Rocks and Minerals ID Lab Juniata College Science in Motion Middle School Rocks and Minerals ID Lab Introduction: Rocks and minerals have many uses in our everyday lives. For everything from using diamonds in electronics and industry to various minerals that are used as vitamins minerals. We could not live in this industrial and technology age with out minerals of all types. Can you think of any uses for rocks or minerals? Minerals are identified my several techniques or characteristics of the minerals. These characteristics include cleavage, fracture, luster, color, streak color, hardness, density, and reactivity with an acid. Purpose/Objectives: Students will recognize the differences between igneous, metamorphic, or sedimentary rocks Students will identify 10-14 or more rocks using chemical and physical means Students will answer questions about the rocks, rock cycle, and type of rock and rock characteristics. Equipment/Materials: o Teacher rocks (labeled) o Students unknown rocks, the same as the teacher rocks (7) o ID kits(7) for identifying rocks by characteristics (glass, steel nail, bottle for HCL, streak plate, copper strip, magnet, beaker for water) such as streak, hardness, cleavage, magnetic properties, density o Ice cube trays (7) for organizing rocks and minerals o Instruction sheet, key and worksheets. o Books Peterson’s Field Guide to Rocks Rocks and Minerals of PA Various maps are available that would show the location of types of rocks and minerals in PA. (upon request) Safety: o Students should not attempt to break or fracture the rocks. This will damage the rock samples and could result in potential eye injury. Safety glasses must be worn by everyone, if a rock hammer is being used. o Caution should be used when dealing with any sharp objects, such as glass, copper plate, or the steel nail. o If hydrochloric acid is used, safety glasses must be worn and all times and all acid safety precautions must be taken in the case of spills. Avoid contact with skin. o In the case of broken glass, notify your teacher and then she will clean up the glass with a dust pan. Procedure: 1. 2. 3. 4. 5. 6. Obtain a sample set of rocks for identification. Obtain the rock and mineral identification manuals. Obtain the rock and mineral identification kit. Read the directions on the “identifying Rocks and Minerals” lab. Answer the questions on the first page of the lab. Observe and note the color of your rock or mineral. (Keep in mind that physical color is the least valuable test for identification.) 7. Perform the following physical and chemical tests to each rock in the unknown rock samples. a. Close Examination of the rock i. Color: Observe and record the color of the rock or mineral. Obvious, but not always definitive. Sulfur is (almost) always yellow, and there are a few others, but not many minerals have a fixed color. Small amounts of impurities can drastically change a mineral's color. ii. Luster: The quantity and quality of light reflected from the surface. Most identification schemes begin with a simple classification based on luster. Because of this, luster is the first fundamental test to be made when identifying any mineral. Most are relatively obvious, but some minerals can exhibit a range of lusters (ex. Hematite). 1. Metallic: looks like a metal. Metallic minerals are commonly shiny and opaque 2. Non-metallic: doesn't look like a metal. There are many subtle differences in the non-metallic lusters, but most are relatively dull, and are often transparent to translucent on thin edges. 3. Waxy 4. Vitreous or glassy iii. Observe the grain size and texture distribution (uniformity) Cleavage: How a mineral breaks is determined by its internal structure, and is there very important. Unfortunately, it can also be the hardest to determine (sorry). There are two (2) major subdivisions: fracture and cleavage. i. DO NOT BREAK YOUR ROCKS!!!!!!!! ii. Fracture: The mineral just breaks, leaving an uneven surface. Most are irregular but there are some special cases (ex: the conchoidal fractures common to quartz and glass) iii. Cleavage: The mineral splits along closely spaces parallel planes, leaving a mirror surface which will flash at you if rotated in the light. Cleavage is controlled by the internal crystalline order of the mineral. A mineral can have 1, 2, 3, 4, or 6 planes of cleavage. If more than one (1) plane is present, it is important to note the angles between the cleavages. Cleavage can be obscured, but is definitive when present. Terms such as Perfect, Good in 2 directions, Poor, etc. are used to indicate the quality or strength of the cleavage. Cleavage