Chemistry 2145 Organic Chemistry I Tulsa Community College, Southeast Campus Fall Semester, 2013 Call No. 12771 Section 301 Call No. 12775 Section 302 T 8:00-8:50 a.m. Room SE8214 Lab T 9:30-10:50 a.m. Room SE8214 Lab TR 11:00-12:20 p.m. Room SE8279 R 8:00-8:50 a.m. Room SE8214 Lab R 9:00-10:50 a.m. Room SE8214 Lab TR 11:00-12:20 p.m. Room SE8279 Email: Jonathan.Frazee@tulsacc.edu Wayne Frazee, Assistant Professor Office: SEC 8267 Phone Number: 918-595-7682 OFFICE HOURS M&W: 7:25-9:25 am T&TH: 7:25-7:55 am Friday: 7:25-10:55 am T & W: 5:30-6:15 pm (On-Line) Office Hours: All meetings are by appointment only. Email to confirm meeting location and time. SCIENCE AND MATHEMATICS DIVISION Associate Dean: Lyn B. Kent Office: SEC 8125 Phone Number: 918-595-7742 TEXTBOOKS AND SUPPLEMENTAL MATERIALS 1) Organic Chemistry, 11th edition, 2014, T.W. Graham Solomons, John Wiley & Sons - Pub. 2) Organic Chemistry Lab Manual, Miller & Briscoe, 2012 3) Safety Goggles and Lab Coat or Apron: 4) Optional Materials: a) Molecular Model Set for Organic Chemistry, Molymod, Printice Hall b) Organic Chemistry Nomenclature Study Cards, Vis-Ed EVALUATION TECHNIQUES 1) Examinations – 500 points total: a) Lecture exams – 500 points total i) 4 exams: 100 points each – questions types will be multiple choice, short answer, essay or problem solving. These exams will cover assigned lecture materials, problem sets, and laboratory experiments. ii) The lowest exam score may be dropped and replaced with the final, so the final would count twice, provided that the final exam score is of a higher value. The final exam score cannot be changed even if it is your lowest score, only the chapter exams may be replaced. The final exam will not replace a missed exam. iii) Lecture Final exam – 100 points, 110 minutes: Common Final exam “Organic Chemistry”, a comprehensive exam. 1 2) Laboratory reports – 240 points total: a) Laboratory Experiments and Reports – 240 points total i) There will be 10 experiments worth 20 points each and 2 multi-step experiments worth 30 points each. The lowest lab score will be dropped and the best 11 lab scores will counted. However, the multi-step experiments cannot be dropped. ii) Students must wear goggles and a lab apron during labs. If a student does not have the appropriate safety equipment available, the student will not be allowed to participate in the laboratory and will forfeit all points associated with that experiment. 3) Evaluation points a) Total points possible = 740 GRADING SCALE Student % 89.5 – 100 79.5 – 89.4 69.5 – 79.4 59.5 – 69.4 0 – 59.4 Student’s grade A B C D F LATE ASSIGNMENT AND MAKE-UP EXAM POLICY 1) Missed Exams a) NO make-up exams will be given. In the case of an EXTREME emergency and notification prior to the exam (24 HOURS) by telephone, the next assigned exam will be doubled to account for a missed exam. It is at the sole discretion of the instructor to determine whether the emergency is extreme (i.e., those which are utterly beyond the control of the student) and whether the next exam will count in place of the missed exam. Vacations, family outings, trips, etc. are NOT unavoidable extreme circumstances! Approval for a missed exam will NEVER be given in such cases! Approval for the next exam to be counted twice must be requested before the exam begins. Approval will NOT be granted for requests made after the exam has been administered! Some form of documentation which validates the need for a missed exam will normally be required. If an exam is missed due to illness, you will be required to present a “doctor’s note” stating that it was not possible for you to attend class on the day of the exam before a make-up exam will be approved. Financial hardship is not an excuse for lacking a “doctor’s note” as there is a campus nurse that can be seen free-of-charge through Student Health Services. No doctor’s note equals no points for missed exam! 2 b) The TCC common Final for Organic II Chemistry Students can not be made up without prior arrangements with me. Missing these exams without prior arrangements will result in a zero (0) for the missed exam. 2) Missed Laboratory a. Laboratory work will be completed during specified lab period. b. Experiments cannot be made up, NO Exceptions. c. An absence during a lab period will result in “0” for that lab. 3) Late Laboratory Reports A. The completed report is due at the start of the following lab period. One minute after the lab period begins is considered late and will not be accepted. B. Late reports will not be accepted. If you have an excused absence when the report is due, hand in next class period with a 25 percent deduction. An excused absence is up to the sole discretion of the instructor. ATTENDANCE It is essential that students attend all classes. All lecture and laboratory material must be read prior to class lectures. Attendance will be taken during each lecture and lab sections. INSTITUTIONAL STATEMENT Each student is responsible for being aware of the information contained in the TCC Catalog, TCC Student Code of Conduct Policy Handbook, and