The Confining Effect of End Roughness on Unconfined Compressive Strength Z. Szczepanik, D. Milne & C. Hawkes Department of Civil and Geological Engineering, University of Saskatchewan, Canada Proceedings of the 1st Canada-US Rock Mechanics Symposium, Vancouver, Canada, 2007, pp. 191-198. ABSTRACT: The influence of sample end effects on the unconfined compressive strength of rock core is well recognised. ASTM standards exist to ensure that minimum standards of sample smoothness are maintained to minimise the influence of friction between the samples ends and loading platens. Sample end preparation is also done to avoid stress concentrations on irregularities on the end surfaces. This paper describes tests that have been conducted on relatively uniform grey granite from northern Manitoba, Canada to investigate the influence of sample end effects. End conditions were varied by polishing the sample ends and by using loading platens with varying degrees of roughness. In one series of tests, lead foil was placed between the sample ends and the loading platens to further decrease frictional effects. In all tests, except the lead foil tests, procedures and sample preparations were conducted within the ASTM standards for unconfined compressive strength (UCS) testing. The test results presented show that sample “hourglassing”, as measured using circumferential strain gauges located near sample ends and at sample mid-points, resulted in strengths as low as 50% of the standard UCS values. Rougher sample ends and platens produced sample “barrelling” with strengths the same, or slightly higher than results from standard tests. These results suggest that standard UCS tests are conducted with a significant degree of effective sample confinement generated by sample end friction. 1 INTRODUCTION Research into factors influencing unconfined compressive strength (UCS) tests have been conducted at the University of Saskatchewan for over 10 years. Early testing was conducted to look at crack initiation and propagation in granitic samples (Eberhardt, 1998). Subsequent creep testing was conducted to determine if the strength of granitic samples was reduced under long term loads in excess of the theoretical strength, causing unstable crack growth (Sczcepanik et al., 2003). Based on the results of these tests, research is concentrating on the influence of sample end conditions on sample strength (Sczcepanik et al., 2005). Test results have shown a relationship between the ratio of circumferential strain at the sample mid point and sample ends versus the sample UCS, and that varying sample to platen contact friction can change the resulting sample UCS by up to about 100%. This paper presents the results of continued tests in this area. Modifications have been made to test procedures to try and vary sample end friction as much as possible. 2 SAMPLES AND PLATENS USED FOR THE TESTING PROGRAM 2.1 Sample Descriptions Samples of a medium-grained grey granite from northern Manitoba have been tested. The granitic rock was divided into two groups based on the P-wave velocity measured for each sample. The slower velocity samples ranged from 3161 metres per second (m/s) to 4373 m/s and the faster velocities were between 4496 m/s to 5134 m/s. Two groups of sample sizes were tested as well. The smaller samples were 35 mm in diameter and the larger samples had diameters of 61 mm. All tests had a length to diameter ratio between 2.0 and 2.5, which is within ASTM (1987) specifications. 2.2 Sample Instrumentation All samples were strain gauged. Circumferential strain gauges were mounted 10 mm from each sample end and at the sample midpoint. For the 35 mm diameter samples, both 14mm and 90 mm long strain gauges were used. For the samples instrumented with 14mm long gauges, 2 gauges were installed at each location and 2 axial strain gauges were also used. For the tests conducted with 90 mm long gauges, only 1 circumferential gauge was used at each location. For the 61 mm diameter tests, 90 mm long strain gauges were used with circumferential gauges 10 mm from each sample end and the sample midpoint. Two axial strain gauges were also used. Two gauges were used at each location to provide redundancy. 2.3 Surface Roughness Measurements Both sample end conditions and platen conditions were varied and a method of quantifying the surface conditions of the sample ends and platens was adopted. A portable surface roughness tester (profilometer) was used to measure sample end roughness to the nearest 0.01 μm. The roughness tester measured roughness along a 12.5 mm profile length. Average surface roughness, Ra, was recorded. Ra is calculated by first determining an average straight profile to represent the surface trace. The areas above and below the profile are calculated and added together. This total area is divided by the straight line profile length to determine the average profile roughness parameter Ra. To account for any directional anisotropy in the roughness of the sample ends, roughness was measured at 60° increments on the sample surface to produce a “roughness rosette”. An average roughness value for each sample end was obtained by averaging the roughness rosette values. Figure 1 shows how the Ra value is calculated. effects between the sample ends and platens and did not conform to ASTM standards. Three platen conditions were also used for testing. In all cases the steel platens had a hardness in excess of 58 (Hardness Rockwell C) HRC, as specified in the ASTM