral technique was used to predicting the cooling rate of the fiber. The model considers the effects of water spray, variation of drawing speed, fiber diameter, environment parameters, and initial conditions, extending earlier work on the subject. The comparison between the experimental data and the theoretical prediction shows integral methods produce the correct trends, but show systematic disagreements with the data. The models with and without spray show similar levels of disagreement. The direction and magnitude of these disagreements are system dependent. Potential causes may include fiber vibration effects, boundary layer transition, and measurement uncertainties. Thus, future work should focus on measuring/modeling the vibration effect and determining the amplitudes/frequencies of the vibration (which are expected to be system dependent). Incorporation of spray dispersion effects is also required for improved modeling. Thesis Supervisor: John H. Lienhard V Title: Professor of Mechanical Engineering Thesis Committee: Professor J. H. Lienhard (Chairman) Professor B. B. Mikic Professor L. R. Glicksman 3 4 To Lijun, Kevin and my parents S5 6 Acknowledgments The authors wish to express his high appreciation to Professor John H. Lienhard V, for both his patient guidance and deep insight in helping completing the present work and providing me a chance to study under his supervision at MIT. I am also indebted him a lot to his invaluable support in my difficult time during April and May in 2001. A very special thank goes to my family. My lovely wife, Lijun, has been a great supporter. During my studies at MIT, Lijun and I have a new baby boy, Kevin. He is so wonderful and so excellent and gives us great pleasure of being his parents. We love you, Kevin. Love and care from my parents, mother-in-law, sister-in-law, brother-in-law, and my two lovely nieces are strong support to finish my research here. Again thank them all. This project has been partially funded by the PPG industry Inc. The author would thank Mr. A. A. "Gus" Astroth, Dr. Charles Smith, Dr. Talsania, Sameer, and Dr. Gaertner, Dean, for their support, suggestion and participation in this project. 7 8 Contents Abstract ........................................................................................................ 3 Acknowledgements ...................................................................................... 7 Contents ........................................................................................................ 9 List of Figures ............................................................................................... 13 List of Tables ................................................................................................. 17 Nomenclatures ............................................................................................... 19 Chapter 1 Introduction ............................................................................... 23 Chapter 2 Review of Previous W ork ........................................................... 29 2.1 Review of previous theoretical studies ............................................... 29 2.2 Review of previous experimental studies ............................................ 34 2.3 Summary ............................................................................................ 36 Chapter 3 Objective of Present Study ........................................................ 37 3.1 Objectives of the present thesis................................................ 37 3.2 Proposed solution methods .................................................. 39 3.2.1 Proposed theoretical modeling method ....................................... 39 3.2.2 Proposed experimental method ................................................. 39 3.2.3 Mechanism of Heated Thermocouple Technique ....................... 40 3.3 Summary ............................................................................................ Chapter 4 Experimental System Design and Model Test .......................... 4.1 The experimental system ................................... 9 42 43 43 4.2 Temperature measurement subsystem design ................................. 48 4.2.1 The heating subsystem ............................................................... 48 4.2.2 The measurement subsystem ..................................................... 49 4.2.3 The mechanical fiber transport subsystem ................................. 50 4.3 Measurement methods ....................................................................... 51 4.3.1 Steady state measurement method ........................................... 52 4.3.2 Transient state measurement method ....................................... 52 4.4 One dimensional fin model test ........................................................ 54 4.5 System operation and data acquisition .............................................. 58 4.5.1 Startup the system and produce the fiber ................................... 58 4.5.2 Measure the temperature and record .......................................... 58 4.5.3 Refill marbles or shut down ........................................................ 59 4.6 Summary ............................................................................................ 60 Chapter 5 Data without Water Spray ........................................................... 61 5.1 The measured method under no water spray ..................................... 61 5.2 The experimental data without spray .................................................... 63 5.3 Summary ............................................................................................ 72 Chapter 6 Data with Water Spray ............................................................... 73 6.1 Understand the measurement under water spray .............................. 73 6.2 Redesign the probe and model test with water spray .......................... 77 6.3 Experimental data under water spray ................................................. 79 6.4 Summary ............................................................................................ 86 Chapter 7 Error Analysis .............................................................................. 87 7.1 Understanding the error sources ........................................................ 87 7.2 Error estimation without water spray ................................................... 91 7.2.1 Temperature fluctuation ............................................................. 91 7.2.2 Heat conduction between the fiber and the sensor ..................... 92 7.2.3 The frictional heating in measurement ...................................... 94 10 7.2.4 Boundary layer cooling ................................................................. 100 7.2.5 Overall uncertainty ....................................................................... 102 7.3 Error estimation with water spray ......................................................... 104 7.3.1 Temperature fluctuation ............................................................... 104 7.3.2 Heat conduction between the fiber and the sensor ................... 105 7.3.3 The frictional heating in measurement ......................................... 106 7.3.4 Overall uncertainty ..................................................................... II 7.4 Summary .............................................................................................. 113 Chapter 8 Theoretical Model and Data Comparison ................................... 115 8.1 Control equations and von Karman-Pohlhausen integration technique ............................................................................ 115 8.1.1 Governing equations of a single moving fiber ............................. 115 8.1.2 Von Karman-Pohlhausen integration method .............................. 117 8.2 Items analysis on solving the fiber boundary layer flow ....................... 121 8.2.1 Estimate the thickness of the thermal boundary layer below the bushing ........................................................................ 8.2.2 Determine the initial temperature To at the tip ......................... 8.2.2.1 Using curve fit to extrapolate To ........................ ... ... .. .... .. ... . 121 125 125 8.2.2.2 Considering the effect of the thermal boundary layer .......... 126 8.2.3 Evaluation of evaporation item and radiation ............................... 127 8.2.3.1 Single water droplet evaporation ......................................... 127 8.2.3.2 Heat sink in the fiber boundary .......................................... 128 8.2.3.3 Evaluate the importance of radiation ................................... 129 8.3 Comparison between our experimental data and the theoretical prediction ............................................................... 130 8.3.1 Comparison for dry data ............................................................... 130 8.3.2 Comparison for wet data ............................................................. 137 8.4 Summary .............................................................................................. Chapter 9 Conclusions .................................................................................. 11 143 145 References ...................................................................................................... 147 Chapter 1 .................................................................................................... 147 Chapter 2 .................................................................................................... 147 Chapter 3 .................................................................................................... 150 Chapter 4 ................................................................................................... 152 Chapter 5 ................................................................................................... 152 Chapter 6 .................................................................................................... 153 Chapter 7 .................................................................................................... 153 Chapter 8 ................................................................................................... 1-53 12 List of Figures Figure 1.1 Some glass fiber products from PPG Inc. ......................................... 25 Figure 1.2 Reinforcement glass fiber manufacturing process ............................ 25 Figure 1.3 Glass fiber production station ........................................................... 26 Figure 2.1 Experimental picture of boundary layer on a continuous cylindrical surface ............................................................................ 30 Figure 2.2 Comparison of the experimental data and prediction curves ........... 35 Figure 3.1 An example of heated thermocouple in measurement ................. 41 Figure 4.1 The experimental system .................................................................. 44 Figure 4.2 The winder ........................................................................................ 45 Figure 4.3 The temperature control system ....................................................... 46 Figure 4.4 LabView program user interface ....................................................... 47 Figure 4.5 Sketch of temperature measurement system for glass fiber ............ 48 Figure 4.6 Cross-section of heating subsystem ................................................. 49 Figure 4.7 The three-dimensional traverse subsystem ...................................... 50 Figure 4.8 Steady temperature profile when a probe is contacted or Uncontacted under different currents ............................................... 51 Figure 4.9 The transient temperature profile under current cut-off .................... 53 Figure 4.10 simplified sketch of thermal contact ................................................ 54 Figure 4.11 Step response of TB to Tc ............................................................... 58 Figure 4.12 Model test sketch ............................................................................ 54 Figure 4.13 The temperature distribution along a copper fin ............................. 57 13 Figure 5.1 Fiber drawing from the tips ........................................................... 62 Figure 5.2 Temperature profile when speed is 1.76 m/s ................................ 64 Figure 5.3 Temperature profile when speed is 2.64 m/s ................................ 65 Figure 5.4 Temperature profile when speed is 3.51 m/s ................................ 66 Figure 5.5 Temperature profile when speed is 4.39 m/s ................................ 67 Figure 5.6 Temperature profile when speed is 5.27 m/s ................................ 68 Figure 5.7 Temperature profile when speed is 6.15 m/s ................................ 69 Figure 5.8 The experimental data in non-dimensional formation .................... 71 Figure 6.1 The sketch of water spray ............................................................. 74 Figure 6.2 Heat convection coefficient change along the distance ................ 75 Figure 6.3 The sketch of the revised probe ................................................... 76 Figure 6.4 Measurement under water spray ............................................ 78 Figure 6.5 Temperature profile when speed is 1.00 m/s ................................ 80 Figure 6.6 Temperature profile when speed is 1.76 m/s ................................ 81 Figure 6.7 Temperature profile when speed is 2.64m/s ................................ 82 Figure 6.8 Temperature profile when speed is 3.51 m/s ................................ 83 Figure 6.9 Temperature profile when speed is 4.39 m/s ................................ 84 Figure 6.10 Temperature profile when speed is 5.27 m/s ............................... 85 Figure 7.1 Instrument used to measure the normal force .............................. 89 Figure 7.2 Temperature fluctuation without water spray ................................ 91 Figure 7.3 Sketch of the contact .................................................................... 92 Figure 7.4 The normal force measurement system ...................................... 94 Figure 7.5 The sketch of the measurement ................................................. 95 Figure 7.6 Normal force without water spray for repeated measurements ...... 96 Figure 7.7 Sketch of friction heat flowing into the probe ............................... 97 Figure 7.8 Temperature fluctuation with water spray ....................................... 105 Figure 7.9 The normal force measurement system under water spray ........... 106 Figure 7.10 Normal force with water spray ...................................................... 14 107 Figure 8.1 A single moving fiber ...................................................................... 116 Figure 8.2 Momentum boundary control volume ............................................. 117 Figure 8.3 Thermal boundary layer control volume ......................................... 118 Figure 8.4 Control volume of fiber ................................................................... 119 Figure 8.5 The sketch of the thermal boundary layer below the tips ............... 122 Figure 8.6 Bushing surface size ...................................................................... 