UCC/UGC/YCC Proposal for Course Change FAST TRACK (Select if this will be a fast track item. Refer to UCC or UGC Fast Track Policy for eligibility) 1. Effective BEGINNING of what term and year?: Fall 2013 See effective dates calendar. 2. College: CEFNS 4. Current course subject and number: 3. Academic Unit: Chemistry CHM 238L 5. Current title, description and units. Cut and (www4.nau.edu/aio/AcademicCatalog/academiccatalogs.htm) Bold the proposed changes in this column to differentiate from what is not changing, and Bold with strikethrough what is being deleted. CHM 238L GENERAL ORGANIC CHEMISTRY II LAB (2) Advanced work in chemical synthesis, use of the chemical literature, and the elucidation of product structures by spectroscopic methods. 6 hrs. lab. Letter grade only. Course fee required. Prerequisite: CHM 235 and CHM 235L and Prerequisite or Corequisite: CHM 238 CHM 238L GENERAL ORGANIC CHEMISTRY II LAB (2) (1) Advanced work in chemical synthesis, use of the chemical literature, and the elucidation of product structures by spectroscopic methods. 6 3 hrs. lab. Letter grade only. Course fee required. Prerequisite: CHM 235 and CHM 235L and Prerequisite or Co requisite: CHM 238 paste, in its entirety, from the current on-line academic catalog*. *if there has been a previously approved UCC/UGC/YCC change since the last catalog year, please copy the approved text from the proposal form into this field. 6. Is this course in any plan (major, minor or certificate) or sub plan (emphasis or concentration)? Yes No If yes, describe the impact and attach written responses from the affected academic units prior to college curricular submission. BS Chemistry, BS Environmental Science; Chemistry Emphasis, BSED Secondary Ed; Chemistry, BS Biology (elective), BS Biomedical Science (elective). See attached. 7. Is there a related plan or sub plan change proposal being submitted? Yes No If no, explain. 8. Does this course include combined lecture and lab components? Yes If yes, note the units specific to each component in the course description above. No 9. Is there a course fee? No Yes 10. Justification for course change. We are proposing to reduce CHM 238L (Organic Lab II) from 2 units to 1 unit. This change is proposed for several reasons: (a) most students who take CHM 238L are not chemistry majors and do not need the extra unit, (2) increased faculty workloads make it difficult to staff a 2-unit lab, (c) medical school requires only a one-unit lab, and (d) most other institutions offer only a 1-unit lab. IN THE FOLLOWING SECTION, COMPLETE ONLY WHAT IS CHANGING If the changes included in this proposal are significant, attach copies of original and proposed syllabi CURRENT Current course subject and number PROPOSED Proposed course subject and number Current number of units 2 Current short course title Proposed number of units 1 Proposed short course title (max 30 characters) Current long course title Proposed long course title (max 100 characters) Current grading option letter grade pass/fail or both Current repeat for additional units Proposed grading option letter grade pass/fail or both Proposed repeat for additional units Current max number of units Proposed max number of units Current prerequisite Proposed prerequisite Current co-requisite Proposed co-requisite Current co-convene with Proposed co-convene with Current cross list with Proposed cross list with Answer 11-15 for UCC/YCC only: 11. Is this course an approved Liberal Studies or Diversity course? If yes, select all that apply. Liberal Studies Diversity Yes Both No 12. Do you want to remove the Liberal Studies or Diversity designation? If yes, select all that apply. Liberal Studies Diversity Yes No Yes No 14. Is the course a Common Course as defined by your Articulation Task Force? Yes No 15. Is this course a Shared Unique Numbering (SUN) course? No 13. Is this course listed in the Course Equivalency Guide? Scott Galland Reviewed by Curriculum Process Associate Both Yes 09/13/2012 Date Approvals: Department Chair/ Unit Head (if appropriate) Date Chair of college curriculum committee Date Dean of college Date For Committee use only: UCC/UGC/YCC Approval Approved as submitted: Date Yes No Approved as modified: Yes No From: Maribeth Watwood Sent: Friday, August 31, 2012 3:13 PM To: Marin Sands Robinson Cc: Teresa