+ Improved tower models SCDS Tower + Quick cost estimates Tower cost, installed = $40,000 + + Convert reboiler and condenser duties to costs Short-cut distillation in black R 1 2 4 5 15 Tower #1 design in red kJ/kg-K kJ/kg 4.187 2270 latent heat Cp, water of steam condenser duty,, reboiler kJ/h duty,CW, kJ/hkg/h Cw, m 3 /h CW cost, $/h steam, kg/h steam, lb/h utilities, $/yr -2.43E+06 2.46E+06 29018 29 $0.58 1.08E+03 $15.71 $130,352 -3.34E+06 3.96E+06 39885 40 $0.80 1.74E+03 $25.30 $208,743 -6.54E+06 7.16E+06 78099 78 $1.56 3.15E+03 $45.74 $378,381 -8.06E+06 8.68E+06 96250 96 $1.93 3.82E+03 $55.44 $458,960 -2.15E+07 2.21E+07 256747 257 $5.13 9.74E+03 $141.17 $1,170,419 Suggested recycle range The tower is inexpensive relative to the operating costs. + Two choices for detailed column design + SCDS: non-ideal K-value chemical systems in distillation, absorption, strippers,… 2 or 3 phase systems + TOWR Note: one of the least likely control methods in the field is to use mole fraction. Have you ever used a mole fraction meter? Rather, a number of variables that are easy to measure and control are the actual choices. These can be set in ChemCad, linking the solution to the control methodology. We will not address this feature in this course. + It is easy to build the TOWR model on the same pdf as the shortcut column. This eases comparisons of the results. The two sheets are separable later. + TOWR #1 Set-up for the MeOH/2-PrOH problem Select TOWR #1 from the ChemCad 5 list + Problem design basis table Set column bottoms to 20% MeOH 10 actual stages @ 48% efficiency gives 5 theoretical stages VLE from NRTL F = 50:50 molar mixture of MeOH, 2PrOH R = {5, 7, 10, 12, 15} Reboiler power = {0.5 kW to 1.75 kW} Feed tray @ 8 or 5; 30 mL/min feed + Format – engineering units + Thermophysical properties + Stream 1 - feed + TOWR#1 - General + TOWR#1 – specifications long list of possible specifications + TOWR#1 - convergence + TOWR#1 – cost estimate Please choose sieve tray instead + Report/Stream compositions/all streams + Plot/Unit ops/Column profile + Column profile Feed on stage 6 + Size/Distillation/Trays + Sieve tray + Tray 2 + Tray 6 + Tray 9 + Design starts Sensitivity analysis - feed tray location – let’s find an optimum location based on reboiler and condenser duties… … it is time to exercise the little gray cells… Sensitivity analysis Evaluate feed location from trays 2 to 9 Record reboiler duty, condenser duty, and reflux ratio Run TOWR#1 at feed stage = 2 prior to running the sensitivity analysis (gives a better chance for a clean run) + Feed @ tray 2 – note the discontinuity in temperature profile + Run/sensitivity study/feed loc/ adjusting + recording + Run/sensitivity/Plot results