123 Figure 8.7 The effect of the thermal boundary layer to the fiber boundary layer .............................................................. 124 Figure 8.8 The effect of the thermal boundary layer to the fiber cooling .......... 124 Figure 8.9 Curve fit for To .......................................... . .. .... .. ... .... ... .. ... ... .. ... .. .... Figure 8.10 Find the true To ........................................... .. .. ... .... ... .. ... ... .. ... .... .. Figure 8.11 Comparison of radiation and the convection ................................ 125 126 129 Figure 8.12 Comparison of the experimental data and the theoretical prediction when drawing speed is 1.76 m/s ................................................... 130 Figure 8.13 Comparison of the experimental data and the theoretical prediction when drawing speed is 2.64 m/s .................................................. 131 Figure 8.14 Comparison of the experimental data and the theoretical prediction when drawing speed is 3.51 m/s .................................................. 132 Figure 8.15 Comparison of the experimental data and the theoretical prediction when drawing speed is 4.39 m/s .................................................. 133 Figure 8.16 Comparison of the experimental data and the theoretical prediction when drawing speed is 5.27 m/s .................................................. 134 Figure 8.17 Comparison of the experimental data and the theoretical prediction when drawing speed is 6.15 m/s .................................................. 135 Figure 8.18 Comparison of the experimental data and the theoretical prediction under no nondimensional coordinate system ............................... 136 Figure 8.19 Comparison of the wet data and the theoretical prediction when drawing speed is 1.00 m/s ........................................................... 137 Figure 8.20 Comparison of the wet experimental data and the theoretical prediction when drawing speed is 1.76 m/s ................................. Figure 8.21 Comparison of the wet experimental data and the theoretical 15 138 prediction when drawing speed is 2.64 m/s ................................. 139 Figure 8.22 Comparison of the wet experimental data and the theoretical prediction when drawing speed is 3.51 m/s ................................. 140 Figure 8.23 Comparison of the wet experimental data and the theoretical prediction when drawing speed is 4.39 m/s ................................. 141 Figure 8.24 Comparison of the wet experimental data and the theoretical prediction when drawing speed is 5.27 m/s ................................. 16 142 List of Tables Table 7.1 Properties of glass fiber and K type thermocouple ........................ 99 Table 7.2 Properties of air at 551K .................................................................. 100 Table 7.3 Properties of air and droplets at 551K ............................................. 108 17 18 Nomenclatures Symbol Description Unit a, r radius m A,S area M2 Cp heat capacity J/kg. K D diffusion coefficient m2 /s D diameter m F force N h heat convection coefficient W/m 2 K L length m L distance m La adiabatic length m m mass flux Kg/m 2 s M mass kg n number density /cm 3 q heat flux density W/m2 Q heat flux W ST standard deviation of temperature K t time s T temperature K V velocity, speed m/s U velocity m/s U speed m/s U overall heat transfer coefficient W/K 19 Symbol Description Unit W width m x distance m X, Y, U, C, D matrix Gr Grashof number hfg latent heat Nu Nusselt Number, Nu= hd/k Pr Prandtl number v/a Ra Ralay number Re Raynold number Re=Vd/v SMD Saunter Mean Diameter KJ/Kg m 1hpm-1 Kg/ m3 p density A difference 6 thickness of boundary layer, diffusive length m a thermal diffusivity m2 /s oY standard deviation of force N e Angle rad a Planck constant 5.67x10 8 W/m2 K4 E Emissivity v kinetical viscosity m2 /s Subscripts air air ave average bl boundary layer 20 Symbol Description conduction heat conduction cooling cooling D based on diameter diff diffusion e electricity err error f fiber fc forced convection friction friction ft between fiber and thermocouple I liquid na natural convection 0 start point S saturation state t thermocouple T thermal total total w water wire thermocouple wire x at location x 00 infinite Superscripts T * trans of matrix total value partial 21 22 Chapter 1 Introduction Glass fibers, usually used as reinforced plastic composites, have many excellent properties [1.1, 1.2] including: 1) low thermal conductivity and non-inflammability; 2) High tensile strength and low density; 3) good chemical and electrical resistance, not subject to water corrosion; 4) good dielectric properties such as high impedance, high breakdown strength, low specific inductive capacity and loss factor; 5) excellent bonding abilities with various reinforced materials, especially polymers. Glass fiber is used by a great variety of industries in almost every major market. Plastics reinforced with glass fiber have hundreds of applications in the transportation, marine, construction, electrical, business machine and appliance markets, and in corrosion-resistant equipment and consumer products [1.2]. Figure 1.1 shows some products of glass fiber from PPG Industries Inc. The manufacture of glass fiber is a complex process as illustrated in figure 1.2. The key step is that molten glass is extruded through orifices in a platinum bushing plate to form glass fibers. The bushing plate is heated electrically to maintain a constant glass temperature. On small production facilities, gas pressure is used to maintain a steady glass pressure at the orifice entrance. High volume production stations maintain a fixed molten glass depth above the bushings to obtain a constant hydrostatic head. The glass that exits the orifices is pulled and wound onto a take-up reel. This causes the molten fiber to neck down until the glass sets at the final fiber diameter. The initial glass temperature at the bushing plate is about 1500 K 23 (a) Reinforcing mats (b) Continuous roving (c) Chopped strand 24 (d) Woven roving Figure 1.1 Some glass fiber products from PPG Industries Inc. [1.2] PONFORCEMENTFMEOLANS :IANUFAMTRINOPROCM$ -om I "MOM~ L '4! am I,, -As #4) F~ -#A A MWm4sS0 -mnS. I assa-S. ov a STASM anag.er I -n QM OAN ELU:Le Figure 1.2 Reinforcement glass fiber manufacturing process [1.2] 25 and the glass solidification temperature is 1390 K. Before the fibers are wound onto the take-up reel, they pass through a surfactant applicator. The fibers must be cooled to a temperature less than 367 K before the surfactant is applied. For sufficient cooling, the distance between the bushing plate and the surfactant applicator is on the order of 1 m. Typical fiber diameters vary between 5 pm and 30 pm with drawing speeds between 15 m/sec and 90 m/sec. Usually the smaller fibers are drawn at higher velocities than the larger fibers, but the same size fiber may be pulled at different speeds on different production stations. Figure 3 illustrates a typical production station. Bushing plates contain an array of one hundred to several thousand orifices with the spacing between orifices varying from 0.6 cm to 1.0 cm. Multiple fibers are gathered into a bundle after the surfactant is applied and are then pulled onto the take-up reel. This process has been in use for over fifty years [1.3, 1.4, and 1.5]. MSlten Gass II ! 1 1 1". , , 1 - _ .1 ___ ___ - . , . ........... . Bushnr ftte ........ .. Nozze Heade Fiber Velodty - U Nozzte Su rfctant pt~cator To Take Up Reet Take Up Reet Figure 1.3 Glass fiber production station [1.6] 26 The high strength of glass fibers is attributed to the rapid cooling process of the fiber while it is being formed [1.7]. Therefore, it is important to predict and control the temperature profile of a drawn glass fiber. Although a substantial amount of research has been performed on the various parts of the fiber forming process (a detailed review will be provided in chapter two), there are still a lot of questions open to answer. The present thesis will be focused on both experimental and theoretical study on the fiber formation process, especially on the water spray cooling process, which has been seldom studied before, to understand the cooling mechanism of the fiber formation, and thus to optimize the production process. This thesis consists of four parts. The first part (chapter one to chapter three) is an introduction of the fiber manufacture, a review of previous work on fiber formation, and a description of the objectives of the present study. The second part (chapter four to chapter seven) is the experimental study of fiber cooling. Chapter four describes the experimental system design. Chapter five and six provide experimental data without water spray and with water spray, respectively. A thorough error analysis is performed in chapter seven. The third part (chapter eight) provides theoretical analysis and comparison between our data and the theoretical modeling results. The last part (Chapter nine) describes the conclusions of the whole thesis. 27 28 Chapter 2 Review of Previous Work Much research has previously been done in the area of characterizing heat transfer in forming filaments. While some of the research was experimental, a great deal of this material is theoretical in nature. An overview is presented in the following two sections of this chapter, one for theoretical studies and the other for experimental research. 2.1 Review of previous theoretical studies Two modes of heat transfer, convection and radiation, need to be considered in the fiber cooling process. From Progelhof and Throne [2.1] and Rea [2.2], if the diameter of the glass fiber is small (less than 100 micrometers), radiation is very small compared with convection and can be ignored. Many approaches to estimate the value of the convective heat transfer coefficient have been used in previous theoretical studies. Glauert and Lighthill [2.3] assumed that the momentum boundary layer was developed from the leading edge of a stationary, infinitely long cylinder in a moving fluid. They derived their results based on a series solution for the boundary layer using the Von Karman-Pohlhausen boundary layer integration technique. They displayed the variation of the skin friction, boundary-layer displacement area and momentum defect area along the cylinder with curves. Although they didn't derive any results for heat transfer, their application of the 29 Von Karman-Pohlhausen technique and their use of the nondimensional coordinate, vx/va2 , were widely adopted in the later studies. Sakiadis [2.4, 2.5, and 2.6] also used this boundary layer integration technique. However, he used a different velocity profile in order to match the momentum boundary conditions in his problem. Unlike Glauert and Lighthill, Sakiadis assumed that the boundary layer was developed from the point where an infinite cylinder was issued from a wall at constant velocity through a surrounding medium at rest. Figure 2.1 is the experimental picture he took in his experiments. The outside two thick white lines are the outlines of the boundary layer of the moving cylinder. Sakiadis considered both laminar and turbulent boundary layers developing from a moving, continuous cylinder. However, he concluded that his model for the velocity profile in turbulent flow couldn't accurately predict the real turbulent boundary layer flow. Figure 2.1 Experimental picture of boundary layer on a continuous cylindrical surface [2.4] 30 Glicksman [2.7] employed a Reynolds analogy based on the work of Glauert and Lighthill to estimate the value of the local convective heat transfer coefficient as 4.3 Nu _ I Va 12.9 F ( 4 (2.1) L V2 The Reynolds analogy assumes that the air Prandtl number is unity and thus requires that the thickness of the momentum and thermal boundary layer surrounding the glass fiber be equal. Glicksman derived the cooling time for the fibers and compared it with other theories and experimental data. Bourne and Elliston [2.8] and later Bourne and Dixon [2.9] used the same Von Karman-Pohlhausen technique to study the development of the momentum and thermal boundary layers of a constant diameter fiber. Their formulation introduced a correction factor if the Prandtl number is less than unity. They estimated that the calculated results they obtained for the Nusselt number tended to underpredict the experimental data available to them by about 2% to 8% depending on different locations. Departing from previous studies [2.3, 2.4, 2.5, 2.6, 2.7, 2.8, 2.9], where the filament was always considered as a constant diameter cylinder and the effect of curvature wasn't taken into account, Sayles [2.10, 2.11], who cited the work of Moore and Pearson [2.12], introduced a formulation that took into account the curvature(measured with 1/a) and showed that the effects of the curvature may increase the value of the Nusselt number by as much as 28%. Sayles estimated the convective heat transfer coefficient resorting to the Reynolds analogy. Beese and Gersten [2.13] also took into account the curvature effect in their study. They used an asymptotic expansion with respect to the perturbation parameter e =1/ Rea . By using the method of matched asymptotic expansions, they developed a local Nusselt expression including both curvature effect and entrainment effects: 31 Nux 0.349 + 0.366 + Re Re a x 23 (x,0,0.7) x Re Ra (2.2) f Kase and Matsuo [2.14] provided the generally accepted correlation for a stationary thin cylinder parallel to the airflow: .3) Nu a = 0.42(Re a 02344 Kase and Matsuo developed their correlation based on the data they obtained by subjecting a 0.2 mm diameter heated wire to airflow parallel to the wire for values of Rea in the range of 0.5-50. Later, Kase and Matsuo [2.15] extended their results to represent the presence of a cross flow more accurately. Morris et al. [2.16, 2.17] also developed a correlation for the local heat convection coefficient based on the filament diameter, the temperature difference between the filament and the airflow, the airflow speed and the angle between the airflow and the filament. h (-0.0118 x 106 d + 0.9057) x (T - T) = + (23.01 x V - 6.612 x 106 x d + 573.5) + V (2.4) x (0.8452 x 1012 d2 - 111.3 x 106 d + 4631) x sin 2 () Morris et al. obtained their correlation by measuring the heat loss from a heated platinum filament at rest, where the forced convective air flowed over the filament. The data were collected for 5 different filament diameters, 25.4, 38.5, 51, 63.5 and 76 micrometers for 5 different dynamic pressure settings, 0.0, 0.466, 0.931, 1.397 and 1.863 mm Hg over a temperature ranger from 400K to 1100K in increments of 1OOK. The angle of the test filament with the freestream 32 was altered producing a crossflow effect and the same data were recorded for 2.50, 50 and 70 cross angles. They estimated the error of the correlation as 11.5% [2.17]. Both equation (2.3) and (2.4) are developed from the airflow that flows along a thin cylinder at rest. However, people also use them when a thin cylinder moves into still air. Richelle, Tasse and Riethmuller [2.18] investigated the difference of the boundary layers between a semi-infinite stationary body and a continuous moving body. They found the growth of the boundary layer was strongly affected by the flow configuration. The friction coefficient and the Nusselt number of the latter can be 20% greater than that of the former. So strictly speaking, the models and correlations developed from examining a stationary cylinder in a moving fluid cannot be quantitatively used in the study of the cooling of the moving fiber. Maebius [2.191 adopted several heat transfer models to study the effects of convective and radiative heat transfer on melt spun fibers. He concluded that the radiation cooling was a dominant form of heat transfer and the spectral emissivity has a large effect on the shape of the fiber. Papamichael and Miaoulis [2.20, 2.21, 2.22] studied the thermal behavior of the optical fibers with different diameters during the cooling stage. They adopted numerical simulation and the Von Karman-Pohlhausen technique. They found that, when the fiber diameter becomes larger, heat conduction in the fiber and radiation from it, which can be ignored when the fiber diameter is small, become important. Kang, Yoo and Jaluria [2.23], Choudhury and Jaluria [2.24], and Lee and Jaluria [2.25] performed an extended study on the heat transfer from a continuously moving heated cylinder. They applied both numerical calculations and experimental methods. However, they focused on thicker diameter cylinders (diameters larger than 1 millimeter). Other authors investigated the air drag on the single filaments and obtained empirical correlations for the skin friction coefficient, then used the Reynolds or the Chilton-Colburn analogy to derive the local convective coefficient. 