MOLECUL AR SPECTROSCOPY Product Specif ications Thermo Scientific DXR2 Raman Family Focus on answers, not the technique DXR2xi Raman Imaging Microscope Easily adapt to any sample challenge using the Thermo Scientific™ DXR™2 family of Raman instruments. With intuitive and easy to use software and instrumentation, you get results faster than ever before. • High-performance, high-spatial resolution Raman imaging system in a complete, integrated package • Produces stunning chemical images and gives research-quality results quickly for all users DXR2 Raman Microscope • Research-grade microscope offering superior combination of performance and ease-of-use • Offers high spatial resolution point-and-shoot Raman microscopy for the most demanding analytical tasks DXR2 SmartRaman Spectrometer • Built for high performance, dedicated bulk sample analysis and designed for busy multi-purpose analytical labs • Provides comprehensive, reproducible, and accurate results in a dependable, low-maintenance platform DXR2 Raman Microscope • Industry-leading performance, reproducibility, and reliability • V ersatile platform with researchgrade optics and light microscopy options • R apid, high-quality point-and-shoot results via an intuitive platform • P owerful software enables mapping of lines, areas, depth profiles, and cross-sectional slices Performance Specifications Stage Options Spatial Resolution Resolution (X, Y axes) with high-precision motorized stage Better than 1 µm Better than 2 µm 1 Confocal depth resolution 1. Measured with 532 nm excitation and 100× objective. Spatial resolution depends on the wavelength of the excitation laser and the objective used. Standard Motorized Stage 125 mm × 75 mm travel X and Y dimensions Step size 1 µm Software-controlled Z focus Joystick controller with focus control knob High-precision Motorized Stage Automated Polarization2 100 mm × 75 mm travel X and Y dimensions Step size 0.1 µm Laser Polarization Software-controlled Z focus Joystick controller with focus control knob Horizontal, Vertical, or Depolarized Analyzer PolarizationNot in beam, Horizontal, Vertical, or Custom Angle (1° increments) 2. O ptional feature Spectrograph Design Physical Dimensions Triplet Spectrograph 3 ApertureFour Software-selectable Apertures No moving parts Width 94 cm 25 and 50 µm confocal pinhole apertures 25 and 50 µm slit apertures Depth 68 cm Height 61 cm Weight 66.5 kg 3. Patented design minimizes aberrations in the primary optics. DXR2 Family Shared Component Specifications The DXR2 family of Raman benchtop instruments is based on the same reliable design, allowing users to easily exchange pre-aligned laser, filter, and grating components among instruments without using tools. General System Features Lasers4 Multiple Excitation Lasers Supported wavelengths 455 nm, 532 nm, 633 nm, 785 nm Laser SafetyClass 1 standard Class 3B when fiber optic interface installed and with some specialized accessories Laser Power RegulatorActive feedback system to control absolute laser power delivered to the sample Fine Laser Power ControlPower controlled and reported at samples in 0.1 mW increments Facilitates laser-to-laser and system-to-system reproducibility Replaceable Components Smart Components Pre-aligned, user-exchangeable system components (lasers, filters, gratings, fiber optic launcher) lock into place and automatically optimize system alignment and calibration upon installation Software checks for laser, grating, filter compatibility Software restores alignment and calibration settings when lasers are exchanged Automatically optimized upon exchange System Alignment Computer InterfaceThrough USB 2.0 or USB 3.0 ports Some accessories may require additional USB or serial ports 4. A ll lasers have a 12 month warranty. DXR2xi Raman Imaging Microscope • E xceptional stability for highest quality Raman imaging over small and large areas • Intelligent autofocus and automated feature identification tools reduce total experiment time • P owerful, real-time component analysis • V isual control and parameter optimization lets you focus on the answer, not the technique Performance Specifications Imaging Performance Spatial Resolution Resolution (X, Y axes) with high-precision motorized stage Better than 0.5 µm Typical Image Collection Time Single 100 μm × 100 μm image with 35 seconds 1 μm image pixel size in both directions Better than 2 μm 10 mm diameter tablet with 20 μm image pixel size 1 Confocal depth resolution 1. Measured with 532 nm excitation and 100× objective. Spatial resolution depends on the wavelength of the excitation laser and the objective used. Laser Polarization Maximum Spectral Acquisition Rate 600 spectra per second Maximum Image Area Automated Polarization2 11 minutes 101.6 mm × 76.2 mm Minimum Image Pixel Size in X and Y 100 nm Horizontal, Vertical, or Depolarized Analyzer Polarization N ot in beam, Horizontal, Vertical, or Custom Angle (1° increments) Imaging with polarization is possible Minimum Step Size in Z 200 nm Physical Dimensions 2. O ptional feature Spectrograph Design Triplet Spectrograph3 No moving parts Camera Technology TE cooled back illuminated EMCCD5 ApertureFour Software-selectable Apertures 25 and 50 µm confocal pinhole apertures 25 and 50 µm slit apertures Width 94 cm Depth 68 cm Height 61 cm Weight 86 kg 3. Patented design minimizes aberrations in the primary optics. 