standards (1987). No effort was made to match the elastic properties of the rock and platens. Instead, the contact friction between the sample and platens was varied. Polished and striated platens were used, all of which conformed to ASTM standards. The polished platen was prepared on a thin section polishing wheel whereas the striated platen (Figure 2) was prepared on a fine grinding wheel. A third platen type was used that consisted of concentric grooves with a roughness in excess of ASTM standards. This platen is shown in Figure 3. The variation in platen types was used to vary sample to platen contact friction. The three types of sample end finish and three platen types that were used are summarized in Table 1, along with corresponding ranges in average roughness. The sample tested using lead foil are also listed in this table. The thickness of these foils were 0.015 mm, 0.03 mm, or in three cases, 1 mm. Profile length Figure 2. Striated platen showing scratch marks. Scale bar shows 1 cm j a b Roughness average (Ra) c d e f g h Centreline i Ra k l m n o p ya yb yc yn n Figure 1: Average roughness, Ra. (after Hebert, 2004) 2.4 Platen and Sample End Preparation Three sample groups were prepared with rough, standard and polished end conditions. All of these sample end conditions were within ASTM standards (ASTM, 1987). An additional suite of samples was tested with lead foil placed between the platens and the rock surface. This was done to reduce frictional Figure 3. Rough platen showing concentric grooves. Scale bar shows 1 cm Table 1. Platen types and sample end finishes used in laboratory UCS tests Platen type / Sample end finish Polished platens Smooth / striated platens Concentric grooved platens Rough sample end condition Standard / smooth sample end condition Polished sample end condition Average Roughness 0.17 μm<Ra<0.21 μm 0.8 μm<Ra<1.0 μm 4.0 μm <Ra<4.6 μm 3.8 μm <Ra< 4.3 μm 2.4 μm <Ra< 3.0 μm 0.6 μm <Ra< 1.2 μm 3 TEST RESULTS ASTM testing procedures were followed for sample testing unless otherwise stated. The sample loading rate was kept constant at 8.1 MPa per minute, which failed the samples in the ASTM recommended time period of 5 to 15 minutes for all but the strongest test results. Load and strain values were continuously recorded. After each test, the sample strains at 50% of the sample UCS were assessed. The ratio of the circumferential strain at the sample mid-point to the average circumferential strain at the sample ends was calculated. The smallest value for this ratio represents the sample end that experienced the greatest strain, which is interpreted as the end with the minimum surface to platen confining friction. Table 2 summarizes the ratios of minimum midpoint strain to average end-point strain measured at 50% of the sample UCS. It is interesting to note that the polished samples tested on the striated platens show the highest circumferential strain ratio, suggesting that the contacts between polished samples and striated platens experienced the highest friction. Rough samples tested on the grooved platens, however, show approximately 1-to-1 mid-point to endpoint circumferential strain ratios, indicating significantly less friction. It appears that the relatively rounded groove surfaces of the concentric grooved platens produce less rock-to-platen friction under loading than the polished or striated platens, even though these have much lower roughness (Ra) values. Additional tests were also conducted on the large samples with the lower compressional wave velocity. Brazilian tests were conducted, according to ASTM standards (ASTM, 1995), to obtain an estimate of the tensile strength of the rock. 8 samples were tested and gave an average tensile strength of 12.1 MPa, with a standard deviation of 1.0 MPa. 4 TEST INTERPRETATION The frictional bond between the loading platens and sample ends is not well understood, however, the application of circumferential strain gauges at sam- ple ends and mid-point allows the frictional effect to be indirectly quantified. Figure 4 shows measured sample UCS versus the sample circumferential strain ratio. Four groups of test results are shown. Tests conducted with lead foil on the sample ends have been circled. The granite samples with the lower compressional wave velocities were expected to be weaker and in general a slightly lower strength is obtained for these samples at a given circumferential strain ratio (Figure 4). Tests with a mid-point to end-point circumferential strain ratio greater than 1.0 are deforming to a barrel shape, showing significant end friction. In this circumferential strain ratio range, relatively high sample strengths between 200 and 250 MPa were consistently measured. At circumferential strain ratios less than 1.0 the samples developed an hourglass shape, signifying reduced end friction. Sample strengths in this circumferential strain ratio range show a distinct trend of reduced strength with increased hourglassing. Strengths range from just over 200 MPa to under 100MPa. Of the 16 samples that show some degree of hourglassing, 8 were tested with lead foil, 7 were tested with polished ends and polished platens, and one was tested with polished platens and standard smooth ends. It is interesting to note that the smooth striated platens produced some of the highest sample strengths and the largest degree of sample barrelling. The striated platen was finished on a fine grained aluminum oxide polishing wheel that left very shallow scratches on