33 2.2 Review of previous experimental studies Compared with the large volume of theoretical studies of fiber cooling, little experimental investigation in this field has been published. The reasons may be that: (i) it is hard to measure the temperature of a thin moving fiber cylinder; (ii) some of the industrial experimental work is confidential and unpublished. Here we list some published work. Alderson, Caress and Sager [2.26] performed experiments on glass fibers and found that, within a quite substantial distance from the orifice, log[Ts(x)-T] decreases almost linearly with the location in the moving direction of motion. Arridge and Prior [2.27] measured the rates for fibers with 10-50 micrometers diameter, pulled down from a rod. They found that the cooling time is about 30 times slower than the theoretical prediction in reference [2.281. Maddison and McMillan [2.29] measured the cooling time of thicker glass fibers (100-200 micrometers) and found the cooling time was proportional to (velocity)-0-7 and (radius)- 5 and typically on the order of seconds. The collected data from these three papers are shown in nondimensional position and temperature coordinates in figure 2.2. The departure of the data from the laminar theory at xv/vd 2 ~ 1600 is suggestive of a turbulent transition or some other change in the cooling mechanism. 34 1.0 --- %IN~ H -(N U)d=4.3/in(16vx/vd 2)- 12.9/[In(1OIvx/vd2)] 6 ------ h = (-1.18e'd+0.9057)(T-T.)+(23. 01 v-6.612e d+573.5) .......-----Bourne and Dixon's theory predi :tion 0.6 H H t- -.. + 0.8 1.1 (Nu),=0.42R ,' ' (N U)d = 0.349*Re d/Re.+0.366 0 Cu 0.4 0.2 * * A 0.0 . 0 Arridge's Data Alderson's Data Maddison's Data . * , 500 1500 1000 xv/Ud I 2000 - 1 2 500 2 Figure 2.2 Comparison of the experimental data and prediction curves Effect of Spray Sweetland and Lienhard [2.30] examined the effect of the water sprays commonly used to cool freshly drawn glass fibers. A model has been developed by using the Karman-Pohlhausen treatment of the velocity and thermal boundary layers and accounting for the evaporation of an entrained water spray. Eletribi [2.31] investigated the entrainment of the water sprays into the air flow induced in the manufacturing process of glass fibers. The spray atomization qualities and the spray dispersion patterns of the nozzles used on the glass production lines were examined by measuring the droplet diameter, velocity, and number flux with a Phase Doppler Particle Analyzer. 35 2.3 Summary The prediction curves of the models without water spray from the references [2.7, 2.9, 2.13, 2.14, and 2.17] are compared with the limited available experimental data (shown in figure 2.1). Although the cooling time that some models predict has the same order as the experiment results, there still exist differences among them. Moreover, there is significant discrepancy among different groups of data. This shows that the experiments were affected by many factors, and that more data are needed to develop and verify the theoretical model. 36 Chapter 3 Objective of Present Study 3.1 Objectives of the present thesis Generally speaking, the theoretical works previously done focused on a stable fiber drawing process with a laminar boundary layer. Few of them considered the effect of water evaporation on the heat transfer, which is common in industrial fiber drawing. At the same time, due to the evaporation, the boundary layer along the fiber drawing may be different. In experiments, too few data are available for analysis. No reference reports the temperature profile obtained under water spray. Therefore, although a lot of study has been done on fiber cooling, some problems still remain to be solved. On the theoretical modeling, how can the effect of the vibration be evaluated? How can the flow pattern be judged: it is laminar flow or turbulent flow? Also, how can the heat transfer process be modeled if water spray is used to accelerate the cooling? On the experimental study of the cooling process, how can the temperature profile be measured more accurately? How can the vibration magnitude be measured? How can the temperature under water spray be measured? These provide the objectives of the present thesis. This thesis includes two sections: (i) experimental study: set up a system to measure the fiber glass temperature profile under different 37 drawing speeds and different diameters. Both with and without water spray cooling. The data, on one side, can help in understanding the cooling process, especially under water spray cooling; on the other side, it can validate the theoretical model and finally lead to an experimental correlation, which is directly useable in the factory. (ii) the theoretical model: An existing model (built by a former master student in this lab) considers the effect of different drawing conditions and water spray cooling to predict the temperature under conditions similar to our experiments. But by comparing, we can revise the model. The model also helps to improve the experimental design. 38 3.2 Proposed Solution Methods 3.2.1 Proposed theoretical modeling method The von Karman-Pohlhausen laminar boundary layer integration technique was widely used in previous studies. The fiber temperature profile predicted by using it agreed with the experimental data of Arridge [3.1] and Madisson [3.2]. This technique will be used in our theoretical model. Sweetland [3.3] developed a model further to consider the water spray in the fiber cooling. We will adopt this model in the present study. Kase and Matsuo [3.4, 3.5] mentioned that vibration of the fiber could enhance heat transfer up to 30%. A series of papers [3.6-3.18], which studied vibration in fiber drawing, will be used as references to understand its effect on the fiber cooling. The stability in fiber drawing is a difficult topic. Sakiadias [3.19] extended the same integration method used in laminar boundary layer flow with a different velocity assumption to solve the turbulent boundary layer, but he failed to get a satisfactory result. Glicksman [3.20] used the Reynolds analogy in turbulent flow and got an expression for the Nusselt number. However, from Figure 2.2, we can see that this result is very close to that developed from the laminar flow via the von Karman-Pohlhausen technique. Therefore, more study needs to be done before selecting a preferred approach to turbulent transition. 3.2.2 Proposed experimental method The measurement of glass fiber temperature usually involves two fundamental methods: contact methods, such as thermocouple techniques, and non-contact methods, such as the thermal-imaging technique and the pyrometer. Both the contact methods and the non-contact methods can measure the temperature of a large-sized body accurately, but they do not easily allow accurate temperature measurement in a small-sized body, such as a glass fiber. In the case of the 39 thermocouple method, for example, this is because the fiber is small compared with the thermocouple. The heat capacitance of the thermocouple junction is large enough to change the temperature of the fiber when contacting it. Thus the measured temperature is not the real temperature of the glass fiber. On the other hand, for non-contact methods such as the pyrometer, the size of typical reinforcing fibers (~10 micrometers diameter) is smaller than the spatial resolution of the pyrometer above 100pm. Therefore, the effect of the background noise can be too big, compared with the effective thermal radiation signal, to obtain an accurate temperature for the fiber. However, large fibers, like optical fibers, have been measured optically [3.21]. To overcome the above stated problems in measuring the glass fiber temperature, a heated thermocouple technique [3.22, 3.23] has been adopted in this experiment (to be discussed in next section). We measured the temperatures of glass fibers with drawing speeds ranging from 1 m/s to 6 m/s, and diameters ranging from 20 to 50 pm. 3.2.3 Mechanism of Heated Thermocouple Technique bh d IIV MVZ it C h v b' Figure 3.1 An example of heated thermocouple in measurement [3.24] The heated thermocouple technique uses a thermocouple whose measuring junction can be adjusted to any preferred temperature (see Figure 3.1). The temperature of the thermocouple junction is equal to the temperature of the measured glass fiber if the temperature of the former does not change when the 40 junction makes a light contact with the fiber. Compared to the regular thermocouple method, the advantage of this method is that it can measure the temperature of a small object with little error [3.21, 3.23]. Arridge [3.1] and Maddison [3.2] also adopted this method in their experiments and showed that the heated thermocouple method can measure a thin filament's temperature. 41 3.3 Summary In the chapter, we set our objectives in the study of fiber cooling. The research will be performed from both theoretical study and experimental measurement. We will adopt von Karman-Pohlhausen boundary layer integral technique in the theoretical modeling. The heated thermocouple technique will be used to measure the fiber temperature both without water spray and with water spray. 42 Chapter 4 Experimental System Design and Proof Testing In this chapter, we will introduce the experimental system, especially the measurement system. In the first part, we briefly describe the whole experimental system we set up. Then, the temperature measurement system is detailed described in detail. Following that, we present the two measurement methods. Finally, an experimental proof test is performed to verify the accuracy of the method. 4.1 The Experimental System Our laboratory experimental system (see picture 4.1) consists of three parts: the fiber production subsystem, the control subsystem, and the temperature measurement subsystem. 43 Figure 4.1 The experimental system The fiber production subsystem's function is to melt the glass marbles using electrical heat and then draw the fibers into a winder. The fiber glass forming process involves a combination of extrusion and pultrusion of molten glass through a 3x3 array of orifices (bushings) in a platinum-iridium bushing plate. The bushings are heated electrically and maintained at a constant temperature of around 1500K. The glass is pulled through the orifice by a take-up reel as well as pushed through by the hydrostatic pressure of the molten glass above the bushing. This causes the glass filament to neck until it solidifies to its final diameter, which is on the order of 10 gm. Necking and solidification occur within a short distance from the bushing. The resulting filaments are brought together and passed across a surfactant applicator, which binds the filaments together into a single fiber. The fiber is then pulled onto a winder [4.1, 4.2]. 44 The principal parts in this subsystem are platinum bushing, which is a tank where the glass marbles are melted and from which the glass is drawn; the transformer, which supplies electrical heat to melt the glass; the water cooling circuit, which prevents high temperature rise in the electrical leads; and the winder, which pulls and wraps up the fiber (see figure 4.2). Figure 4.2 The winder The control system mainly controls two variables: temperature inside the bushing and the speed of the winder. Temperature control system consists of a built-in thermocouple in the inner wall of the bushing, which provides input to a controller (Eurotherm) that adjusts, the thyristor driving the transformer. The thyristor adjusts the current supply to the bushing, changing its temperature (see figure 4.3). 45 Figure 4.3 The temperature control system The speed of the winder is controlled with-a LabView program user interface, which was designed specially for the experiments (see figure 4.4). The interface also monitors the bushing temperature. 46 Figure 4.4 LabView program user interface [4.1] 47 4.2 Temperature Measurement Subsystem Design The temperature measurement subsystem consists of three subsystems: a thermocouple heating subsystem, a measurement subsystem, and a mechanical fiber traversing subsystem. tiusnina I A/D Nozzle Computer thermocouple probe Computer +- Motor Glass Fiber Drum Figure 4.5 Sketch of temperature measurement system for glass fiber 4.2.1 The thermocouple heating subsystem The heating subsystem includes an electrical heater, an adjustable electrical resistance, an adjustable voltage source and an amp meter (see Figure 4.6). The heater is a Ni-Cr thin plate, which is installed on the tip of a three-bondedcylinder bracket. The Ni-Cr plate is wired with copper wires, which go through the holes of the two outer cylinders and are connected to the power source to create 48 a circuit. The thermocouple junction is affixed by cement on the surface of the plate. It is electrically insulated from the heater. The temperature of the Ni-Cr plate increases due to electrical heating when current flows through it. The plate transfers the heat to the thermocouple junction to raise its temperature. Different temperatures of the thermocouple junction can be obtained by adjusting the supplied voltage. Thermocouple Probe Adjustable Resistance Amp Meter Power Figure 4.6 Cross-section of heating subsystem 4.2.2 The measurement subsystem The measurement subsystem includes a thermocouple, a PC-4350 board and a computer. The voltage signal containing temperature information from the thermocouple is converted to a digital signal by the PC-4350 board. Then the signal is input into the computer. The computer transforms the voltage signals into temperature signals, shows them on the screen, and saves them for later analysis. 