Del Vecchio Lane Subject: RE: 1 unit CHM 238L Marin, That change is perfectly fine with us – Thank you for checking. We support the change. Best wishes, Maribeth Maribeth Watwood, Ph.D. Chair, Department of Biological Sciences Northern Arizona University Flagstaff, AZ 86011-5640 From: Marin Sands Robinson Sent: Friday, August 31, 2012 2:18 PM To: Maribeth Watwood Subject: 1 unit CHM 238L Hi Maribeth, Beginning in Fall 2013, chemistry is proposing to reduce Advanced Organic Lab, CHM 238L, from 2 units to 1 unit. For the curriculum committee, we will need a short email from you stating that you support this change. CHM 238L is currently listed in two of your plans as an option for “up to 6 units of non-BIO prefix courses” (see below). You can probably just leave it this way. We do recommend, however, that your advisors make it clear to pre-meds that medical school does require CHM 238L, especially now that it is 1 unit and not 2. B.S. Biomedical Sciences Up to six units of non-BIO prefix courses from: CHM 238L, 461, 462; NTS 256; PHI 332 B.S. Biology up to 6 units of non-BIO prefix courses from the following (lots of options): CHM 238L, 320/320L, 360L, 440, 461, 462C, 560 Let me know if you have any questions! Thanks, Marin From: Scott Anderson Sent: Wednesday, September 12, 2012 8:48 PM To: Marin Sands Robinson Cc: Stuart S Galland; Michael Ort; Nancy Johnson; Roderic Alan Parnell; Angie Moline; Erik Nielsen; Scott Anderson Subject: RE: 238L Marin, If you feel this won't necessarily impact the student experience I support you on this one. I am sure that we can find an additional credit hour somewhere for our students. Thanks for the heads up. Scott R. SCOTT ANDERSON Professor of Paleoecology & Program Chair of Environmental Sciences School of Earth Sciences & Environmental Sustainability Building 19, Room 119 (Box 5694) Northern Arizona University, Flagstaff, AZ 86011 From: Marin Sands Robinson Sent: Wednesday, September 12, 2012 2:26 PM To: Scott Anderson Cc: Stuart S Galland Subject: 238L Hi Scott, We are proposing to reduce our two-unit second-semester organic chemistry lab (CHM 238L) from 2 units (6 contact hours per week) two one unit (3 hours per week). We are doing this for staffing reasons and because most students taking CHM 238L are biology majors and do not need the in-depth organic lab experience. Students will still have 2 units of organic lab (CHM 235L and 238L), which is what most schools offer. Because this affects the ENV-CHM emphasis degree, we will need an email of support from you. Let me know if you have questions, and thanks! Cheers, Marin Chemistry Emphasis (43 units- reduced to 42): CHM 235/235L, 238/238L, 320/320L, 341, 425C/425L (22 units, reduced to 21 units) ENV 430 (3 units) MAT 136 and 137 (8 units) PHY 161 and 262 (7 units) (PHY 262L is not required) One additional upper-division ENV course (3 units) Dr. Marin S. Robinson Professor and Chair of Chemistry and Biochemistry (CHM 122) PO Box 5698 S. Beaver Street Bldg 20, Room 125 Flagstaff, AZ 86011-5698 928.523.6295 (ph) 928.523.8111 (fax) EXISTING SYLLABUS (2 UNITS) College of Engineering, Forestry & Natural Sciences Department of Chemistry and Biochemistry CHM 238L-A, Organic Chemistry Lab II Spring 2010 Course Number 4976 9:35 a.m. – 12:45 p.m. TuTh, SLF 205 (Bldg 17) Instructor: Dr. Cindy C. Browder Office: CHM 120 (Bldg 20) email: cindy.browder@nau.edu Office Hours: W 11:15 – 1:15, Th 1:00 – 2:00 Phone: 523-9062 website: https://vista.nau.edu/webct/logon/31076871582041 TA: Joshua Ohland email: jto3@nau.edu phone: 928-707-2464 Prerequisite: CHM 235 & 235L Course Materials: 1. Chemical Education Resources Course Pak (required). 2. Indirectly or non-vented goggles (required). 