5. F ront illuminated EMCCD available on request. DXR2 Family Shared Component Specifications Lasers 455 nm 532 nm Laser Type Frequency-stabilized single mode diode laser Maximum Laser Output Power 25 mW 633 nm 785 nm (high brightness) 785 nm (high power) 6 Diode-pumped, solid state HeNe gas (DPSS) Frequency-stabilized single mode diode laser Multiple transverse mode, narrow-spectrum diode 24 mW 20 mW 80 mW 420 mW Laser Power at Sample7 Maximum power at sample 6 mW Maximum power at sample 10 mW Maximum power at sample 8 mW Maximum power at sample 30 mW Maximum power at sample 150 mW Center Wavelength 455 ± 0.2 nm 532 ± 1 nm 632.8 nm 785 ± 0.2 nm 785 ± 0.5 nm Transverse Mode TEM008 TEM008 TEM008 TEM008 — 6. 785 nm high-power laser recommended for SmartRaman or fiber optic measurements only. Not recommended for microscope work. 7. Continuously variable to the maximum laser power at the sample in 0.1 mW increments. 8. Eliminates the need to aperture the laser and provides a Gaussian profile, optimizing confocality of the laser. DXR2 SmartRaman Spectrometer • L arge sampling compartment enables flexibility in experimental design • Ideal for bottles to vials to bulk powders – and everything in-between • B road range of sampling accessories for most applications and sample formats • P owerful, Variable Dynamic Point Sampling enables rapid averaging over large sample area Performance Specifications Laser Spot Size at Sample Nominal 10 µm Sampling AreaUser-selectable from single spot to 5 mm × 5 mm with Variable Dynamic Point Sampling (VDPS) technology (available with the Universal Platform Sampling Accessory) Spectrograph Physical Dimensions Design Triplet Spectrograph3 No moving parts Aperture F our Software-selectable 25 and 50 µm confocal pinhole apertures Apertures 25 and 50 µm slit apertures 3. Patented design minimizes aberrations in the primary optics. Width 94 cm Depth 56 cm Height 44 cm Weight 52.8 kg DXR2 Family Shared Component Specifications System Performance – Spectral Range and Resolution Lasers 455 nm 532 nm 633 nm 785 nm Full-Range Grating Spectral Resolution9 Better than 5.0 cm-1 FWHM Better than 5.0 cm-1 FWHM Better than 5.0 cm-1 FWHM Better than 5.0 cm-1 FWHM Spectral Dispersion 2 cm-1/CCD pixel element 2 cm-1/CCD pixel element 2 cm-1/CCD pixel element 2 cm-1/CCD pixel element Upper Cutoff 3500 cm 3500 cm 3500 cm 3250 cm-1 Lower Cutoff 10 85 cm-1 50 cm-1 50 cm-1 50 cm-1 2 cm FWHM 2 cm FWHM 2 cm-1 FWHM High-Resolution Grating Spectral Resolution Spectral Dispersion -1 -1 11 -1 -1 -1 1 cm-1/CCD pixel element 1 cm-1/CCD pixel element 1 cm-1/CCD pixel element Upper Cutoff 1800 cm 1800 cm 1800 cm-1 Lower Cutoff 10 50 cm-1 50 cm-1 50 cm-1 Extended-Range Grating Spectral Resolution 11 cm FWHM Upper Cutoff 6000 cm-1 Lower Cutoff 50 cm-1 10 -1 -1 -1 9. The system spectral resolutions is measured using ASTM Method E2529-06 and a 100× objective. 10. 50% maximum transmitted power. The use of some accessories such as fiber optic probes may reduce the spectral range. Check accessory specifications. 11. The DXR2xi upper cutoff for the 532 nm full-range grating spectral range is 3400 cm-1. DXR2 Microscopy Options Illuminator Options Microscopy Options Brightfield Microscope Illuminator, plus Nosepiece Reflection illumination. Accepts brightfield objectives. Reflected and Transmitted12 Light Polarized Kit/Fixed Analyzer Brightfield/Darkfield Microscope Illuminator, plus Nosepiece Reflection illumination. Accepts brightfield/darkfield objectives and brightfield-only objectives with adaptor. Supports optional transmission illumination. Reflected and Transmitted12 Light Differential Interference Contrast (DIC) or Nomarski Illumination Kit Rotatable Analyzer 12. Requires transmission illumination option Objectives Standard Working Distance Objectives Sampling Stage Options 10×, 20×, 50×, 100× Heated and Cooled Stage from Linkam Scientific Long Working Distance Objectives10×, 20×, 50×, 100× Oil Immersion Objectives 50×, 100× Water Immersion Objectives 60× Macro Sampling AdapterIncludes 4× objective, accepts brightfield objectives only User-supplied Objectives Must be compatible with Olympus® BF or BD nosepieces Extended Reach Sampling Accessory13 Enables external sampling DXR2 Macro Sampling Options Sampling Accessories Universal Platform Sampling Accessory Toolheads for Universal Platform Sampling accessory: Well-Plate/Tablet Autosampler, Tablet Holder, Bottle Holder, Universal Plate Hot-swappable Pinned-in-place Smart: reports identity and serial number to Carousel Autosampler Sampling AccessoryThermo Scientific™ OMNIC™ software 180 Degree Sampling Accessory The Universal Platform Sampling accessory with Bottle Holder Polymer SlicerVertically secures a multilayered polymer for cross-sectional analysis Single and Dual Holds one or two standard Slide Insertmicroscope slides (75 mm × 25 