49 4.2.3 The mechanical fiber traversing subsystem [4.2] The heating system and the measuring system are fixed together and supported by a cylinder that can move in three directions along a three-dimensional traverse. The temperatures at different locations along the glass fiber can be measured by moving the cylinder. _ I_ - -- -I I) 1-DPositkioing Table HIIa 2-DPositonig Table Figure 4.7 The three-dimensional traverse subsystem [3.2] 50 4.3 Measurement Methods Before discussing the measurement methods, we first show the response of the thermocouple when contacting an object. Three types of responses of the junction temperature are possible when the thermocouple slightly contacts the measured object (see Figure 4.8): 12001 1 (ii) 900 -4 CL e (i) 600- - 300 1 201 401 601 801 Time (0.1 second) Figure 4.8 Steady temperature profile when a probe is contacted or uncontacted under different currents (i) An upward peak is observed when the fiber is contacted at around 220 seconds as Figure 4 shows. This means the temperature of the thermocouple is lower than the measured object. When they contact, the object transfers heat to the thermocouple to raise its temperature. (ii) A downward peak is observed at around 700 seconds as Figure 4 shows. This means the temperature of the thermocouple is higher than the measured object. The temperature of the thermocouple decreases when it contacts the object. 51 (iii) No obvious change occurs to the thermocouple temperature upon contact. This means the temperature of the probe is very close to the temperature of the measured object. Almost no heat is exchanged when they contact. Depending on the state of the thermocouple when contacting the glass fiber, two measurement methods, steady state and transient state, can be used in measuring the glass fiber temperature. 4.3.1 Steady state measurement method If the steady state measurement method is used, contact is made only when the temperature of the thermocouple is steady. In the first procedure, an estimated temperature is set, and then the thermocouple is permitted to contact the object. One of the above mentioned three response types will occur. If type (i) happens, we increase the current of the circuit to increase the junction temperature; if type (ii) happens, we decrease the current to reduce the junction temperature; or if type (iii) happens, the temperature of the glass fiber is obtained. Under type (i) & (ii), after adjusting the current to obtain another steady temperature, we make another contact. This loop will be repeated until type (iii) happens. The advantage of this method is that we can adjust the current to any preferred temperature. This method was used in the current experiments. 4.3.2 Transient state measurement method In the transient measurement method, contact occurs while the temperature of the thermocouple is cooling (see Figure 4.9). In this procedure, the thermocouple temperature is first allowed to rise to a temperature that is little 52 360 34. . 350 -340 - - ---- Temperaure change curve without contact ......- Temperaure change cur with contact 330 - 320 - measured temperaure 310 300- 1 25 50 Time (0.1 second) Real T=331 K 75 100 Figure 4.9 The transient temperature profile under current cut-off higher than that estimated for the object. Then the current is reduced or cut off to let the probe temperature drop. At the same time, the object is repeatedly put in contact with the thermocouple. A temperature profile like in Figure 5 will be recorded. By analyzing the measurement data, the temperature of the object can be obtained. The figure shows that the temperature peak is downward during first contact; this means that the probe temperature is higher than that of the object because the probe is heating the fiber. Following that, no temperature peak can be found during contact, and it means the thermocouple temperature is near the temperature of the object. Later, upward temperature peaks can be found, indicating that the probe temperature is lower than the temperature of the fiber and that the fiber is heating the probe. The temperature of the object can be read from Figure 4.9. The advantage of this method is that the object temperature can be obtained rapidly. However, its accuracy may be greatly affected by the contacting frequency. 53 4.4 One Dimensional Fin Model Test A copper wire's temperature is measured by the heated thermocouple method as a proof of the accuracy of this method (see figure 4.10). Tair A wire TebCopper Figure 4.10 Model test sketch The straight and thin copper wire can be considered as a long fin. Its one side is heated and the other end is free in the air. Its temperature was measured by a heated thermocouple and the base temperature, Tb, is measured with a regular thermocouple. The theoretical distribution can be obtained according the fin temperature distribution equation [4.3]. 54 d 2(T-Tco)p2(TT)O dx2 T Ix=0 = Tb (4.1) dT dx =0 x=L pf=h Solve equation 4.1, we have the theoretical temperature along the fin as (T - T ) cosh[/(L-x)] T(x) = T + +0 b 00 cosh[piL] (4.2) where heat loss from the free end is assumed to be small. The temperatures along the fin from the measurement are compared with the theoretical results in Figure 4.11. 300 250 - T,=23 0 C Tb=193 C p=20.3m~ L=11.5cm * Measurement data Theoretical prediction 200 _ 00 a) 150 - 100 - a) U) 0. E a) I- 50 - 0 0 2 5 Distance (cm) (a) 55 6 r 250 250- T,=220 C Tb=181 0 C L=11.5cm p=24m' 0 Measurement data Theoretical prediction 200 - 1500) CU 100- E 50 - 0- 9 8 7 6 5 4 3 2 1 0 Distance (cm) (b) 300 - ________________ Te=25 0 C Tb=228"C 250 -p=25m' L=11.5cm Measurement data * 2 Theoretical prediction - . 200 150 - CU 100 50- 0 . 0 1 2 4 3 5 Distance (cm) (c) 56 I1 - 6 7 8 300 T,=250 C T b=190C 1 p=27.5m~ L=11.5cm Measurement data 0 Theoretical prediction 250- . 200 - 00 - (D - 100a) F- 50- 00 2 4 6 i 8 10 Distance (cm) (d) Figure 4.11 The measured and theoretical temperature distribution along a copper fin Four groups of data obtained four different days show that the errors of the measurement are within 10%. This proves the method is accurate. 57 4.5 System Operation and Data Acquisition Usually, the experiment has three steps: 1) Startup the system and produce the fiber; 2) Perform the measurement and record the data; 3) Repeat or shutdown the system. 4.5.1 Startup the system and produce the fiber [4.1] This process always takes two to three hours from start. The major steps include: 1. Turn on the cooling water system and fill the marbles into the bushing; 2. Set the bushing set-point temperature as 2400 *F; 3. Turn on the bushing power switch; 4. Wait for one hour or more until the bushing temperature to reach 2400 *F; 5. Wait another one hour to let the marbles completely melt and reach a steady temperature of 2400 *F; 6. Change the bushing temperature to 2250 *F and wait until it becomes stable; 7. Turn on outside air pressure to the bushing and wait for the glass to start flowing out; 8. Use steel poker to pull the glass to the winder. This needs high skill and requires a great deal of practice; 9. When the fiber is drawing steadily, measurement can be performed. 4.5.2 Measure the temperature and record This process always takes ten to fifteen minutes. One always needs to prevent the fiber from breaking. If it breaks, the data recorded will be no use. The major steps here are: 58 1. Turn on the supplied circuit to raise the temperature of the thermocouple to a preferred value and wait it reaching stable. The process is quite quick. 2. Let the probe make a gentle contact to the fiber. See the response in the screen, and change the current supply then. Try the second contact to see the response until almost no change when contact happens compared to no contact. Then change the current supply and perform another two measurements at the same location. 3. Change locations and perform another measurement same as step 2. 4. Finish all the measurements and then turn to record and analyze the data. If during the measurement the fiber breaks, you need give the data and remeasure from the start point. 4.5.3 Refill marbles or shut down If you want to continue another measurement, you can refill marbles and repeat the steps in the first and the second part. If you want to shutdown, you need set the temperature in the bushing to 0 *F first. Then wait for about one to one and a half hours until the temperature drops to 600 OF. Then turn off the power supply. Finally, cut off the cooling water supply. Thus one measurement cycle is finished. 59 4.6 Summary A laboratory scale experimental system was described in this chapter. Each subsystem was described in detail. Two methods, which could be used in the experiments, were introduced. A proof test based on a copper fin shows this method can be used in the measurement. 60 Chapter 5 Data without Water Spray In this chapter, we describe our measurements without water spray in detail. We show the data graphically, using both dimensional and nondimensional coordinate systems. A brief analysis is provided along with the figures. 5.1 The measured method under no water spray As described in section 3.5 of the last chapter, once the system is producing thin glass fibers at a steady state, the measurements can start. Measurements under no water spray are relatively easy compared to that with water spray. The main steps in the measurements are setting a preferred steady temperature for the thermocouple tip, making a slight contact, then adjusting the current supply till there is no obvious change to the probe due to the contact. Using this method, we always measured five to six along the drawing direction. During the initial measurements, we used 0.005" K type thermocouple, but these data were poor. We then changed the size of the thermocouple to 0.002" or 0.003" (under water spray). To ensure a "good" contact, we performed measurements three times at one location and averaged them. The drawing speeds we chose in the measuring are from 1 m/s to 6 m/s. If the speed is too slow, the diameter of the fiber increases thicker and it is easily broken. On the other side, if the speed is too high, the fiber is also easy to break in drawing. Figure 5.1 is a picture of the fiber being drawn. 61 Figure 5.1 Fiber drawing from the tips 62 5.2 The experimental data without spray Figure 5.2 to 5.7 shows data with drawing speeds of 1.76 m/s, 2.64 m/s, 3.53 m/s, 4.39 m/s, 5.27 m/s and 6.15 m/s, respectively. There are two pictures in each figure, picture (a) is the temperature profile at different locations, and picture (b) is the temperature of different times after leaving the bushing. Analyzing each figure, we find several common characteristics: i) at the first stage of cooling, the temperature of the fiber drops very quickly, then after several centimeters, the cooling rate decreases. It is expected in the final stage, that the cooling rate will go to zero. ii) in each figure, although we have set sane drawing speed, the diameter of the fiber still varied - that because the variation of the pressure in the bushing. iii) under the same drawing speed, the thinner the fiber is, the faster the cooling is. iv) we find it is impossible to measure the fiber temperature at the tip because the glass is in a liquid state and because strong thermal radiation and high temperature prevent the measurement there. 63 1200 0o 900 - 7 H 600Ti= 302 K V = 1.76 m/s -0- d=48.%pm -- 0- d=42.Opm 3001 0.10 0.05 0. 0 X (m) (a) Temperature distribution along the fiber axis 1000- 800- (D AA 600CO E 400- T,= V = -m-A- 29 0C 1.76 m/s d=48.0pm d=42.0pm 200 0 20 40 Time (ms) (b) Temperature as a function of cooling time Figure 5.2 Temperature profile when speed is 1.76 m/s 64 60 1200 Tk=302 K V = 2.64 mIs -vd=26.Opm d=28.5pm --- -, 900 2' -0-A- d30.0pm d=30.Opm -0- d=35.4pm V- I600 \A 300 0.00 0.15 0.10 0.05 0.20 X (m) (a) Temperature distribution along the fiber axis 1000 Tk= 29 *C V = 2.64 m/s -0- d=26.0pm --d=30.Opm -A- d=30.0pm --d=35.4pm A 800 - cc 600- L E 400 - - 200 0 30 15 45 Time (ms) (b) Temperature as a function of cooling time Figure 5.3 Temperature profile when speed is 2.64 m/s 65 60 1200 900- ITa= V = -M-A-0-- 600- 303 K 3.51 m/s d=36.Opm d=35.Opm d=28.Opm d=27.pm --------- 300 . i 0.10 0.05 0.00 X (m) (a) Temperature distribution along the fiber axis 1000T,= 30 "C V = 3.51 m/s -Ad=36.0 pm -v- d=35.0 pm -o- d=28.0 pm 800- p G) b.D 600 - CU L.. U) 0. E U) I- 400- 200 .4. 0 i 20 10 Time (ms) (b) Temperature as a function of cooling time Figure 5.4 Temperature profile when speed is 3.51 m/s 66 30 1200 v T =303 K V = 4.39 nms -0- d22.5pm -0- =22.5pm -el- d=21.0pm -A- d20.5pm 900- I600- -I0I 0.00 0.15 0.10 0.05 X(m) (a) Temperature distribution along the fiber axis 800 T.= 30 "C V = 4.39 m/s -Md=22.5pm 4 d=21.Opm -0- d=20.5pm 600 -0 ao L U -U E 400 () F- 0 . i 200 0 20 10 Time (ms) (b) Temperature as a function of cooling time Figure 5.5 Temperature profile when speed is 4.39 m/s 67 30 1200 900- S H 600T.= 302 K V = 5.27 nVs -0- d=23.Opm -- d=20.0pm 300 0 0.10 0.05 X (m) (a) Temperature distribution along the fiber axis 800 . Tk= V = -0-M- 29 -C 5.27 m/s d=2 3.Opm d=2 0.p 60000 a) L. CU I- 0) 0. E 4) 400- H 200 0 10 5 15 Time (ms) (b) Temperature as a function of cooling time Figure 5.6 Temperature profile when speed is 5.27 m/s 68 20 1200 T.= 302 K V = 6.15 m/s d = 20.0 pm -@- 900 - e@ H 600- 300A 0.10 0.05 0.00 X (m) (a) Temperature distribution along the fiber axis 800 -S 600 -0 CL E 400 -0- Ta.= 29 *C V = 6.15 m/s d = 20.0 pm 200 0 5 10 15 Time (ms) (b) Temperature as a function of cooling time Figure 5.7 Temperature profile when speed is 6.15 m/s 69 . 20 It is a little hard to compare the data at different drawing speeds. But we can find a non-dimensional coordinate system to put them together. Theoretical study [5.1, 5.2] shows that the non-dimensional temperature is a function of nondimensional distance, heat capacity ratio and Prandtl number. The expression is: o)f T = -T . ai TT-T. 0 air fr, " f(X, =(~,r = Pr) X =xv Ud2 Pr = Prandtl number (6.1) (pcP)air (p )fiber In these experiments, rl and Pr are constant. The non-dimensional form of the experimental data is listed in figure 5.8. We can see the data converge themselves very well. It shows that our measurements are consistent in the whole set of experiments. 70 1 D - -w U U U 0.8- U U * 0.6 U U - 0.4 - U * U. U 0.2 U - 0.0 * 0 500 I I 1500 1000 1 1 2000 vx/vd2 Figure 5.8 The experimental data in non-dimensional form 71 2500 5.2 Summary The whole process in measuring without water spray was described in this chapter. The data figures were listed as different speeds. The non-dimensional formulation of all the data shows the measurements in the whole experiments are consistent. 72 Chapter 6 Data with Water Spray In this chapter, we deal with the measurements under water spray. With water spray, the measurements become more difficult than without water spray. In the first part of this chapter, we check the difference between experiments with water spray and with no water spray. We redesign our probe for better measuring in the second part. In following part, we present our data. 6. 1 Understanding the measurements under water spray In all factory systems, the glass fiber pulled from the bushing is cooled by water droplets to hasten cooling. However, no reports have been seen of studies of this cooling mechanism using both experiments and theory. The reason is very simple: it is very hard to measure the temperature of the fiber under water spray. When the fiber is thicker, people can use optical methods to measure the temperature without water spray. But it is very difficult to use this method in the water spray because the water will absorb radiative energy. In the last chapter, we successfully used the heated thermocouple technique to obtain the fiber temperature. One thing needs to be checked: can we use this method in measurements with water spray? Before answering this, we need to analyze the difference between these two situations. 