Heating Curves 1 Name ______________________________________________ Date _________ Period ______ Heating Curves Lab Pre-Lab Discussion (Do Not Write in Lab Report) When heat is added to ice, it will melt and change to water. As water is heated, its temperature rises. Eventually, the water will boil and change into a vapor (gas). The substance has gone through two changes in phase. The temperatures at which these phase changes occur are important characteristic properties. The relationship between the heat energy and the behavior of the substance is also important in understanding the difference between heat and temperature. In this lab experiment you will be dealing with the relationship between heat energy and changes in phase of matter. Purpose To create a heating curve for water from solid ice to water vapor. Equipment / Materials 250mL Beaker Ring Stand Iron Ring Wire Gauze Bunsen Burner Vernier Temperature Probe Ice Liquid Water Test Tube Clamp Stirring Rod Procedure 1. Fill a 250 mL beaker 2/3 full with ice and add water to cover the ice. 2. Place the beaker on a wire gauze on a ring stand. Clamp a Vernier probe so that it is below the water line. Do not let the sensor rest on the bottom or side of the beaker. 3. Stir carefully with a stirring rod until the temperature stabilizes at or below 0.0°C. Record the temperature at 30-second intervals. 4. After two minutes (record the time below the table), warm the ice water over a Bunsen Burner and continue to record the temperature at 30-second intervals. NOTE: Once the Bunsen Burner is set, leave it at this setting and make no adjustments to the flame. Stir continuously while heating. 5. Record the time at which all the ice has melted. Also record the time at which the water begins to boil. 6. Continue to heat the water for at least 3 minutes after the water begins to boil, recording the temperature at 30-second intervals. After three minutes, turn off the burner and record the time. 7. Plot a heating curve using your data. On the curve, indicate the point at which the ice melted and the liquid water boiled. Heating Curves 2 Data Time Elapsed (minutes : seconds) Beaker Temperature (°C) Time Elapsed (minutes : seconds) 0:00 13:00 0:30 13:30 1:00 14:00 1:30 14:30 2:00 15:00 2:30 15:30 3:00 16:00 3:30 16:30 4:00 17:00 4:30 17:30 5:00 18:00 5:30 18:30 6:00 19:00 6:30 19:30 7:00 20:00 7:30 20:30 8:00 21:00 8:30 21:30 9:00 22:00 9:30 22:30 10:00 23:00 10:30 23:30 11:00 24:00 11:30 24:30 12:00 25:00 12:30 25:30 Beaker Temperature (°C) Heating Start Time______________ Ice Melting Time________________ Heating End Time_______________ Water Boiling Time_____________ Heating Curves 3 Questions 1. What was happening to the water when the lines on the graph were mostly flat? What kind of energy was being added to the system? _______________________________________________________________________ _______________________________________________________________________ _______________________________________________________________________ _______________________________________________________________________ 2. What was happening to the water when the lines on the graph were mostly sloped? What kind of energy was being added to the system? _______________________________________________________________________ _______________________________________________________________________ _______________________________________________________________________ _______________________________________________________________________ 3. Was the energy flow into the beaker constant? How did you know? Can you make a useful heating curve if the energy flow is not constant? Why or why not? _______________________________________________________________________ _______________________________________________________________________ _______________________________________________________________________ _______________________________________________________________________ Conclusion Based on your heating curve, determine the melting and boiling points of water. Does this match the accepted values (0°C for melting and 100°C for boiling)? What sources of error (3+) are there in the experiment that may keep you from having the perfect melting and boiling points? _______________________________________________________________________ _______________________________________________________________________ _______________________________________________________________________ _______________________________________________________________________ _______________________________________________________________________ _______________________________________________________________________ Heating Curves 4