semester information listed in the Class Schedule. CLASSROOM ETIQUETTE: Open and mutually respectful communication of varied opinions, beliefs, and perspectives during classroom or online discussion encourages the free exchange of ideas that is essential to higher learning and to the ability to learn from each other. Use of any electronic device is at the discretion of the instructor. Cell phones are to be turned to vibrate before class begins. If a cell phone rings or a student is found using a cell phone during class, you will be asked to leave. If a cell phone rings during a test, you will be asked to hand in your test and leave. Laptop use is a privilege and will be revoked if students are caught using a laptop for tasks other than taking notes or completing homework assignments. iPods are to be turned off during class and cannot be used during a test. Classroom conduct that is not conducive to the learning environment will be dealt with on an individual basis and may involve removal of students from the learning environment for the remainder of the class period or semester. To be clear in what constitutes misconduct and unacceptable behaviors in the classroom, a list has been complied. Note: The following list is not all inclusive. Repeatedly interrupting an instructor while he/she is lecturing or conversing with another student without first raising one’s hand and waiting until called upon. Asking questions not pertinent to the topic of discussion. Causing classroom disruptions by o walking out of the classroom abruptly or leaving the classroom multiple times o repeatedly talking during lecture o using an inappropriately raised voice o tardiness o distracting classmates 3 o using approved electronic media in a manner not relevant to the lecture/lab Displaying a lack of respect or courtesy to faculty or classmates through derogatory language, threatening or offensive words or behavior, or unwanted invasion of personal space. Using a prohibited electronic device in the classroom. Working on material not related to this class. Refusing to follow directions from faculty. Intentional destruction of college property. Influencing or attempting to influence another person to violate these misconduct policies. Rude and/or disrespectful communication in class, lab, and emails. Be careful how you communicate in emails. Refrain from using exclamation points, inflammatory language, etc. At the college level, everyone enrolled in this course is considered an adult and as such you are expected to act accordingly. It is not my wish to have to remove anyone from the learning environment; however, if I feel any of the misconduct rules have been violated, you will be asked to leave the classroom for the remainder of the lecture/lab even during an exam or lab. For example, if you send a rude email before the exam, you will not be allowed in class and will miss the exam and will not be able to make it up. A meeting between the instructor and student will occur before you are allowed to enter the classroom again. If you violate the rules of misconduct a second time, you will be removed from the course permanently. As stated in the syllabus, AWs are not given. The removal from the course will result in a grade being assessed at the end of the semester according to your scores earned on all assignments from week 1 to week 16. Tuition paid for the class will not be refunded, and failure to complete the course may have a negative impact on current and future financial aid. I want each student to be successful in this class and avoid these negative consequences of any continued inappropriate classroom behavior. 1) Cheating is simply using any means to obtain information other than what is allowed. a) Exams i) Cheating on an exam is using any information that is not in the exam package. ii) Pre-programming a calculator with formulas and/or text material is not allowed. iii) Cheating will result in a 0 on the exam for all involved. b) Lab reports i) Each student must turn in their own report, written using their own words and their own calculations. ii) No Xerox copies iii) Cheating will result in a 0 on the lab report for all involved. c) Other i) Use of reference materials, such as the Internet, books, tutors, etc. is not cheating. In fact I encourage using these reference materials. 