the platen surface. The scratched surface produced a low Ra roughness value of 0.8 to 1.0 μm, however, the scratched or striated surface produced an apparent high friction between the samples and platen. The failure mechanism, as well as strength, between hourglassing and barrelling samples appears to be different (Figures 5 and 6). Figure 7 shows the location of the circumferential strain gauges. Figure 5 shows a typical failed sample that deformed to a barrelled shape before failure. The sample ends were relatively intact after failure and a shear type failure developed in the sample. Figure 6 shows a typical failed sample that deformed to an hourglass shape before failure. Axial fracturing developed in the sample and the UCS was significantly lower than for the samples that deformed to a barrel shape prior to failure. The three test results for the lower velocity samples with the greatest degree of hourglassing before failure had circumferential strain ratios between 0.48 and 0.50 (Table 2) and an average UCS of 98 MPa (Figure 6). It is interesting to note that the average unconfined compressive strength for these three samples is 8.1 times the tensile strength. This is remarkably close to the theoretical 8:1 ratio between UCS and tensile strength predicted with Griffith’s crack theory (Griffith, 1924). Table 2. Minimum ratio of sample mid-point to end-point circumferential strain Circumferential strain ratio for rough sample ends Sample / platen description 61mm diameter samples: Concentric grooved platens Circumferential strain ratio for smooth / standard ends Circmferential strain ratio for polished sample ends 1.113 1.029 Smooth striated platens 1.449 1.847 1.778 Polished platens 1.802 1.111 0.822 0.482 lead foil 0.502 lead foil 0.489 lead foil 35mm diameter samples: Polished platens 1.065 1.12 1.063 0.799 0.743 0.838 0.862 0.845 0.505 0.908* 0.837* 1.409* 0.637 lead foil* 0.818 lead foil 0.524 lead foil 1.552 lead foil 0.790 lead foil * One sample end strain gauge failed for these tests – the remaining sample mid to end circumferential strain ratio is shown 300 Sample Barrelling Sample Hourglassing 250 UCS (MPa) 200 Samples Tested with Lead Foil 150 100 High Velocity Small Samples High Velocity Small Samples - 1 End Gauged Low Velocity Large Samples High Velocity Large Samples 50 0 0 0.5 1 1.5 2 Strain Ratio Figure 4. Sample UCS versus the minimum mid-point to end-point circumferential strain ratio. Figure 5. Post-failure photograph of a sample that showed relatively high strength with pronounced sample barrelling before failure. Circumferential Gauges Figure 6. Post-failure photograph of a sample that showed relatively low strength with sample hourglassing before failure. Strain Figure 7. Strain gauged sample showing circumferential gauge locations. 5 CONCLUSIONS Testing has been conducted on relatively uniform medium grained granitic rocks. The samples tested were divided into two groups based on compressional wave velocity, and the lower velocity samples appeared to have a slightly lower strength. Circumferential strain gauges applied at centre of the sample and 10 mm from the each sample end provided an indirect measure of the friction end confinement due to the contact between the platens and the rock. Sample hourglassing resulted in sample strength dropping to less than 50% of the maximum UCS values obtained. In half the cases of sample hourglassing, lead foil had been placed between the loading platens and the sample ends. Hawkes and Mellor (1970) reported similar testing procedures with the application of paper or Teflon between the loading platens and samples. It was reported that thicker layers, in excess of 0.5 mm, extruded under loading and the failed samples exhibited axial cleavage. It was thought that the axial cleavage was evidence that the material placed between the sample ends and platens was inducing a tensile stress at the samples ends and this approach was not recommended. The tests reported in this paper suggest that rock failure by axial cleavage can be obtained simply by reducing end friction during testing and that this can significantly influence the reported unconfined compressive strength of the rock. Additional testing is planned at the University of Saskatchewan to test other rock types and to better quantify sample end constraint and friction effects. REFERENCES ASTM D2938-86. 1987. Standard test method for unconfined compressive strength of intact core specimens, ASTM, Philadelphia, Pennsylvania, USA. ASTM D3967-95a. 1995. Standard Test Method for Splitting Tensile Strength of Intact Rock Core Specimens, ASTM, Philadelphia, Pennsylvania, USA. Eberhardt, E. 1998. Brittle rock fracture and progressive damage in uniaxial compression. Ph.D. thesis, Department of Geological Sciences, University of Saskatchewan, Saskatoon. Griffith, A.A. 1924. Theory of Rupture, First Intern. Congr. Appl. Mech., Delft, pp. 55-63. Hawkes, I. And Mellor, M. 1970. Uniaxial testing in rock mechanics laboratories, Engineering Geology, 4, pp 177-285. Hebert, M., 2004, “Get the Roll Surface Right”, Plastics Technology,Website, http://www.plasticstechnology.com/articles Szczepanik, Z., Milne, D., Kostakis, K. and Eberhardt, E. 2003. Long term laboratory strength tests in hard rock, International Society of Rock Mechanics, Gauteng, South Africa. Szczepanik, Z., Milne, D., Hawkes, C. and Greenlay, K. 2005. The influence of end effects on unconfined compressive strength, CGS - AGM, Saskatoon, September, (CD-ROM).