73 Water spray will enhance cooling process in three ways: first, the water droplets will evaporate close to fiber and thus take away a lot of heat; second, the water vapor in around the fiber will change the air properties surrounding the fiber - its heat capacity, density and conductivity; third, water spray will reduce the thickness of the thermal boundary layer. However, the water will also bring more difficulty in measurement. The droplets will cool the probe in the measuring, too. We have to add more power to sustain the temperature. Also, the spray will bring more vibration to the fiber because it has crossflow. Moreover, the spray will bring more fluctuation to the measurement. So, how big are these effects? Let's first check some data. Bushing 35 cm 15 c n E 0 Nozzle LIZ Drum Figure 6.1 The sketch of water spray 74 Figure 6.1 is a simple picture of the drawing with water spray. The approximate cross-sectional area of water droplets at the fiber is 15cm x 35cm. In our measurement, the gauge pressure is 45 psi and the water flow 24.4 ml/min. The average speed at x = 35 cm (reaching the fiber) is 3 cm/second. From the correlation equations of reference [6.1], the SMD (Saunter Mean Diameter) of the water droplets is 62 ptm. The average number density of water droplets: 4436 per cm 3 . It is equal to 0.90 ml water uniformly distributed in the 1000 ml air. So it is clear that the water droplets are very sparse. We assume that the water spray will not change the flow field in the drawing. However, we must check its effect to the heat transfer. We use the theoretical model, which is adopted from reference [6.2] to calculate the heat transfer coefficients for no water spray and for water spray (see Figure 6.2). 1500- 2 Without water spray h,=775 W/m K D = 20 pm V = 5.27 m/s - With water spray h e=1269 w/m2K SMD = 62 pm n = 4336 /cm3 0)0 10000 500 0.0)0 0.05 0.10 0.15 Distance (m) Figure 6.2 Heat transfer coefficient versus the distance along the fiber 75 0.20 So, how does the water spray change the heat convection coefficient of the thermocouple with 0.002"? It is hard to get an accurate result. We can use the following method to estimate: Method one is to adopt the data from the fiber with d = 50 tm: without water spray is 556 W/m2 K, with water spray is 681 W/m2 K. Above is only an estimated value. Sometimes when the water droplet happens to evaporate close to the thermocouple tip, the heat convection coefficient will be large compared with the average value. But from a time average viewpoint, the estimate may be reasonable. 76 6.2 Probe redesign and proof test with water spray The presence of water spray will take away more heat from the probe, so we need provide more current. Also, we need to redesign the probe to prevent the most of the sensor from being wetted with water spray. A revised device was designed to use in the measurements with water spray (see Figure 6.3). 1111111111111A i I I_ i 7777727727~777727~7777772X//2Z/zZ2Z ,2 __ I wzxzzzzzzzzzzzzzzzzzzzzzA U-shaped probe 7777773 Current supply Water shield Figure 6.3 The sketch of the revised probe We performed two groups of proof tests under water spray (see Figure 6.4). This tests were done on moving fibers. It is shown that this method still works with water spray after we made some improvements. So, we will use this technique in our measurements under water spray. 77 inn water spray affected region 800 - 2' U) L.. 600 - C', U) 0~ E U) I- v=2.64 m/s T=2 96K -NNo water spray, d=40 jim 400 - -m- has water spray, d=40 jim -e- No water spray, d=33 jim -0- has water spray, d=33 pm ' 200 0 i 8 4 16 12 Distance (cm) (a) 1200 water spray affected region 1000 cc - 800U L E 600- 400 200 v=3.51 m/s T= 296K -0- No wate r spray, d=23 Pm -0- has water spray, d=23 pm -0- No water spray, d=30 pim -0- has water spray, d=30 pm - U 4 ' 0 8 4 12 Distance (cm) (b) Figure 6.4 Measurement under water spray 78 16 6.3 Experimental data under water spray Similar steps were used as in the measurements under no water spray. We chose the drawing speeds from 1m/s to 5.27 m/s. When the speed is above 5.27m/s, we found it is very hard to perform one complete set of measurements while keeping the fiber from breaking. The data are shown in Figure 6.5 to 6.10. Each figure has two pictures - one indicates the temperature profile along the fiber axis and one indicates the temperature change versus the time. The following conclusions can be drawn from the figures: 1. Water spray enhances the cooling process. The no spray case will have the slowest cooling speed in a group with fixed speed and similar diameters; 2. The locations at which the spray starts will affect the cooling process. At the same location, the curve whose spray starts earlier will have a lower temperature than that whose spray starts later. 3. In the final stage of cooling, the cooling effect of water spray becomes less obvious. 79 1200 - 900 - -M- d=44.Osm, no spray d=44.5pm, spray starts @ x=0.023 m -0- d=42.0pm, spray starts @ x=0.073 m 40 U U 0 E U * * 600 - Tir U 0 ~~O~~ -'~ -I- U 0 Z0 V=1.00 m/s 300 I.nn 0.15 0.10 0.05 0.00 X (cm) (a) Temperature distribution along the fiber axis 800 600 -0 00 0) L. 400 CU I-. 0) 0. E 0) H 200 0 T= 26 C V=1 .00 m/s -U- d=44.0pm, no spray m -0- d=44.5pm, spray starts @ x=0.023 -0- d=42.Opm, spray starts @ x=0.073 m 0 I 0 80 40 I * . 120 Time (ms) (b) Cooling history in fiber drawing Figure 6.5 Temperature profile when speed is 1.00 m/s 80 -1 160 1200 no Spray spray starts @ x=0.00m spray starts @ x=0.04m -E-e-A- artLO 900 - 600 - = n0 . x%",A II cc L E -m- v=1.76m/s d=35pm -e- v=1.76m/s d=33pm v=1.76m/s d=36pm v=1.76m/s d=35pm -- A-v- 1 300 0.20 0.15 0.10 0.05 0.00 X (m) (a) Temperature distribution along fiber axis 800 - 600- 0) 1... 4-a CU 1... 0) 0. E 0) H 4007 200 V=1.76 rn/s - -0- d=35 pm no Spray -0- d=33 pm spray starts @ x=0.00m -A- d=36 Am spray starts @ x=0.04m -V- d=35 pm spray starts @ x=0.08M 0 -II I0 20 40 60 80 Time (ms) (b) Cooling rate in fiber drawing Figure 6.6 Temperature profile when speed is 1.76 m/s 81 100 1200 ----A-0- d=30pim, no spray d=30pim, spray starts @ x=0.00m d=29pm, spray starts @ x=0.06m d=29pmn, spray starts @ x=O.1Om 900 (D L E 600 300 -.1 V 2.64 m/s Tair = 25 *C -. 0.00 0.15 0.10 0.05 X (m) (a) Temperature distribution along fiber axis 800 600 - 400CU E V = 2.64 m/s T,= 25 C d=30pim, no spray -Ud=30pm, spray starts @ x=0.00m ----A- d=29pm, spray starts @ x=0.06m -0- d=29m, spray starts @ x=0.IOm 200- 0 .1 0 . 30 15 45 time (ms) (b) Cooling history in fiber drawing Figure 6.7 Temperature profile when speed is 2.64m/s 82 60 1200 -M- d=27.0pm, no spray -0- d=28.Opm, spray starts @ x=0.09 m -A- d=26.5pm, spray starts @ x=0.06 m --- d=25.Otpm, spray starts @ x=0.00 m 900 L- CL E 600 - U) TaIr =260 C V=3.51 m/s 300 ,in- 0.00 0.10 0.05 0.15 X (m) (a) Temperature distribution along fiber axis 800- 600- (D400Cu E U) Ta =260C V=3.51 M/s d=27.0im, no spray -U-0- d=28.0pm, spray starts @ x=0.09 m -A- d=26.5pm, spray starts @ x0.06 m d=25.Opmn, spray starts @ x=0.00 m --- 200- 0 .41 0 30 15 time (ms) (b) Cooling history in fiber drawing Figure 6.8 Temperature profile when speed is 3.51 m/s 83 45 1200 . -0- d=23.5pm, no spray -O- d=22.Opm, spray starts @ x=0.02m -A- d=24.Opm, spray starts @ x=0.05m -0-- d=23.5pm, spray starts @ x=0.08m U) L. 800 - 4-a CU L. U) 0~ E U) F- Tair =260 C V=4.39 m/s 400 0.00 0.15 0.10 0.05 X (m) (a) Temperature distribution along the fiber axis 800 T.= 26'C V=4.39 m/s -0- d=23.5pm, no spray -4-- d=22.Opm, spray starts @ x=0.02m -A- d=24.0prn, spray starts @ x=0.05m -0- d=23.5pm, spray starts @ x=0.08m 600 - cP U) I4-. CU I- U) 0~ E U) 400- H . i . . i0 200 0 20 10 30 time (ms) (b) Cooling history in fiber drawing Figure 6.9 Temperature profile when speed is 4.39 m/s 84 40 1200 -0-A---0- a) d=21.Opm, d=20.Opm, d=20.0pm, d=22.5pm, no spray spray starts @ x=0.023m spray starts @ x=0.043m spray starts @ x=0.093m 800 L E a) = 2 50C V=5.27 M/s Tar 4A fl A- 0.00 0.15 0.10 0.05 X (m) (a) Temperature distribution along the fiber axis 800 600 0 - 400- E () 200- 0 Ta= 25 C V=5.27 n/s d=21.pn, no spray -U-A- d=20.0pm, spray starts @ x=0.023m -4- d=20.Opn, spray starts @ x=0.043m -0- d=22.5pm, spray starts @ x=0.093m -F 0 -LI_____________________________________________ 10 0 _____________________________ 20 time (ms) (b) Cooling history in fiber drawing Figure 6.10 Temperature profile when speed is 5.27 m/s 85 30 6.3 Summary An analysis was performed before we made any measurements with water spray. Our tests show that after some revision, the heated thermocouple method can be used in our measurements under water spray. A series of data were obtained with water spray. Analysis shows that the spray can enhance heat transfer but the magnitude depends on the location at which spraying starts. 86 Chapter 7 Error Analysis We have obtained measurements of the fiber's temperature with water spray and without water spray. Now it is time for us to establish the accuracy of these data, i.e., we need perform error analysis on these data. Before we do that, we first need to identify the error sources in the measurement. 7. 1 Understanding the error sources Error usually comes is of two types: one is systematic error and the other is random error, assuming that we have performed the experiments correctly [7.1]. The systematic error we consider here includes limitations of the system resolution and loading error. We used K type thermocouples and National Instruments 4350 DAQ board in our measurement system. The former will have ±6K maximum errors in our measurement range; the precision of the later is ±2K. As to the loading error, it occurs because the measuring process inevitably alters the characteristics of both the source of the measured quantity and the measuring system itself [7.1]. The measured value will always differ by some amount from the quantity whose measurement is sought. Normally, when a thermocouple is used to measure a large, still body, the loading error is so small 87 that it can be neglected. But when the object is so small that it has lower mass than the thermocouple, the loading error can be very large. The loading error in the present experiments is of critical importance in our measurements because we use tiny thermocouple sensors and because the glass fiber is so small. To estimate the magnitude of the loading error, we need understand the characteristics of our measurement system. The measured object is a moving thin glass fiber of 20 to 50 micrometers diameter. It is hot and is cooled by air or water spray while being drawn. Our measurement sensor is K type thermocouple. Its diameter is 50 to 75 micrometers. The size of the fiber is less than the size of the thermocouple. Also, because the fiber is moving, we have to consider frictional heating when the thermocouple contacts the fiber while measuring. Moreover, because the thermocouple size is very small, its temperature will fluctuate with the environment. Generally, we need consider the loading error from the following four sources: i) the temperature fluctuation of the thermocouple under the air or water spray due to its small size; ii) the temperature change of the fiber and the sensor due to heat exchange between them when they contact; iii) the temperature increase of the fiber and the sensor because the friction between the fiber and the thermocouple generates heat which flows into them; iv) the thermocouple cooling when it enters the boundary layer of the moving fibers. In the following sections, I will analyze each item one by one. The temperature fluctuation of the sensor happens due to the small heat capacity of the thermocouple. The fluctuation can be recorded by the computer when we provide constant electrical current to heat the thermocouple. We find its temperature varies about a fixed value. The magnitude of variation may differ with and without water spray. When the thermocouple contacts the fiber, heat conduction will occur since they are not exactly at same temperature. This heat flux can be big in an unheated thermocouple measurement because the temperature difference is big. But, in the heated thermocouple method, because we can adjust the temperature of the sensor to match the fiber, the heat flux will be small - this is the advantage 88 of this method. However, because of the small size of the fiber and the sensor, we still need to check the magnitude of the transient conduction error. We will build a simple model to estimate the value. The frictional heating while measuring is an unknown factor in the error analysis. To calculate the value, we need to know the frictional force, which is small. To check this, we use a sensitive force measurement instrument to measure the normal force applied to the fiber in measuring. We obtain the frictional force and the frictional heating. Figure 7.1 is a picture of the instrument, which is used to measure the normal force later. Fig. 7.1 Instrument used to measure the normal force Another error source to be considered is the boundary layer cooling. The fiber is moving during in measurement. Thus there is a very thin thermal boundary layer around the fiber. The thermocouple sensor will enter the boundary layer 89 during the measurement, whereas it is outside the boundary layer before measuring. Before measuring, there exists only natural convection heat transfer to the sensor, but while measuring, the sensor is cooled by forced convection inside the boundary layer. We need to consider the effect of difference in the thermal resistance. As to the random errors, we don't perform detailed analysis here because random error is not as important as systematic error in present experiments. We have also performed three measurements at each point and taken the average of these values as the temperature. It is considered that if the temperature difference between two measurements is within 10K to 15K, the two contacts are "good". This method, on one side, can check if the contacts while measuring are "good"; on the other side, it can reduce the random error. 90 7.2 Error estimation without water spray 7.2.1 Temperature fluctuation The typical temperature fluctuation was measured as follows. We set everything the same as when performing experiments except that we don't let the sensor contact the fiber. The location of the sensor is now outside the fiber boundary layer. The current is held fixed, and when the temperature of the thermocouple reached a steady mean value, we began to record the fluctuating temperature signal. The temperature as a function of time is shown in Figure 7.2. 875 - no water spray T = 678 K ST = 16.5 K 7750 625 500 0 100 200 300 400 500 600 Time (Second) Fig. 7.2 Temperature fluctuation without water spray It was found that a change of fiber drawing speed has no effect on the fluctuating signal. Also, changing the current supplied has only a small effect on the fluctuation of the thermocouple. So, from the figure, we can conclude that the standard deviation of the fluctuation of the thermocouple is around ±16.5K. This 91 standard deviation is presumably lower when the temperature difference between the probe and the air is lower. 