3. Laboratory Notebook (required). Course Objectives: Advanced work in organic synthesis; use of the chemical literature; and the elucidation of organic structures by spectroscopic methods. Corequisite: CHM 238 GRADING CRITERIA Post Labs: Post-labs will be due no later than the Friday the week after the completion of the experiment (see the laboratory schedule for specific dates). The specific details for each Post-Lab will be discussed at the beginning of the experiment. There will be a total of 5 post-labs worth 50 points each. Lab Reports: In addition to the post-labs, there will be a total of 6 lab reports due. All lab reports will be due two Mondays after the completion of the experiment (see the laboratory schedule for specific dates). You will be given separate, specific guidelines for writing lab reports. Each lab report will be worth 100 points. Literature Search: Students will be required to complete a literature search of an assigned subject and/or chemical compound. Details of the project will be discussed later in the semester. Attendance: Attendance is required and you must complete all labs. There will be no make-up labs. One lab missed for legitimate reasons (e.g. trips sponsored by the university) will be factored out of your grade only if the instructor or TA was notified before the absence. Please note that a medical or dental appointment is not an acceptable reason for missing a lab except in case of an emergency. In case of an emergency, you must provide written proof of for any absence (e.g. a signed note from a physician). Late Work: You will lose 5% of the points for the assignment per day late. Maximum Possible Points: Post-Labs (5 x 50 pts each) 250 pts Lab Reports (6 x 100 pts each) 600 pts Lab Notebook (collected on 4/15) 100 pts Lab Performance 350 pts Total: 1300 pts Grade for the Course: A = 100% - 90% B = 89% - 80% C = 79% - 70% D = 69% - 60% F = 59% - 0% Laboratory Performance: (1300 - 1170 pts) (1169 - 1040 pts) (1039 - 910 pts) (909 - 780 pts) (779 - 0 pts) Laboratory performance will be evaluated in the following areas and in the following priority: lab safety, preparedness, technical skills, and cleanliness. More details will be given in class. Dropping This: The deadline to drop/delete this course is Friday, February 5, 2009. The deadline to drop with a “W” is Course: Friday, March 12, 2009. If you drop the lab, your locker drawer must be checked out and keys returned during your normal lab section before Reading Week. The penalty for not checking your locker is $20 for each key not returned, and $30 for the clean-up charge. You will also be billed for any broken or missing equipment or glassware. Remember that a drop/add for this course is not complete until you have it processed through the Registrar’s office. Laboratory Schedule: Expt. # Dates Report type Due Date --- 1/12 – 1/14 Check-in --- --- 707 1/19 – 1/21 Separating a Mixture of Biphenyl, Benzhydrol, and Benzophenone by Thin Layer Chromatography Post-lab 1/29 708 1/26 – 1/28 Separating Ferrocene and Acetylferrocene by Adsorption Column Chromatography (dry-pack method) Post-lab 2/5 --- 2/4 Literature Search Post-lab day of lab 711 2/9 – 2/11 Using Nuclear Magnetic Resonance Spectroscopy (NMR) to Identify an Unknown Compound Post-lab 2/19 717 2/16 – 2/18 The Diels-Alder Reaction of Anthracene with Maleic Anhydride Lab Report 3/1 715 2/23 – 2/25 Reducing Benzil using Sodium Borohydride Lab Report 3/8 718 3/2 – 3/4 Nucleophilic Addition to Carbonyl: Grignard Reaction with an Aldehyde Lab Report 3/22 3/9 – 3/11 Friedel-Crafts Acylation: Synthesis of 4-Methoxyacetophenone Lab Report 3/29 723 Experiment Title 721 3/30 – 4/1 The Wittig Reaction: Synthesis of trans-9-(2-phenylethenyl)anthracene Lab Report 4/12 720 4/6 – 4/8 The Aldol Condensation: Synthesis of Dibenzalacetone Lab Report 4/19 731 4/13 – 4/15 Post-lab 4/15 --- 4/20 --- --- Luminol Synthesis and Chemiluminescence Check-out PROPOSED SYLLABUS (1 UNIT) DEPARTMENT OF CHEMISTRY AND BIOCHEMISTRY CHM 238L GENERAL ORGANIC CHEMISTRY LABORATORY II – 1 CREDIT FALL 2012 WEDNESDAY 1:50 – 4:50 PM 1 CREDIT (3 HOURS) Instructor Information Dr. Cindy C. Browder Bldg 20, Rm 120 cindy.browder@nau.edu 928-523-9062 Office hours TWTh 11:30 am – 12:30 pm TA Information Kellan Finney kbf8@nau.edu 970-275-3918 Course prerequisites Prerequisite: CHM 235 and CHM 235L and Prerequisite or Corequisite: CHM 238. Cannot be taken for credit if credit has been earned for CHM 238L. Course description Advanced work in chemical synthesis and the elucidation of product structures by spectroscopic methods. Emphasis will be on synthesis, purification, and analysis techniques. Chemistry structure drawing and spectra processing software will be utilized. Student Learning Expectations/Outcomes for this Course Expand on skills and techniques from CHM 235L, including distillation, crystallization, chromatography (preparative and analytical), standard