Honors Chemistry Lab 2: OBSERVING AND INFERRING Name PURPOSE To practice making accurate and complete observations of physical and chemical processes and to learn how to formulate hypotheses that account for these observations. We continually use our senses to make observations about our environment. Below is a list of sensory words that are helpful when describing what are observing: Sight words billowing blazing blochy blurred bright brilliant clear Shapes Curved Cylindrical Domed Touch words Cold Cool Damp Dry dim faded faint filmy fluorescent glistening glittering Flat Globular Hollow Elastic Fuzzy Hot Icy Irregular Lumpy Spindly Oily Rough Rubbery Sandy glittery glossy glowing grimy hazy indistinct Luminous Split Square Straight Sharp Silky Slippery Smooth misty opalescent opaque shadowy shimmering shiny smudged Tapering Thin Tubular Soft Spongy Sticky Warm sparkling streaked striped tarnished translucent Wavy Wide Waxy Wet INTRODUCTION Observations, followed by development of hypothesis, are often the first steps in a scientific method. Experiments are then designed and carried out to test these hypotheses under controlled conditions. If the results of the initial experiment support the hypothesis, additional testing is done to further test the hypothesis. If, however, the experimental results do not support the original hypothesis, then the hypothesis must be changed or modified. When the results of many, many, experiments support a hypothesis, it may become a theory. A theory is a well-tested explanation for a broad set of observations. In this lab you will perform a series of experiments, and you will make and record observations. You will then formulate hypotheses to explain your observations. TERMS: Observation an act or instance of noticing or perceiving. an act or instance of regarding attentively or watching. the faculty or habit of observing or noticing. an act or instance of viewing or noting a fact or occurrence for some scientific or other special purpose: the observation of blood pressure under stress. Inference the process of deriving the strict logical consequences of assumed premises. the process of arriving at some conclusion that, though it is not logically derivable from the assumed premises, possesses some degree of probability relative to the premises. a proposition reached by a process of inference. Hypothesis If …., then …. Statement a proposition, or set of propositions, set forth as an explanation for the occurrence of some specified group of phenomena, either asserted merely as a provisional conjecture to guide investigation (working hypothesis) or accepted as highly probable in the light of established facts. a proposition assumed as a premise in an argument. a mere assumption or guess. Theory a coherent group of tested general propositions, commonly regarded as correct, that can be used as principles of explanation and prediction for a class of phenomena: Einstein's theory of relativity. a proposed explanation whose status is still conjectural and subject to experimentation, in contrast to wellestablished propositions that are regarded as reporting matters of actual fact. MATERIALS PartI Insulated gloves Safety goggles Lab apron Crucible tongs 100/150, 250-mL beakers 100-mL graduated cylinder 2 watch glasses 1 large/1 small test tube stirring rod Plastic wash bottle 0.1 M Silver nitrate – AgNO3 0.1 M Sodium hydroxide NaOH 3% Hydrogen peroxide calcium acetate Ca(C2H3O2)2 Copper wire Cornstarch Wood splints 1 L graduated cylinder Pipet Ice, H2O Dry ice, CO2 Manganese (IV) oxide, MnO2 Universal indicator solution Distilled water, H2O Metal spoon Distilled H2O SAFETY Wear safety goggles, nitrile gloves, closed-toed shoes and a lab apron at all times in the laboratory. No food or drink is allowed in the laboratory at any time. Do not touch the dry ice with your bare hands. It can cause frostbite. Use insulated gloves or tongs. Avoid contact with silver nitrate solution. It can cause temporary skin discoloration and skin burns. Ethanol is flammable PROCEDURE ***NOTE: RECORD DETAILED OBSERVATIONS IN THE DATA TABLE*** Make at least 4 observations for all steps 1. Place the piece of copper wire into the small test tube. Cover the copper wire with the silver nitrate solution. Place the test tube into a 50 ml beaker so it doesn’t fall over. Observe this system every 5 minutes during the class period, and record your observations. When finished place waste in container waste Silver nitrate. 