7.2.2 Heat conduction between the fiber and the sensor In regular measurements using thermocouples, heat conduction is the "driving force" to let the thermocouple's temperature approach the object's temperature. We don't care about the change in the object's temperature because it is always assumed that the object's heat capacity is large enough that the heat flux doesn't affect its temperature. But in our situation, since the thermocouple has a large heat capacity relative to the fiber, we need to determine whether the measurement alters the temperature of the fiber. wire sernsor fiber wire L Fig. 7.3 Sketch of the contact 92 Table 7.1 Properties of glass fiber and K type thermocouple Density Diameter 5 Capacity Conductivity (kg/m 3 ) (xl 0- m) (J/kg.K) (W/ m.K) 8500 5.0 420 19 (Ni/Cr) K type thermocouple 32 (Ni/Al) Glass fiber 1300 2 - 5 2600 2 The heat transfer rate during contact is estimated by Q conduction I4 D k AT (7.1) We choose ATfi= 30K (that is the largest AT we estimated to occur during a heated thermocouple measurement that appears to be properly adjusted), L = 50gm, Uf = 3 m/s, kft= (kf+ kt)/2 = 12.5 W/m-K. Thus AT fiber,conduction - ft 2 pCp fffUf D 4f 2 k tA TtDt2(7) pfCpfUfD L = 3.40 K This should be an upper bound estimation because the contact area is really less than I4 7Dt2 93 7.2.3 The frictional heating during measurement Although it is a very gentle contact that the sensor makes with the fiber, it is still necessary to check the frictional heating effects because the sensor is so small and the fiber is in motion. The frictional force is very small. Thus we need a very sensitive force or pressure detector to measure the normal force. In the present experiment, an electronic force gauge with 0.01 Newton resolution was used to measure the normal force during contact. The measurement system arrangement is shown as Figure 7.4. We set everything as in previous measurements but we attach the thermocouple sensor wire to the force tip of the force gauge (see Figure 7.5). We use the sensor to contact the fiber and record the normal force with the detector. The results without water spray are shown in Figure 7.6. Fig. 7.4 The normal force measurement system 94 Thermocouple probe Fibe Force Measure Gauge Fiber\ Force Sensor movement . Fig. 7.5 The sketch of the force measurement arrangement 95 12.5- without water spray = 3.76 *10-2 N F 10.0- SF= 1.31 *10-2 N Z7.5- 5.0L.. (aE 2.50 z 0.0- -2.50 5 10 15 20 25 30 Measurement number Fig. 7.6 Normal force without water spray for repeated measurements Thus the normal force is around (3.76±1.31) x10-2 1b. We measured the normal force at a drawing speed of 5.27 m/s and along the whole measuring length of fiber. That high speed is expected to have the largest value of friction. The friction coefficient of the glass fiber is 0.25 [7.2], thus the frictional force is (4.27±1.49) x10-3 Newton. The contact time in the measurement is around 0.2 second. So the frictional heat is Qfriction = UfFfictionAt (7.3) = 0.0045J Assume that one half of the heat flows into the fiber and the other one half of heat flows into the thermocouple. The temperature rise of fiber due to frictional heating is then: 96 fI f ,friction 1D 2friction 2Uf AtpfCpf 2x0.0045 (7.4) 3.14x(20x10-6)2 x5.27x0.2x1300x2600 =2.01K Dt friction Figure 7.7 Sketch of friction heat flowing into the probe For the thermocouple, things will be a little more complex. Figure 7.7 shows the friction heat flows into the probe. First, we use steady state conduction to estimate the temperature jump of the probe. This estimate is upper bound estimation because the real process is still in the transient state. Here the two wires can be treated as two long fins. The energy conservation equations are: 97 4 St,frictin( hf, + kNilCrAhwireP+ VkNiIAlAhwirP 2At (7.5) Here, hwire is the heat convection coefficient of the wires and hfc is the heat convection coefficient of the probe. From a correlation for the Nusselt number for cylinders, hwire can be obtained. The Reynolds number of the cylinder is Uf-Dt ReD (7.6) V a =3.6 Using a correlation equation for boundary layer forced convection [7.3], we have NuD = 0.3 + 0.62 Re 1/2 Pr1/3 D ( /4 1+(0.4/ Pr)213] D = 1.27 Thus, an upper bound for the forced convection coefficient is: h wire -kNuD D = (7.8) 1271W/n 2 K In a later section, we find hfc=1823 W/m2.K. So, the temperature increase is 98 Qfriction AT t,fricton = 2At 22 2 3frD 4h + kNi/Cr Ah.ire P+ kNi/ AlAh .irP (7.9) = 36.9K An alternative estimate is to consider the sensor with its wire as a single body. Within the 0.2 second of contact, the diffusion length, which is used in calculation of average heat transfer, is Ldiff =38 flux =wmAt = (7.10) 1.95mm The total energy balance should be 21 ATA riction (2pt Cp t + 2;rDt Ldiff hfc At) = 4LtL diff Qfiio fr""""o 2 (7.11) Thus At,friciton QfCiction = (ptCpt7rDt Ldiff +4;cDtLdffhfc At) (7.12) = 5.7K This evaluation is lower bound estimation because AT is not uniform along the sensor and the wires and also because forced convection cooling can't take so much heat away. We believe the lower bound is much more close to the "real" 99 error. But to be conservative, we adopt a weighted average of these two estimates as the uncertainty due to frictional heating. It is AT t, friction = (36.9 + 5.7)/ 2 - (7.13) 21.3 K 7.2.4 Boundary layer cooling Boundary layer cooling only happens to the thermocouple sensor before and when the sensor moves into the boundary layer that is generated by the moving fiber. The thickness of the boundary layer is around several millimeters. When the sensor contacts the fiber, it definitely lies inside the boundary layer, but before it contacts the fiber, it is outside the boundary layer. So the sensor experiences natural convection outside the boundary layer and forced convection in the boundary layer. The air average temperature is 302K. The average temperature of the sensor is 820K. So the boundary layer film temperature is 561K. At 561 K, the properties of air are listed in Table 7.2. Table 7.2 Properties of air at 551 K air Density Viscosity Capacity Conductivity Prandtl (kg/m 3 ) (10-6 m2 /s) (J/kg.K) (W/ m.K) number 0.645 43 1009 0.0418 0.69 Using Uf as an upper bound velocity, the Reynolds number is Re D = ft V (7.14) = 9.2 100 Using a correlation equation under force boundary layer convection [7.3], we have 0.06 Re2/3 NuD = 2 + (0.4 Re1/2+ RD ±OORD) = 2 + (0.4 x 9.21/2 = 1/4 + 0.06 x 9.2 2/3) x 0.690.4 (7.15) 3.27 Thus, an upper bound for the forced convection coefficient is: kNuD h-bi D (7.16) =1823 W/m2K For natural convection to a small sphere, Gr 3 - giATD 2 9.8x 1 x500x(75x10-6 3 302 -6 2 (7.17) - (43x10 ) << 1 So the Nusselt Number is 2.0 [7.3]. Thus 101 kN hna D = (7.18) W/m2 = 1115 The temperature drop of the heated probe due to moving into the forced convection boundary layer is A t,cooing -- ifD 2 (hbI -hna )ATAt ptCptrD2Ldiff _ (hbl -hna )ATAt (7.19) ptCptLdff = 9.8K This is an upper bound estimate. The fiber, before contact with the probe, experiences forced convection. Upon contact, no convection cooling occurs, so h is effectively zero. Thus, the cooling error should be f- A= Dt2 (hbl-O)AT PfCPf (7.20) 4 <<1 K 7.2.5 Overall Uncertainty Combining the various estimates, the overall uncertainty for the probe is 102 AT t,err = V(±16.5)2 + (21.3)2 + (-9.8)2 = 28.7 (7.21) K Also, the uncertainty for the fiber is A Tf,err = (±3.40)2 + (2.01)2 + (0)2 (7.22) = 3.95 K Generally speaking, the measurement has a little effect on the fiber temperature, and the loading error comes mainly from the thermocouple sensor. The overall measurement uncertainty, which includes both loading error and resolution error, is ATtotal,err + (6)2 )2 + (±3.95)2 (±29.5(7.23) + (±2)( = 29.7 K The relative error, based on a typical fiber-to-air temperature of difference 400K, is 14.8% at 95% confidence (2a level). 103 7.3 Error estimation with water spray For the case with water spray, we perform an error analysis similar to that without water spray. But first we need to carefully check the difference between these two situations. The difference in error sources without water spray and with water spray lies in: 1. Water spray increases the heat loss both from the thermocouple and the fiber, so that the temperature fluctuation in both will increase; 2. The atomizer produces cross-flow which overwhelms natural convection near the thermocouple probe; 3. The water spray reduces the thermal boundary layer thickness, so boundary layer cooling to the thermocouple doesn't change as much compared to the cooling outside the boundary layer. According to this, we only consider the errors that come from heat conduction between the moving fiber and the sensor, the frictional heating and the temperature fluctuation of the sensor under water spray. We don't consider the boundary layer cooling here. 7.3.1 Temperature fluctuation The system we developed and the procedure is same as without water spray. The temperature profile as a function of time is recorded in Figure 7.8. 104 875 750- L E 625- with water spray T = 708 K ST = 27.5 K 500I 100 0 I 200 I 300 400 500 600 700 Time (second) Fig. 7.8 Temperature fluctuation with water spray As before, the drawing speed has little effect on the temperature profile. Also, changing the electric current supplied also has a small effect on the fluctuation of the thermocouple. From the figure, it can be concluded that the standard deviation of temperature fluctuation of the thermocouple in the presence of spray is around ±27.5K. Same as before, ST will be lower if the temperature is closer to the probe temperature. 7.3.2 Heat conduction between the fiber and the sensor Here, we choose ATft= 42K (this is an estimated value and we will check it when the overall uncertainty is obtained), L = 50ptm, Uf = 3 m/s. The heat transfer rate is calculated as 0 Qft 2 =4VrDtk 4 t ft AT L (7.24) ' 105 And ATf= f, 2 4pfCpfUf ;rDf SkftATftDt2 (7.25) PfCpfUfD L =4.7 K As before, this should be an upper bound estimation. 7.3.3 The frictional heating in measurement Fig. 7.9 The normal force measurement system under water spray 106 To keep water spray off the force detector, we installed a shield to cover the instrument. The measurement system arrangement is shown as Figure 7.9. The results without water spray are shown in Figure 7.10. 16 with water spray Fave = 5.70 *10.2 N 12- aF M C) = 1.98 *102 N 0 80 LL 0 z U. U * 4- U 0 2 0 5 15 10 20 25 30 Number Fig. 7.10 Normal force with water spray Thus the normal force is around (5.70±1.98) x10- 2 N. We measured it at drawing speed is 5.27 m/s and along the whole measuring range. The friction coefficient of the glass fiber is 0.25, thus the frictional force is (6.47±2.25) x10-3 Newton. The contact time in the measurement is around 0.2 second. So the frictional heat generated is Qfriction = UfFfitionAt (7.26) = 5.27 x 6.47 x 10-3 x 0.2 = 0.0068J 107 The temperature rise of the fiber due to frictional heating is estimated by assuming that half of the heat generated flows into it. ATf,fiction -ffD 4Qfriction I 2UfAtpCpf 2x0.0068 3.14x(20x10-6)2 x5.27x0.2x1300x2600 (7.27) = 3.04K Still using the model from the last section, but we need to consider the properties of air with water droplets: Table 7.3 Properties of air with droplets (n=4436) at 551K Density Viscosity Capacity Conductivity Prandtl (kg/m 3 ) (10-6 m2 /s) (J/kg.K) (W/m.K) number 25.8 2669 0.249 0.78 1.088 air+droplets Here, for the wires U -D ReD (7.28) a =6.2 Using a correlation equation under force boundary layer convection [7.3], we have NuD =0.3+ 2 0.62 ReD 1/ r1/3 (7.29) 1+(0.4 / Pr)2/3 /4 D = 1.70 108 TJus, an estimate for the forced convection coefficient along the wires is: hwire -kNuD = D 7.30) 2 8466W/n K For h Re D =Uf Dt 7.31) V a( = 17.88 Using a correlation equation under force boundary layer convection [7.3], we have Nu =2 + (0. 4 Re1 = 2 + (0.4 x 9.21 Pr 4 + 0.06 Re2) + 0.06 x 9.2 2/3) x 0.690.4 (7.32) = 3.98 Thus, an upper bound for the forced convection coefficient is: h fc KNuD D (7.33) 2 =13 214 W/m K 109 So Qfriction 2At AT t,friciton 3rD 4 thfc+ A kN, /Cr Ah wire P+ kNiI AlAh wire p (7.34) = 18.9 K Another estimate is to consider the sensor with its wire as a single body. Within the 0.2 second of contact, the diffusion length, which is used in calculation of average heat transfer, is L diff -5 = flux 7aAt (7.35) =1.95mm The total energy balance should be ATt,friction (2ptCpt 4Ldi + 2 / DtLdiff hcAt) = "2 (7.36) Thus A7 t,friciton = Qfiction (ptCp tzDt Ldiff +4zt Ldiff hfc t (7.37) = 1.4K 110 This evaluation is lower bound estimation because AT is not uniform along the sensor and the wires and also because forced convection cooling can't take so much heat away. To be conservative, we adopt the average of these two estimates as the uncertainty due to frictional heating. It is (18.9 + 1.4) / 2 AT t, friction (7.38) = 10.2 K 7.3.4 Overall Uncertainty From the preceding calculations, the uncertainty due to the thermocouple is AT t,err = J(±27.5)2 + (10.2)2 (7.39) = 29.3 K And, the uncertainty of the fiber temperature is AT f,err = - (±4.74) 5.6 + (3.04) (7. 40) K Thus, the overall uncertainty, which includes loading error and resolution error, is 111 AT total,err = V(±29.3)2 + (±5.6)2 + (±6) + (±2)2 (7.41) = 30.5 K The relative error, based on a typical fiber-to-air temperature of difference 400K, is 15.3% at 95% confidence (2a level). 112 7.4 Summary We performed a thorough error analysis in this chapter, considering the effect of the measurement on the fiber and the probe. Analysis shows that the major error comes from the probe. The error analysis shows that without water spray, the uncertainty is 14.8% and with water spray, the uncertainty is 15.3%. These estimates are believed to be conservative. 