mm) 13. Class 3B The Universal Platform Sampling accessory with Well-Plate Rotating Stage InsertAccepts standard microscope slide, provides manual rotation to any position Sample Holder Provides maximum flexibility Breadboard with Clipsfor holding small and uniquely shaped samples without risk of contamination with adhesives Microtiter Well-plate Holds standard 96 well Holdermicroplates Capillary Tube Array Holder The DXR2 SmartRaman spectrometer with the Carousel Autosampler Sampling accessory InstallationPre-aligned, user-installable/removable without the need for tools Fiber optic port is precision-locked into place Compatibility Compatible with 532 nm and 785 nm excitation laser frequencies, accepts probes with standard FC connectors Smart Technology Fiber optic port stores serial number Accommodates up to 16 capillary tubes XPS Sample HolderPermits easy transfer of samples from the Thermo Scientific™ K-Alpha™ X-ray photoelectron spectrometer The 180 Degree Sampling accessory for the DXR2 SmartRaman spectrometer Fiber Optic Port for DXR2 Raman Family SmartLock Installation Temperature range: –196 °C–600 °C Seamless compatibility with Linkam software In addition to the common components, the DXR2 instruments share the following general specifications. Available Thermo Scientific Software Options14 OMNIC Software Full featured molecular spectroscopy acquisition and analysis software OMNIC Series Software Supports time-based data collection OMNIC Array™ Automation Software Automated data collection and post-collection data analysis from micro-well plates and similar array formats OMNIC Atlμs™ Software Provides software-controlled hyperspectral mapping and image analysis OMNIC Specta Provides efficient data management, simplifies data process, and provides powerful spectral identification OMNIC Macros\Pro™ Software Interface for advanced Visual Basic programming OMNICxi Raman Imaging Software Visually driven chemical imaging and analysis software ValPro™ System Qualification Software Full featured system qualification package for verifying instrument design and performance 14. Not all software packages available on all systems Instrument Alignment, Calibration, and Optimization Alignment Entirely Software-controlled 15 Automated alignment technique aligns laser, Raman emission and visual beam paths to m icroscope crosshairs Calibration Wavelength Software-controlled calibration using multiple neon emission lines Laser Frequency Software-controlled calibration using multiple polystyrene Raman peaks Intensity Software-controlled calibration using standardized white light source Automatic Intensity Correction Provides instrument-independent results with all excitation lasers Laser Power Regulator Absolute excitation laser power at the sample controlled by OMNIC software Laser power at sample reported in mW Automatic Fluorescence Correction Compensates for potential fluorescence in data User Interface Autofocus Optimizes signal from sample Autoexposure Automatically sets optimal exposure time and number of repeat scans for highest quality data acquisition Smart Background 15. Standards incorporated into patented Alignment/Calibration Tool Automatically accounts for dark current, improving spectral quality and saving time † Instrument Serviceability Other Specifications Additional Lasers or Replacement Lasers, User-installable without tools Filter, Grating Sets Environmental Minimum temperature: 16 °C Maximum temperature: 27 °C Instrument Performance Monitoring Humidity range: 20–80% Electric Requirements 100–240 VAC, 47–63 Hz Regulatory Approval CE, UL/CSA/ETL, 21 CFR1040, 10 S oftware provides real-time visual status of system readiness, including error condition checking and diagnostics Warranty Information12-month warranty standard on the complete DXR2 SmartRaman spectrometer, DXR2xi Raman imaging microscope, and DXR2 Raman microscope. Extended warranties are available. www.thermofisher.com/raman The DXR2 SmartRaman spectrometer, DXR2 Raman microscope, and DXR2xi Raman imaging microscope, in their default configurations, are Class 1 laser products. Installation of a fiber optic port and fiber optic probe will convert all DXR family instruments to Class 3B laser products. † DXR2 Raman microscope and DXR2 SmartRaman spectrometer may be manufactured under or covered by US Patents 7345760, 7471390, 7233870, 7605918, 7688530, and 8111392. DXR2xi Raman imaging microscope may be manufactured under or covered by US Patents 7233870, 7345760, 7688530, and 8111392. The Universal Platform Sampling Accessory may be manufactured under or covered by US Patent 7595873. ©2013-2016 Thermo Fisher Scientific Inc. All rights reserved. ISO is a trademark of the International Standards Organization. Olympus is a registered trademark of Olympus Optical Co., Ltd. All other trademarks are the property of Thermo Fisher Scientific and its subsidiaries. Specifications, terms and pricing are subject to change. Not all products are available in all countries. Please consult your local sales representative for details. 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