2. Place a piece of ice and a piece of dry ice on separate watch glasses. Observe what happens with time. 3. Fill a plastic wash bottle half-way, with distilled water. Obtain several small pieces of dry ice from the teacher. Once you are standing at your lab table, replace the jet assembly of the wash bottle and tighten. NOTE: Direct the jet assembly toward the sink only. Record your observations. 4. Add about 20 drops of universal indicator solution to 750 ml of distilled water in a 1-L graduated cylinder. Record what happens when 100 ml of sodium hydroxide solution is added and the mixture is stirred. Observe what occurs when several small pieces of dry ice are added. 5. Add 1 gram of copper I chloride to a test tube and add 10 ml of water. Stir, then touch the bottom of the test tube. 6. At the hood, observe the 3 baggies and 3 test tubes with cornstarch water mixtures were prepared by the teacher . Each contains 3.00g of cornstarch. Baggie/test tube 1 has 5 ml of water, baggie/test tube 2 has 7 ml of water, and /test tube 3 has 10 ml of water. Observe what happens when each mixture is stirred either by gently messaging the baggie or by mixing with a stirring rod in the test tube. Also note what each mixture looks line when some of each mixture is picked up with the rod. 7. Add 5 mL of 3% hydrogen peroxide solution to a large test tube (in your lab drawer). Light a wooden splint and gently blow it out so that it is glowing. Add a small amount (pea size) of manganese (IV) oxide powder to the test tube containing the 3% hydrogen peroxide. Observe what happens when you insert the glowing splint into the upper part of the test tube. 8. Observe what happens when 25 ml of calcium ethanoate solution is poured into a100ml beaker containing 25ml of ethanol. Pre-lab: Read lab and enter it into your lab notebook with the proper format and include a data table to collect your observations Post lab ANALYSIS/CONCLUSIONS 1. For each reaction, write 1 hypothesis that could explain the behavior that you observed. 2. What is the difference between physical and chemical changes? 3. How do you know that a chemical reaction took place? Give at least 4 examples. 4. Classify the following as a physical or chemical change: 1. glass breaking 10. Melting ice cream 2. hammering wood together to build a house 11. fireworks exploding 3. a rusting bicycle 12. squeezing oranges to make orange juice 4. melting butter for popcorn 13. frying an egg 5. separating sand from gravel 14. pouring milk on your oatmeal 6. spoiling food 15. burning leaves 7. Freezing chocolate covered bananas 16. making salt water to gargle with 8. 17. cream being whipped the lawn 9. corroding metals 18. burning toast DATA/OBSERVATIONS SYSTEM/STEP OBSERVATIONS (IT’S ALL ABOUT THE OBSERVATIONS – BE VERY DETAILED!) COPPER/SILVER 1. NITRATE 2. STEP 1 3. 4. ICE/DRY ICE STEP 2 1. 2. 3. 4. DRY ICE/WASH BOTTLE 1. STEP 3 3. 2. 4. H2O/UNIVERSAL 1. INDICATOR/NaOH 2. / DRY ICE 3. STEP 4 4. Copper Ii chloride and water 1. Step 5 3. 2. 4. Cornstarch 5ml/7ml/10ml wate 1. 2. 3. STEP 6 MnO2/H2O2 STEP 7 4. 1. 2. 3. 4. Calcium ethonate Step 8 1. 2. 3. 4. Honors Chemistry name______________________________________ period____________ Lab 2: OBSERVING AND INFERRING RUBRIC – 70 points _____ 1. Lab entered in to table of contents (1 pt) _____2. Lab entered properly in lab notebook(title, page number, objective, materials, procedure – 5 pts) _____3. Lab completed by the student in the lab within one week of the lab day assigned (12 points) _____4. Data Table drawn neatly with a straight edge or neatly cut and taped into lab book (1 pt) _____5. Data Table completely filled out with 4 observations for steps 1-8 (16 pts) _____6. All questions answered in complete sentences (2 points) _____7. Post lab question 1. A hypothesis for each step that could explain the behavior you observed in step in each step (16 pts) _____8.Post lab question 2 (4 points) _____9. Post lab question 3 (2 points) _____10. Post lab question 4. (9 points) ____11.. Lab station and lab notebook clean and neat(2 pts)