4 ii) Plagiarism is claiming, indicating, or implying that the ideas, sentences, or word of another writer are your own. Plagiarism will result in a score of 0 for each occurrence. LABORATORY SAFETY Students are to follow all guidelines listed on “Safe Rules of the Chemistry Laboratory” . COMMUNICATIONS: Email: All TCC students receive a designated TCC Outlook address (ex: john.doe@tulsacc.edu). All communications to you about TCC and course assignments will be sent to your TCC Outlook email address. You must use TCC Outlook email to send email to, and receive email from, the instructor regarding this course. Inclement Weather: TCC rarely closes. If extreme weather conditions or emergency situations arise, TCC always gives cancellation notices to radio and television stations. This information is also posted on the TCC website (www.tulsacc.edu). FAILURE TO WITHDRAW POLICY Failure to withdraw may result in the student receiving a regular grade of “F” at the end of the semester. Last day to change form credit to audit or last day to withdraw is Friday November 8, 2013. AW (Automatic Withdrawals) are not given in this course for failure to withdraw. ADA POLICY It is the policy and practice of Tulsa Community College to create inclusive learning environments. Accommodations for qualifying students in compliance with the Americans with Disabilities Act (ADA) and Section 504 of the Rehabilitation Act are available. To request accommodations, contact the Education Access Center (EAC) at eac@tulsacc.edu or call (918) 595-8685 or 7659 (Voice). Deaf and hard of hearing students may text (918) 809-1864. COURSE DESCRIPTION AND COURSE PREREQUISITE Organic Chemistry I is the first of two courses that cover the fundamental concepts of the chemistry of the compounds of carbon. See listings in the TCC catalog for other chemistry courses. This course has a pre-requisite of Chemistry II (CHE 1415) with a “C” or better. Organic Chemistry I is a study of the fundamental concepts of organic structure and bonding, reactions of principle functional groups, mechanisms, and nomenclature of hydrocarbons and their derivatives. Laboratory emphasis is on purification, separation, synthesis and instrumental methods of studying organic systems. Lecture 4 hours. Laboratory 2 hours. NEXT COURSE IN SEQUENCE Organic Chemistry I CHEM 2245 GENERAL EDUCATION GOAL STATEMENT The General Education Goals are designed to ensure that graduates of Tulsa Community College have the skills, knowledge, and attitudes to carry them successfully through their work and personal lives. The General Educational Goals that may be addressed in this course are: Critical thinking, Effective communication, Civic responsibility, Computer proficiency and Global awareness. 5 COURSE OBJECTIVES Chemistry is divided between theoretical and practical knowledge. This course will deal with the synthesis and reactions of the reactive functional groups. Reactions of functional groups include; halo-alkanes, alcohols, alkanes, alkenes, carboxylic acids and other compounds. The terminology and vocabulary used by the chemist will be developed and applied as well as qualitative techniques to solve Organic Chemistry problems. During the laboratory sessions the student will have the opportunity to perform laboratory procedures that correspond with the chapters covered during lecture. TEACHING METHODS This course will use lectures and laboratory experiments supplemented with multimedia material. Examinations, problem sets and written reports will be used to evaluate the student’s level of knowledge. COMPUTER SERVICES ACCEPTANCE USE Access to computing resources is a privilege granted to all TCC faculty, staff, and students. Use of TCC computing resources is limited to purposes related to the College’s mission of education, research, and community service. TOBACCO-FREE CAMPUS Tulsa Community College is a Tobacco-Free College in accordance with the Governor’s Executive Order 2012-01 and Title 63 of the Oklahoma Statutes, Section 1-1523 which prohibits smoking or the use of any tobacco products in all public places, in any indoor workplace, and all vehicles owned by the State of Oklahoma and all of its agencies and instrumentalities. This Order includes property leased, rented, or owned by TCC including, but not limited to, all grounds, buildings, facilities, and parking lots. Tulsa Community College’s policy includes a tobacco free environment on all campus and off-campus locations conducting TCC credit or noncredit classes. The TCC Campus Police is responsible for ensuring compliance with the Tobacco-Free Environment Policy. Violations of the policy may be addressed through issuance of campus or state citations. STUDENTS RESPONSIBILITY It is the responsibility of the student to read and follow this syllabus. REVISION POLICY I reserve the right to revise this syllabus and schedule to meet the ability, needs and the available time of the class. I will inform students of all changes verbally and/or in writing on Blackboard. 6 TENTATIVE SCHEDULE Week EXAMS LAB LECTURE 8/19 Safety Film & Check in Ch. 1 8/26 (1) Physical Property Measurements Ch. 1/2 9/02 (3) Partition Coefficients by Extraction Ch. 2/3 9/09 (4) Infrared Spectroscopy Ch. 3 (5) Isolation of Caffeine Ch. 4 9/23 (7) Open-Column Chromatography Ch. 4/5 9/30 (8) Polarimetry Ch. 5 10/07 (6) Sep. Acid, Base, & Organics Ch. 6 10/14 Exam II-Ch. 4&5 (6) Separtation Exp. Continued Ch. 7 10/21 (8) Synthesis of 1-Octanol Ch. 7 10/28 (10) Reaction of tert-pentyl Alcohol Ch. 8 11/04 (11) Dehydration of 2-Octanol Ch. 8 11/11 Exam III-Ch. 6&7 (13) Dehydrohalogenation Ch. 10 11/18 (13) Dehydrohalogentation continued Ch. 10/11 11/25 Thanksgiving No Laboratory this week Ch. 11 12/02 Exam IV- Ch. 8,10&11 (16) Williamson Ether Synthesis Ch. 11/12 12/9 Check Out Final Exam 9/16 Exam I-Ch. 1-3 7