113 114 Chapter 8 Theoretical Modeling and Comparison to Data In this chapter, a theoretical model is introduced to predict the cooling process. The integral technique - the von Karman-Pohlausen boundary layer integral method - was used to find the temperature distribution in the laminar boundary layer flow. The method, which is used in calculating heat transfer from a moving cylinder, developed by Dixon [8.1], is adopted in solving a single moving fiber. A Maple program based on this method, written by Matthew Sweetland [8.2], is used to evaluate the fiber temperature for both no water spray and with water spray. The theoretical results are compared to our experimental data. 8.1 Conservation equations and von Karman-Pohlhausen integral technique 8.1.1 Governing equations for a single moving fiber To simplify the study, we focus on a single moving fiber (see figure 8.1). We don't consider vibration during the drawing, either. The Reynolds number in our situation is on the order 104, so it is laminar flow. For the fiber, due to its small diameter, the Biot number in the r direction is far less than 0.1, so the fiber temperature will only change along drawing direction, x. For this low speed flow, the Mach number is much less than 0.2, thus the flow can be treated as 115 incompressible flow. Generally, the control equations for a laminar, steady state, incompressible flow on a continuous fiber in still air are: // --\ Fiber I - I4 Tf S (x) x Figure 8.1 A single moving fiber OU 6 r Vr (8.1) &:ci- r0 +r Ju -+ a pv- 22u t+2 oT U-+V-= o7 C+ k PC (r +r) 1 0 (8.2) r+r& rJ 0 (r P 0 The boundary conditions of Eqn. 8.1 to 8.3 are 116 r)T0 +r) C' (8.3) u =U,v = 0 u -> at r = 0 0,v -+ 0 T(x,r) T(x,r) (8.4) as r -+ oo Tfiber (x) at r = 0 = -+ T00 (8.5) as r -> oo 8.1.2 Von Karman-Pohihausen integral method The von Karman-Pohlhausen integral technique can be used in calculating the heat transfer from the fiber [8.3]. First, we can developed the momentum conservation equation in the boundary layer Velocity Boundary Layer Ax Momentum BL Control Volume --- -- o J2z(r + r)pu(r)dr + 0 f2zc(r + r)pu(r)dr N x 2fr + 0 f 2Jz(r + r)Pu(r)dr Ax (0 ro U Figure 8.2 Momentum boundary layer control volume 00 d f dx 0 2 (r + r)dr = 0 P0& r (8.6) P 0r r=0 117 Similarly, we can develop the energy conservation equation in the thermal boundary Thermal Boundary Layer Momentun Boundary Layer Momentum BL Control Volume ~ ~--------------/-------------/ ---- ---- - - -- ------------- - - - - - - f2r(r + r)pC u(r)T(r)dr + Op 0 fJ21r(r + r)pC u(r)T(r)drlAx d 0----- -------------- _---------- tfiber radius r fiber drawing speed U 0 ------------------------------------------------ ---------------- Op------------------------~---------------- Figure 8.3 Thermal boundary layer control volume d f pCPT(r)u(r)(r + r)dr = -r k |,_' + Jq,(r + r)dr (8.7) U 0 Since the temperature of the fiber changes along the drawing direction, we also have another control equation for the fiber 2604(T4 4 4)+2 dx ro dT) d dxA ((pCT)fU-k f 118 T T_ ) env 2k ro aT Or (8.8) r r0r (aT - 2zr0kvy )rr=O Ax +2 0 4 4 f env EAxc(T 1 - ) r( pCT)fU +(r2 ir(pCT)f U dT. 2 d k f o f dx o f d (pCT)fU)Ax d 2 d( k dx ofdx/ Figure 8.4 Control volume of fiber Following that, we need model the profiles of the temperature and the velocity within the boundary layers. Based on the work of Glauert and Lighthill [8.4] for axial flow over a long cylinder and the analysis of an infinite cylinder issuing from a slot by Sakiadis [8.5], the velocity profile and the temperature file are u(xy) U 1 a(x) In r i(x) r+ (8.9) u(x,r)O0 r > 6(x) U T(x,r)-T 1- T (x)-T In1 + I r T(x) (8.10) T(x,r)-T T (x)-T r > ST(x) = 0 00 where U is the speed of fiber drawing, To is the temperature at the tip of the bushing and T.o is the temperature of ambient air. From Eqn. (8.9) and (8.10), we can find the thickness of the momentum boundary and the thickness of the thermal boundary layer as 119 3(x) = (ea(x) ST(x) = r (e (8.11) (8.12) - 1) Now we have three equations, 8.6, 8.7 and 8.8, and three unknowns, Tf(x), a(x), and P(x). So, theoretically, we can solve the problem. But unfortunately, it is not so easy to get the solution. We need to do a little bit more work. First, we can derive an equation which only involves x and a as da dx 2 2. - )+ a + )(.3 = Urr2 02(e(a a 2 2v 2 (8.13) Bourne and Dixon [8.1] developed a differential equation for p as a function of a only in this case without water spray (q e = 0): d3 da P 2 a a (a- ,)(ae - sinh a) a cosh a - sinh a .- (8.14) 2ea2 [(1 + 8) sinh a - a cosh a - a eJ At x=0, 6= 6-r =0 and a=P=0 are the initial conditions. From this point, we set a value for a, then we can find x and P separately from Eqn. 8.13 and 8.14. Matthew Sweetland [8.2] developed a Maple program to solve these equations. His program was used in present study to calculate the temperature profile along the fiber drawing. He also developed a detailed theory for q e , the evaporative cooling effect, which is described later. 120 8.2 Items analysis on solving the fiber boundary layer flow We have set up a group of equations to solve the boundary layer flow. However, several items are still needed before we can do the simulation. First, we need to know To in eqn. 8.10, which is the outlet temperature of the fiber at the tips. Since it is pretty hard to measure To experimentally, we need estimate it using a theoretical method. To obtain To, we must first estimate another thermal boundary layer thickness -- the bushing thermal boundary layer below the tips. We also need to evaluate the heat sink due to the evaporation of the water droplets. 8.2.1 Estimate the thickness of the thermal boundary layer below the bushing Because the bushing and the tips are very hot, there must exist a thermal boundary layer below the bushing (see figure 8.5). The existence of this boundary layer will warm the fiber in this region and thus affect the fiber cooling. So we must first calculate the thickness of this layer and estimate its effect on the fiber temperature profile. 121 I F\ b am a T00 T Fiber if V T TTx X Figure 8.5 The sketch of the thermal boundary layer below the tips The natural convection boundary layer below the heated plate is affected by the unheated edges of the glass meter that surround the hot bushing plate. Hatfield and Edwards [8.6] developed a correlation equation to calculate the Nusselt number of this boundary layer. NuL = C1 [1 + C 4L / W][(1 + X) 'm -x 3m ]RaLn (8.15) n+ X = CRa" 2 L C3 (La L) a where C 1 , C2 , C3 and C4 are constants. L, W, and La are sizes of the plate (see figure 8.6). Here, C1 =6.5, C2 =0.38, C3 =13.8, C4 =2.2, L=5cm, W=5cm and La =10cm. 122 L W4 .~w La -0 I. ---------------------- ------------------.................. ........ Figure 8.6 Bushing surface dimensions (as viewed from below) According above parameters, we can estimate that the thickness of this thermal boundary layer is 1.5cm (60 = 2L/Nu). This value is used in later calculations. The existence of this thermal boundary layer has an obvious effect on the cooling process. It changes the initial temperature of the air surrounding the fiber and slows the initial cooling. This variation of Too can easily be added to the numerical model. Figure 8.7 shows the calculated thickness of the boundary layer with and without the warm boundary layer under the bushing. We can see that the bushing thermal boundary layer has little effect on the momentum boundary layer, it also has little effect on the thermal boundary layer around the fiber. Figure 8.8 is the temperature profile of the fiber with and without the bushing thermal boundary layer. The presence of this boundary layer will reduce the cooling rate of the fiber, but the effect disappears about 20cm away from the bushing tip. 123 0.020---- 0.015- V =4.39 n/s d =21 pm -- 8 without warm BL 8 without warm BL - with 1.5cm warm BL -6 with 1.5cm warm BL 0.010- 8t- .) |0.005- 0.000- 0.00 0.10 0.05 0.15 Distance (m) Figure 8.7 The effect of the bushing thermal boundary layer on the fiber boundary layers 1400 warm BL with 1.5cm warm BL -Without 1200- 1000Ca L E 800- a) 600 - 400 -L 0.00 0.05 0.10 0.15 0.20 Distance (m) Figure 8.8 The effect of the bushing thermal boundary layer on the fiber temperature 124 8.2.2 Determination of the initial temperature To at the tip Since it is hard to measure the tip temperature, To, experimentally, we have to use a theoretical method to extrapolate this value. We will use two steps to obtain it. First, we use curve fit from our experimental data to obtain a temperature T*o without considering the effect of the thermal boundary layer under the tips. Then, we add the effect of the bushing thermal boundary layer to correct the T*o and obtain To. 8.2.2.1 Using curve fits to extrapolate T*o We use several methods to fit our data to approach T*o when x approaches 0. The curves and fits are shown in Figure 8.9. 1400Experimental data 2nd order poly. fit T 1200---- 1000 - 1131K 3rd order poly. fit T =1236K 4th order poly. fit f 0 =1296K 1 nd order expo. fit T,=1 212K order expo. fit T =1241K 32nd I-- S800- -.. E . 600- 400- 0.00 0.02 0.04 0.08 0.06 0.10 Distance (m) Figure 8.9 Curve fits for T*o 125 0.12 0.14 So, we have an estimated value for T*o is (8.16) T o = 1223 ±60 K 8.2.2.2 The effect of the bushing thermal boundary layer Here, we first set T*o to 1223K and calculate the distribution of the temperature without considering the existence of the thermal boundary layer below the bushing. Then we calculate another T* considering the effect the thermal boundary layer. When these two curves are matched far downstream, we consider resulting value of T* to be the true To in the experiments. The final value is To as 1165 K, read from Figure 8.10. 1400- without warm BL (To=1223K) 1200- with 1.5cm warm BL (TO=1 165K) 10008003 a. E ai) F- 600400200- 0 1 0.0 0.10 0.05 0.15 0.20 Distance (m) Figure 8.10 Correction for the effect of the bushing thermal boundary layer 126 8.2.3 Evaluation of evaporation and radiation In the case with water spray, the effect of water droplet evaporation is very important in the cooling process. In the present model, we first study single droplet evaporation, and then we calculate the heat sink, qe, in equation 8.7 by considering the distribution of the water droplets in the fiber boundary layer. 8.2.3.1 Single water droplet evaporation As we stated in Chapter 7, although the volume density of the water droplets is very small, ts relative mass concentration is larger than 0.2. We use high mass transfer theory to estimate the evaporation of a single droplet. Mills [8.7] provide a solution for the water droplet mass evaporation rate as 12 = 2pD P'1 D ,, M, m '1s 1,s -m + 1+I 'Le MIs -1 J 2 = CPj(T -T) k1c D P nI+ Sn1 hf9(.7 (TP) s' This equation can be solved by iteration. From eqn. 8.17, we can develop a wellknown formula which describes the lifetime of a water droplet: (8.18) t D2 = D2 - k evap 0 where k evap = 8pD12 In I + M '1 (8.19) -'s M 127 if m,e is set to zero. 8.2.3.2 Heat sink in the fiber boundary To simplify the calculation, we make several assumptions about the water droplets in the fiber boundary [8.2]: 1. The droplets are fully entrained; 2. The relative humidity is 0% far from the fiber; 3. The transient warm-up time of the droplets are quite short compared to droplet lifetime; 4. The droplet diameter across boundary layer is uniformly at the spray's Sauter mean diameter, SMD; 5. Since the fiber is above Tsat and since few drops will collide with the fiber, we can assume no droplets will touch fibers; 6. The droplet density through the boundary layer varies linearly, i.e., n -no 05 Thus, the heat sink term in eqn. 8.7 is T 9 Td ( th d] f~~o+ r)4edr =J 2z(ro + r)[ dro)Ajhgr (8.20) 0 0 where rndrop nor 4r D 3P = L U a r ( (8.21) ro Combining eqns. 8.18 to 8.20, we can calculate the evaporation term in eqn. 8.7. 128 8.2.3.3 Evaluate the importance of radiation According to Sweetland's work [8.2], the importance of radiative heating of the fiber from the bushing is very small compared to the effect of forced convection cooling because the very small view factor. The fiber radiative heat loss to the environment can be examined by comparing the radiative heat transfer coefficient with the forced convection heat transfer coefficient (see figure 8.11). 10000 ------ Heat Convection Coefficient Heat Radiation Coefficient 1-4 1000 - 100C U cc 0.00 0.10 0.05 0.15 Distance (m) Figure 8.11 Comparison of radiation and convection heat transfer coefficients It is clear that the forced convection coefficient is almost two orders of magnitude larger than the radiation heat transfer coefficient. Thus, we don't need to consider thermal radiation in the cooling process. 129 8.3 Comparison between our experimental data and the theoretical prediction 8.3.1 Comparison for dry data Without water spray cooling, we may use the equations and assumptions discussed above, put our experimental parameters into the programs, and obtain theoretical predictions of the fiber temperature profile based on the von KarmanPohihausen integral technique. We put the data with these predictions into figures (see figure 8.12-8.17). In each figure, the diameter of simulation is the average of those diameters in the experiments. 1500 - Moving Fiber Laminar Boundary Layer Numerical Integration 1200- 900 - 600 - 300 - 2 H Ta-r= 332 K V = 1.76 m/s ---@- 0 El d=48.Opm d=42.0pm .4' - 0.00 0.05 , I. 0.10 0.15 0.20 X (m) Figure 8.12 Comparison of the experimental data and the theoretical prediction when the drawing speed is 1.76 m/s 130 1500 Moving Fiber Laminar Boundary Layer Numerical Integration 1200- 900 VV - H 600 - Tar = 332 K 2.64 mTVS 7d=26.Opm -4 h-d=28 .m -@- d30.Opm -A- d=30.Opn d=35.4pm -UV 300 0.00 = . 0.10 0.05 0.15 X (m) Figure 8.13 Comparison of the experimental data and the theoretical prediction when the drawing speed is 2.64 m/s 131 0.20 1500 Moving fiber laminar Boundary Layer Numercal Integration 1200- 7900 600 T,= 332 K V =3.51 nVs d=36.Opm --0- d=35.4pm -E- d=28.0pm -A- d=27.Qpm 300 0.00 0.05 0.10 0.15 0.20 X (m) Figure 8.14 Comparison of the experimental data and the theoretical prediction when the drawing speed is 3.51 m/s 132 1500 Moming Fiber Larmrnar Boundaiy Layer Numerical integration 1200- 900- H 600K T.=333 ar V =4.39 mfs d=22.5 pm 300- --0- d=22.5pm -M- d=21.Opm -A- d=20.5pm A I 0.00 I I I 0.10 0.05 0.15 X(m) Figure 8.15 Comparison of the experimental data and the theoretical prediction when the drawing speed is 4.39 m/s 133 0.20 1500 Moving Fiber Laminar Boundary Layer Numerical Integration 1200- 900- 600 - 300 0- T.=332 K ar V = 5.27 n/s d=23.Opm --@- d=20.Opm - - 0.00 , - - .I * 0.10 0.05 0.15 X (m) Figure 8.16 Comparison of the experimental data and the theoretical prediction when the drawing speed is 5.27 m/s 134 0.20 1500 Moving Fiber Laminar Boundary Layer Numerical Integration 1200- 900 - 600- 300 - T1 = 302 K V = 6.15 m/s -0- d = 20.0 pim 0 0.00 I 0.05 I 0.10 * * I 0.15 0.20 X (m) Figure 8.17 Comparison of the experimental data and the theoretical prediction when the drawing speed is 6.15 m/s From figures 8.12 to 8.17, we find that the theoretical results correctly predict the trend of the cooling and that the predicted values are close to our data. For a more convenient comparison of the data sets, we plot all data on a nondimensional coordinate system (see figure 8.18). 135 1.2 0 1.0- 0.8 - - I - 0.6 - b Prediction curve Experimental Data 0.4- 0.2 - 0.0 - 0 500 1500 1000 2000 2500 vx/Ud 2 Figure 8.18 Comparison of the experimental data and the theoretical prediction in nondimensional coordinate system Here we consider the effect of the bushing thermal boundary layer and use the corrected To in 8.2.2 as the initial temperature of the fiber. The comparison shows that our data are close to the prediction curve but a little lower than it. This finding is reasonable because the von Karman-Pohlhausen approximation typically underpredicts the heat convection rate, and in addition the model does not consider vibrational enhancement of heat transfer. 136 8.3.2 Comparison for data with water spray Using a similar process, we can provide the predicted temperature profiles for the cases with water spray. Here, we use the parameters we calculated in section 6.1. 1200 * * d=44.Opm, no spray d=44.5pm, spray starts @ x=0.023 m d=42.0um, spray starts @ x=0.073 m No spray numerical simulation -- --- spray x = 0.000 m with density 44361cr&3 --spray x = 0.075 m with density 4436/cm 900 (D L E 600- 300 Tar,= 260 C V=1.00 m/s -, - 0.00 -0 ~'~~ 0.05 0.10 -I 0.15 X (cm) Figure 8.19 Comparison of the wet data and the theoretical prediction when the drawing speed is 1.00 m/s 137 0.20 I 1200 * no Spray o Spray starts @ x=0.00 m A An I 900 Spray starts @ x=0.04 m No spray numerical simulation '"1, 'I AIgy 3 -.----.-.spray x= 0.045 m wit!1density 44361cm 3 - E) L.. At,- 600 - U ,inn , 0.00 0 A v=1 .7ms 0= Pim v=1.76m/s d=36pm v=1.76m/s d=35pm 0.05 0.10 0.15 0.20 X (m) Figure 8.20 Comparison of the wet experimental data and the theoretical prediction when the drawing speed is 1.76 m/s 138 1200 0 d=30pm, no spray * d=30p1m, spray starts @ x=0.03m A d=29pm, spray starts @ x=0.07m No spray numerical simulation 3 ------ spray x = 0.032 m with density 4436/cm 900- -- -- spray x = 0.078 m with density 4436/cm 3 %. E(D) 600I-A V = 2.64 m/s T1 = 25 "C 0.00 0.10 0.05 0.15 X (m) Figure 8.21 Comparison of the wet experimental data and the theoretical prediction when the drawing speed is 2.64 m/s 139 0.20 1200 * d=26.5pm, no spray A d=27.Opm, spray starts @ x=0.06 m d=25.Opm, spray starts @ x=0.00 m posray numerical simulation 3 ------ spray x = 0.073 m with density 4436/cm ------- spray x=0.000 m with density 4436/cm3 * 900 - (D L E 600 T., = 260C V=3.51 M/s 0.00 0.10 0.05 0.15 X (m) Figure 8.22 Comparison of the wet experimental data and the theoretical prediction when the drawing speed is 3.51 m/s 140 0.20 1200d=23.5pm, no spray d=22.Opm, spray starts @ x=0.02m d=24.Opm, spray starts @ x=0.05m No spray numerical simulation 3 spray x = 0.015 m with density 4436/cm -.