organic synthesis techniques, and characterization of organic compounds through physical properties and NMR. Maintenence of a proper and detailed laboratory notebook is required. Using professional tools (chemical structure drawing and spectra processing software) is necessary for presentation and analysis of results, including preparation of laboratory reports. Course structure/approach Laboratory course. Students will work individually to demonstrate mastery of laboratory skills as well as proficiency in synthesis, purification, and product characterization. Assessments will also require proficiency in keeping laboratory records (laboratory notebook), chemical structure drawing, and spectra processing. Textbook and required materials Chemical Education Resources Course Pak Indirectly or non-vented goggles Laboratory Notebook Recommended optional materials Lab coat or apron Organic Chemistry 10th Ed., Solomons and Fryhle, or comparable text Molecular model kit Course outline All experiments are to be carried out during the scheduled week. No make-up labs are allowed. Date Laboratory work 8/29 Check-in; Safety/orientation; Lab/drawer prep 9/5 TECH 707: Separating a Mixture of Biphenyl, Benzhydrol, and Benzophenone by Thin Layer Chromatography 9/12 TECH 708: Separating Ferrocene and Acetylferrocene by Adsorption Column Chromatography (dry-pack method) TLC report due, 50 points 9/19 SYNT 718: Nucleophilic Addition to Carbonyl: Grignard Reaction with an Aldehyde Chromatography report, 50 points 9/26 SYNT 718: Grignard Reaction with an Aldehyde (continued) NMR Processing 10/3 The Friedel-Crafts Reaction: Acetylation of Ferrocene Grignard report, 100 points 10/10 The Friedel-Crafts Reaction (continued) Solid-phase Photochemistry Notebooks due at end of lab period 10/17 No lab 10/24 Solid-phase Photochemistry (continued) Experiment 31: Chiral Reduction of Ethyl Acetoacetate Friedel-Crafts report, 50 points 10/31 Experiment 31: Chiral Reduction of Ethyl Acetoacetate (continued) Photochemistry report, 100 points 11/7 SYNT 721: The Wittig Reaction: Synthesis of trans-9-(2phenylethenyl)-anthracene Yeast report, 100 points 11/14 SYNT0731: Luminol Synthesis and Chemiluminescence Wittig report, 100 points 11/21 Thanksgiving – no lab 11/28 SYNT0731: Luminol Synthesis and Chemiluminescence (continued) Luminol report, 50 points 12/5 Final exam and Check-out Notebook due Final exam Revised 06/22/2011 Assignment(s) due Assessment of Student Learning Outcomes Methods of Assessment Students will be graded based on their notebooks, post-lab reports, and laboratory performance. Notebook guidelines are provided in a separate handout, and specific requirements for each experiment will be discussed in the lab lecture preceding each experiment. Notebooks will be checked daily and collected twice during the semester. Each submission is worth 50 points. The details for each report will be discussed at the beginning of each experiment as well. The point value of each report varies, and all reports will total 600 points. A portion of the grade will also be based on laboratory performance. Laboratory performance will be evaluated in the following areas and in the following priority: lab safety, preparedness, technical skills, and cleanliness. More details will be given in class. A final exam over laboratory concepts will be given in the last week of the lab. This exam will cover a variety of laboratory concepts, including questions on the use of various laboratory techniques and the interpretation of data (TLC, NMR, etc.). Timeline for Assessment For all labs, experiments must be carried out during the week designated in the course outline. Lab assignments for these experiments are due one week from the completion of the experiment, as indicated in the course schedule. Notebook submission dates are also listed in the course schedule. The final exam will be given at the start of the laboratory period on the scheduled date. Grading System Maximum Possible Points Post-Labs (50-100 pts each) Lab Notebook (2 x 50 pts each) Lab Exam Lab Performance Total: Grade for the Course: A B C D F = = = = = 600 pts 100 pts 100 pts 200 pts 1000 pts 100% - 90% (900 - 1000 pts) 89% - 80% (800 - 899 pts) 79% - 70% (700 - 799 pts) 69% - 60% (600 - 699 pts) 59% - 0% (<600 pts) Course policies Attendance