-----3 S------ spray x = 0.052 m with density 4436/cm * * A -- 900 L.. 600- Ta= 260 C V=4.39 m/s -IIIII 0.00 300 - - 0.10 0.05 II 0.15 X (m) Figure 8.23 Comparison of the wet experimental data and the theoretical prediction when the drawing speed is 4.39 m/s 141 0.20 1200 M d=21.Opm, no spray d=20.0pm, spray starts @ x=0.023m A d=20.pm, spray starts @ x=0.043m srav pNo numerical simulation 3 spray x = 0.012 m wit h density 4436/cm * ------ spray x = 900 - 600 - 3 0.045 m wit h density 4436/cm 2' 60 cc E- Tair = 25 0C V=5.27 m/s 300 0.00 0.10 0.05 0.15 0.20 X (m) Figure 8.24 Comparison of the wet experimental data and the theoretical prediction when the drawing speed is 5.27 m/s From above figures, it is clear that the theoretical results predict the cooling effect of water spray reasonably well. It is also very clear that spray from different locations will affect the cooling rate differently. 142 8.4 Summary In this chapter, a theoretical model based on the von Karman-Pohlausen boundary layer integral technique was built. The numerical simulation results, which contain our experimental parameters, were compared to the experimental data from both the no water spray cases and water cooled cases. It is shown that the prediction is close to our data, but has somewhat higher values compared to the experimental results. The potential reasons of the difference may be the vibratonal effect and a tendency for the model to underpredict that data. 143 144 Chapter 9 Conclusions We have following results from the present work: 1. A heated thermocouple technique was used in the experiments. The temperature profile of glass fiber under no water spray and water spray was obtained under various conditions. 2. The error analysis shows that without water spray the error is 14.8% and that with water spray, the error is 15.3%. The main error comes from the uncertainty of the thermocouple probe's reading. 3. The Karman-Pohlhausen technique was used in theoretical model to predict the temperature profile of the fiber. The comparison between the experimental data and the theoretical prediction shows that integral methods produce the correct trends, but that they show systematic disagreements with data. 4. The direction and magnitude of these disagreements are system dependent. Potential causes may include vibration effects, boundary layer transition, and uncertainties. Thus, future suggested work will be: 1) measure/model vibration effect; 2) decide the amplitudes/frequencies of the measurement vibration. 5. Spray models show similar levels of disagreement. More detailed knowledge of the spray dispersion in the fiber bundle air flow will be required for accurate modeling. 6. The effect of the thermal boundary layer under the bushing plate was analyzed by adapting the theoretical model. The results show an effect on 145 fiber temperature near the plate, but this effect doest not explain that disagreement of the data with the theory. 146 References: Chapter 1: 1.1 http://www.semboda.cor/glassfib/story.htm. 1.2 Glass fiber at PPG, Inc. URL: http://www.ppq.com/fgs main/reinforcernents.htm. 1.3 M. Sweetland and J.H. Lienhard V, 2000, Evaporative Cooling of Continuously Drawn Fibers by Water Sprays, Intemational Journal of Heat and Mass Transfer, vol.43, p.777. 1.4 K. L. Loewenstein, 1993, The Manufacturing Technology of Continuous Glass Fibers, 1.5 3 rd ed., Elsevier Science Publishers B. V., Amsterdam. Shereen Eletribi, 1999, Dispersion of Water Sprays in a Transverse Air jet and the Aging of Spray Nozzles, Master Thesis, Massachusetts Institute of Technology, Cambridge, Massachusetts. 1.6 M. Sweetland, 1998, Nozzle Analysis and Heat Transfer Model for Spray Cooling of Glass Fibers, Master Thesis, Massachusetts Institute of Technology, Cambridge, Massachusetts. 1.7 S. Bateson, 1958, Critical Study of the Optical and Mechanical Properties of Glass Fiber, Journal of Applied Physics, Vol.29, No.1, p.13. Chapter 2: 2.1 R. C. Progelhof and J. L. Throne, 1971, Comment on "Heat Transfer through the Axially Symmetric Boundary Layer on a Moving Circular Fiber", International Journal of Heat and Mass Transfer, Vol.14, p.2166. 2.2 Samuel N. Rea, 1975, "Rapid Method for Determining Concentric Cylinder Radiation View Factors", AIAA Journal, Vol.13, No.8, p.1122. 2.3 M. B. Glauert and M. J. Lighthill, 1955, The Axisymmetric Boundary Layer on a Long Thin Cylinder, Proceedings of Royal Society, Series A, p.188. 147 2.4 B. C. Sakiadis, 1961, Boundary-Layer Behavior on Continuous Solid Surfaces: 1. Boundary-Layer Equations for Two-Dimensional and Axisymmetric Flow, A.L.Ch.E. Joumal, Vol.7, No.1, p.26. 2.5 B. C. Sakiadis, 1961, Boundary-Layer Behavior on Continuous Solid Surfaces: 11. The Boundary Layer on a Continuous Flat Surface, A.l.Ch.E. Joumal, Vol.7, No.2, p.221. 2.6 B. C. Sakiadis, 1961, Boundary-Layer Behavior on Continuous Solid Surfaces: Ill. The Boundary Layer on a Continuous Cylindrical Surface, A.l.Ch.E. Joumal, Vol.7, No.3, p.467 2.7 L. R. Glicksman, 1968, The Cooling of Glass Fibres, Glass Technology, Vol.9, No.5, p.131. 2.8 D. E. Bourne and D. G. Elliston, 1970, Heat Transfer through the Axially Symmetric Boundary Layer on a Moving Circular Fibre, Intemational Joumal of Heat and Mass Transfer, Vol.13, p.583. 2.9 D. E. Boerne and H. Dixon, 1971, The Cooling of Fibres in the Formation Process, International Joumal of Heat and Mass Transfer, Vol.24, p.1323. 2.10 R. E. Sayles, 1984, A Local Similarity Solution for the Viscous Boundary Layer Flow Longitudinal to a Cylinder, AIAA Journal, Vol.22, p.717. 2.11 R. E. Sayles, 1990, Approximate Solution for the Viscous Boundary layer on a Continuous Cylinder, AIAA Joumal, Vol.36, No.12, p.1917. 2.12 C. Moore and J. R. A. Pearson, 1975, Experimental Investigation into an Isothermal Spinning Threadline: Extensional Rheology of a Separan AP 30 Solution inn Zglycerol and Water, Rheologica Acta, Vol.14, No.5, p.153. 2.13 E. Beese and K. Gersten, 1979, Skin Friction and Heat Transfer on a Circular Cylinder Moving in a Fluid at Rest, Joumal of Applied mathematics and Physics, Vol.30, p.117. 2.14 S. Kase and T. Matsuo, 1965, Theoretical Analysis of Melting Spinning, Joumal of Text. Mach. Society of Japan, Vol.18, No.3, p.188. 2.15 S. Kase and T. Matsuo, 1965, Studies on Melt Spinning. I. Fundamental Equation on the Dynamics of Melting Spinning, Joumal of Polymer Science, Part A, Vol.3, p.2541. 148 2.16 G. J. Morris, J. L. Loth, and R. E. Bond, 1997, Cooling Rate of a Filament, Final Contract Report to PPG Industries, Inc. 2.17 G. J. Morris, J. L. Loth, R. E. Bond and A. J. Cragg, 1999, Cooling Rate of a Drawn Glass Filament, Final Contract Report to PPG Industries, Inc. 2.18 E. Richelle, R. Tasse and M. L. Riethmuller, 1995, Momentum and Thermal Boundary Layer along a Slender Cylinder in Axial Flow, Intemational Journal of Heat and Fluid Flow, Vol.16, No.2, p.99. 2.19 E. E. Maebius, 1985, The Effects of Heat Transfer in Melt Spinning, Journal of Applied Polymer Science, Vol.30, p.1639. 2.20 H. Papamichael and I. N. Miaoulis, 1991, Thermal Behaviour of Optical Fibers during the Cooling Stage of the Drawing Process, Joumal of Material Research, Vol.6, p.159. 2.21 H. Papamichael and I. N. Miaoulis, 1991, Axial Heat Conduction Effects in the Cooling of Optical Fibres, Glass Technology, Vol.32, No.3, p.102. 2.22 H. Papamichael and I. N. Miaoulis, 1992, The Cooling of Optical Fibres during the Drawing Process, Glass Technology, Vol.33, No.4, p.136 2.23 B. H. Kang, J. Yoo and Y. Jaluria, 1994, Experimental Study of the Convective Cooling of a Heated Continuously Moving Material, Journal of Heat Transfer, Vol.116, p.199. 2.24 S. R. Choudhury and Y. Jaluria, 1994, Forced Convective Heat Transfer from a Continuously Moving Heated Cylindrical Rod in Materials Processing, Journal of Heat Transfer, Vol.116, p.724. 2.25 S. H. -K. Lee and Y. Jaluria, 1996, Effects of Variable Properties and Viscous Dissipation during Optical Fiber Drawing, Journal of Heat Transfer, Vol.118, p.350. 2.26 J. V. Anderson, J. B. Caress and R. L. Sager, 1968, The Cooling Rate of a Glass Fiber in the Continuous Filament Process, Laboratory Report No. L.R.235 of Pilkington Bros. Ltd., Lathom, Lancashire. 2.27 R. G. C. Arridge and K. Prior, 1964, Cooling Time of Silica Fibers, Nature, Vol.203, p.386. 149 2.28 L. Anderson, 1958, Cooling Time of the Strong Glass Fibers, Journal of Applied Physics, Vol.29, No.1, p.9. 2.29 R. Maddison and P. W. McMillan, 1978, Cooling Rates of Glass Fibers, Glass Technology, Vol.19, No.5, p.127. 2.30 M. Sweetland and J.H. Lienhard V, 2000, Evaporative Cooling of Continuously Drawn Fibers by Water Sprays, International Journal of Heat and Mass Transfer, vol.43, p.777. 2.31 S. Eletribi, 1999, Dispersion of Water Sprays in a Transverse Air Jet and the Aging of Spray Nozzles, S. M. Thesis, Massachusetts Institute of Technology, Cambridge, Massachusetts. Chapter 3: 3.1 R. G. C. Arridge and K. Prior, 1964, Cooling Time of Silica Fibers, Nature, Vol.203, p.386. 3.2 R. Maddison and P. W. McMillan, 1978, Cooling Rates of Glass Fibers, Glass Technology, Vol.19, No.5, p.127. 3.3 M. Sweetland, 1998, Nozzle Analysis and Heat Transfer Model for Spray Cooling Glass Fibers, S. M. Thesis, Massachusetts Institute of Technology, Cambridge, Massachusetts. 3.4 S. Kase and T. Matsuo, 1965, Theoretical Analysis of Melting Spinning, Journal of Text. Mach. Society of Japan, Vol.18, No.3, p.188. 3.5 S. Kase and T. Matsuo, 1965, Studies on Melt Spinning. I. Fundamental Equation on the Dynamics of Melting Spinning, Journal of Polymer Science, Part A, Vol.3, p.2541. 3.6 J. R. Pearson and M. A. Matovich, 1969, Spinning a Molten Threadline, Stability, I & EC Fundamentals, Vol.8, No.4, p.605. 3.7 J. R. Perason and Y. T Shah, 1972, Stability Analysis of the Fiber Spinning Process, Transaction of the Society of Rheology, Vol.16, No.3, p.519. 3.8 Y. T. Shah and J. R. Pearson, 1973, Stability of Non-isothermal Flow in Channels, Part I - Temperature Dependent Power-Law Fluids without 150 Heat Generation, University of Cambridge Polymer Processing Research 3.9 Center Report, Cambridge, England. J. R. Pearson and Y. T. Shah, 1973, On the Stability of Isothermal and Non-Isothermal Fiber Spinning of Power-Law Fluids, Imperial College Polymer Processing Group Report, Cambridge, England. 3.10 Y. T. Shah and J. R. Pearson, 1973, Stability of Non-Isothermal Flow in Channels, Part /// - Temperature-Dependent Power-Law Fluids with Heat Generation, University of Cambridge Polymer Processing Research Centre Report, Cambridge, England. 3.11 R. Anantanaratanan and A. Ramachandran, 1958, Effect of Vibration on Heat Transfer from a Wire to Air in Parallel Flow, ASME Journal of Heat Transfer, Vol.80, p.1426. 3.12 F. K. Deaver, W. R. Penney and T. B. Jefferson, 1962, Heat Transfer From an Oscillating Horizontal Wire to Water, ASME Journal of Heat Transfer, Vol.84, p.251. 3.13 P. D. Richardson, 1967, Effect of Sound and Vibration on Heat Transfer, Applied Mechanics Reviews, Vol.20, No.3, p.201. 3.14 J. M. Faircolth, JR. and W. J. Schaetzle, 1969, Effect of Vibration on Heat Transfer for Flow Normal to a Cylinder, ASME Journal of Heat Transfer, Vol.91, p.140. 3.15 B. H. Thrasher and W. J. Schaetzle, 1970, Instantaneous measurement of Heat Transfer from an Oscillating Wire in Free Convection, ASME Journal of Heat Transfer, Vol. 92, p.439. 3.16 B. F. Armaly and D. H. Mansen, 1971, Heat Transfer from an Oscillating Horizontal Wire, ASME Journal of Heat Transfer, Vol.93, p.239. 3.17 U. C. Saxena and A. D. K. Laird, 1978, Heat Transfer from a Cylinder Oscillating in a Cross-Flow, ASME Journal of Heat Transfer, Vol.100, p.684. 3.18 K. D. Murphy and T. A. Lambert, JR., 2000, Modal Effects on the Local Heat Transfer Characteristics of a Vibrating Body, ASME Journal of Heat Transfer, Vol.122, p. 2 3 3 . 151 3.19 B. C. Sakiadis, 1961, Boundary-Layer Behavior on Continuous Solid Surfaces: Ill. The Boundary Layer on a Continuous Cylindrical Surface, A.I.Ch.E Joumal, Vol.7, No.3, p. 4 6 7 3.20 L. R. Glicksman, 1968, The Cooling of Glass Fibres, Glass Technology, Vol.9, No.5, p.131. 3.21 P. G. Simpkins and P. A. Blythe, 1997, Laws for Fiber Temperature Prediction during Drawing, Joumal of Heat Transfer, Vol.199, p.652. 3.22 N. Sasaki, 1950, A New Method for Surface-Temperature Measurement, The Review of Scientific Instruments, Vol.21, No.1, p.1. 3.23 N. Sasaki and A. Kamada, 1952, A Recording Device for Surface Temperature Measurements, The Review of Scientific Instruments, Vol.23, No.6, p.261. 3.24 M. F. Culpin and D. M. Jones, 1959, Measurement of the Temperature of 28 a Running Threadline, Joumal of Scientific Instruments, Vol.36, p. . Chapter 4: 4.1 C. R. Ansbergs, 1999, Optimization of the Glass Fiber Forming Process for Single-Tip and Small-Number-Tip Position, Master Thesis, Massachusetts Institute of Technology, Cambridge, Massachusetts. 4.2 B. M. McKeone, 1999, Measurement of Air Temperature and Velocities in the Fiber Glass Forming Environment, Master Thesis, Massachusetts Institute of Technology, Cambridge, Massachusetts. 4.3 John Lienhard IV and John Lienhard V, 2001, A Heat Transfer Textbook, 3 rd Edition, Phlogiston Press, Cambridge Massachusetts. Chapter 5: 5.1 D. E. Bourne and D. R. Davis, 1958, Heat Transfer through the laminar boundary layer on a circular cylinder in axial incompressible flow, Quarterly Journal of Mechanics and Applied Mathematics, Vol. Xl, part 1, 1958. 152 5.2 L. R. Glicksman, 1968, The Cooling of Glass Fibres, Glass Technology, Vol.9, No.5, p. 1 3 1 . Chapter 6 6.1 M. Sweetland, 1998, Nozzle Analysis and Heat Transfer Model for Spray Cooling of Glass Fibers, Master Thesis, Massachusetts Institute of Technology, Cambridge, Massachusetts. 6.2 A. F. Mills, 1995, Heat and Mass Transfer, R. D. Iwrin, Chicogo. Chapter 7 7.1 T. G. Beckwith, R. D. Marangoni and J. H. Lienhard V, 1993, Mechanical Measurements, 5 th edition, Addison-Wesley Publishing Company, Reading Massachusetts. 7.2 Narottam P. Bansal, 1986, Handbook of Glass Properties, Academic Press, Orlando. 7.3 A. F. Mills, 1995, Heat and Mass Transfer, R. D. Iwrin, Chicogo. Chapter 8 8.1 D. E. Bourne and H. Dixon, 1971, The Cooling of Fibres in the Formation 1 Process, International Journal of Heat and Mass Transfer, Vol.24, p. 323. 8.2 M. Sweetland, 1998, Nozzle Analysis and Heat Transfer Model for Spray Cooling of Glass Fibers, Master Thesis, Massachusetts Institute of Technology, Cambridge, Massachusetts. 8.3 B. C. Sakiadis, 1961, Boundary-Layer Behavior on Continuous Solid Surfaces: Ill. The Boundary Layer on a Continuous Cylindrical Surface, A.I.Ch.E. Journal, Vol.7, No.3, p.467 8.4 M. B. Glauert and M. J. Lighthill, 1955, The Axisymmetric Boundary Layer on a Long Thin Cylinder, Proceedings of Royal Society, Series A, p.188. 153 8.5 B. C. Sakiadis, 1961, Boundary-Layer Behavior on Continuous Solid Surfaces: 1. Boundary-Layer Equations for Two-Dimensional and Axisymmetric Flow, A.l.Ch.E. Journal, Vol.7, No.1, p.26. 8.6 D. W. Hatfield and D. K. Edwards, 1981, Edge and Aspect Ratio Effects on Natural Convection from the Horizontal Heated Plate Facing Downwards, Intemational Joumal of Heat and Mass Transfer, Vol.24, No.6, p. 1019. 8.7 A. F. Mills, 1995, Heat and Mass Transfer, R. D. lwrin, Chicogo. 154