Attendance is required and you must complete all labs during the week in which they are scheduled. There will be no make-up labs. One lab missed for legitimate reasons (e.g. trips sponsored by the university) will be factored out of your grade only if the instructor or TA was notified before the absence. Please note that a medical or dental appointment is not an acceptable reason for missing a lab except in case of an emergency. In case of an emergency, you must provide written proof of for any absence (e.g. a signed note from a physician). Late Work You will lose 5% of the points for the assignment per day late. Laboratory Safety and Lab Performance Contract The hazards encountered in CHM 299L are significantly higher than those encountered in other laboratory courses. You must be aware of safety hazards associated with each experiment before Revised 06/22/2011 you begin work and do a risk assessment. Read the experiment and review MSDS safety information on hazardous chemicals before starting each experiment. The safety and introductory exercises handed out on the first day of lab must be completed, signed, and turned in to your TA along with a “Lab Performance Contract” before you will be allowed to begin experimental work. Students with known conditions (i.e. respiratory problems, allergies, pregnancy, etc.) should consult the instructor for special precautions. Laboratory Lockers (Drawers) Students will be assigned a Laboratory Locker on the first day of lab. It is your responsibility to maintain the locker and the equipment within it so that it is ready to use at the start of each lab period. After the check-in day, any locker equipment that is missing, broken, or otherwise unusable must be replaced at the stockroom window. Students may be billed and/or lose performance points for excessive loss or breakage of equipment, or for accumulating surplus equipment in their drawers. Laboratory and Glassware Cleaning Students are responsible for the cleanliness of their assigned drawer, hood space, bench space, and all common use areas (dispensing / waste hoods, balance area, etc.) At the end of each lab, hoods and benches must be wiped down with a damp sponge. Glassware should be cleaned with Simple Green and water – not acetone. Consult your instructor and/or TA if this is not a sufficient cleaning process. Dropping This Course The deadline to drop/delete this course is Thursday, September 6, 2012. The deadline to drop with a “W” is Friday, October 26, 2012. If you drop the lab, your drawer must be checked out and keys returned during your normal lab section before the last class meeting. You will be billed a $30 cleanup charge if you fail to check out of your drawer, in addition to the costs for any broken or missing equipment or glassware. Remember that a drop/add for this course is not complete until you have it processed through the Registrar’s office. University Closure In the unlikely event of an unanticipated university closure, experiments will be rescheduled at the instructor’s discretion. Academic dishonesty The Department of Chemistry and Biochemistry strictly enforces the University’s policy on academic dishonesty. Fabrication or falsification of data, or using another student’s unknown, unknown number, data, or results are examples of academic dishonesty. Plagiarism, including using information from another student on a laboratory report, is also academic dishonesty. If you use information from a published source (such as the lab manual), be sure to cite that source in your report; otherwise it will be considered plagiarism. Any incident of academic dishonesty will result in a zero on the assignment without an opportunity to improve the score. Subsequent infractions will result in dismissal from the laboratory and a grade of F for the course. Incidents involving students with a department or university record of academic dishonesty will result in dismissal from the laboratory, a F in the course with no opportunity to repeat the course or improve the grade, and possible expulsion from the University. University policies Information on the Safe Working and Learning Environment, Students with Disabilities, Institutional Review Board, and Academic Integrity policies can be found at http://www4.nau.edu/avpaa/UCCPolicy/plcystmt.html. Revised 06/22/2011