can be tough to distinguish from external crystalline form, and it's always a shame to break a good "crystal" when checking for cleavage. c. Specific Gravity: i. Defined as "the weight of a specific volume of a mineral divided by the weight of an equal volume of water (at 4°C.)" Since water is always 1.0, it's the same number as density without any units (they cancel). This is almost impossible to measure in the field, but a rough approximation and be determined. ii. Hit: Some igneous rocks will be less dense than water and float, such as pumice. d. Effervescence/ Acid Test i. Drop a drop or two of hydrochloric acid or lemon juice (acetic acid) on the rock ii. Does it fizz? iii. This would mean that carbon dioxide is being given off and the rock is a carbonate (limestone) iv. Minerals containing calcium carbonate (CaCO3) will generally react when exposed to hydrochloric acid (HCl). Carbon dioxide (CO2) is released and the mineral or rock literally "fizzes." Some may need to be powdered (increases surface area) before any reaction can take place e. Hardness: Test the Mohs Hardness of the rock/mineral i. Hardness is the resistance of a mineral to scratching. It does NOT refer to how easily the mineral is broken. Hardness is a measure of the bond strength between atoms. If these bonds are strong, the mineral is not easily scratched. Minerals with weaker bonds are more easily scratched. Pencil "lead" is softer than paper, so it b. f. g. h. i. writes. Try writing with a steel-tipped pencil. Now the pencil rips the paper. This is clearly related to the relative hardness of each substance. Hardness in minerals can vary due to impurities, but is usually definitive. We determine the relative hardness of minerals using a scale devised by mineralogist Friedrich Mohs. The scale assigns hardness to ten common index minerals, and is based on the ability of one mineral to scratch another. ii. Try to scratch the various substances (see key) with the rock iii. Try to scratch the rock with the various substances Streak test: i. Rub the rock on the white unglazed porcelain tile. ii. The color of the powdered mineral. Streak can be definitive. Good examples include hematite (always a deep red no matter what form it's in) and chromite (distinguished from the hundreds of other black minerals by its chocolate-brown streak). iii. Observe and record the color of the streak on the tile. Magnetism: Some rocks have natural magnetism. Magnetite, i.e., the lode stone, is naturally magnetic Taste: Some minerals have a distinctive taste. Notable examples include Halite (rock salt), and Chalcanthite (a copper arsenide - be careful with this one!!). DO NOT TASTE THESE ROCKS!!! Smell: Some minerals have a distinctive odor. Sulphur is a good example. Remember to waft all chemicals, including rocks in the laboratory. 7. Record all results on the chart of rock characteristics. Mineral & Rock ID The following rocks in the small baggie. They are rocks that might be a little easier for middle school students to ID and there are sedimentary, igneous and metamorphic rocks in the baggie. I would suggest using 10-14 of these rocks for your Rock ID Lab. You can use any rocks you wish with your classroom, put please notify us if the same rocks are not in the small baggie. You can fill in the following chart similar to the ice-cube tray before you start as a key for yourself. You can also give a blank sheet to the students for their answers. You can give them a word bank consisting of only the rocks you give them, or add a few more rock names or no work bank at all. You will need to check the organization of the rocks in the ice cube tray routinely because they often get switched around. Thanks 1. Talc 2. Galena 3. Pyrite 4. Halite 5. Graphite 6. Slate 7. Pumice 8. Mica, Muscovite 9. Schist, Mica 10. Conglomerate 11. Granite 12. Gypsum 13. Quartz 14. Sandstone 15. Limestone 16. Magnetite 17. Obsidian 18. Garnet 19. Calcite 20.Pumice Mineral & Rock ID 1 2 3 4 5 6 7 8 9 10 11 12 13 14 The Mohs Scale of Relative Mineral Hardness The Mohs scale was devised by Friedrich Mohs in 1812 and has been a valuable aid to identifying minerals ever since. Here are the ten standard minerals in the scale. 1. Talc 2. Gypsum 3. Calcite 4. Fluorite 5. Apatite 6. Feldspar 7. Quartz 8. Topaz 9. Corundum 10. Diamond You use the scale by testing your unknown mineral against one of these standard minerals. Whichever one scratches the other is harder, and if both scratch each other they are both the same hardness. The Mohs scale is strictly a relative scale, but that's all that anyone needs. In terms of absolute hardness, diamond (hardness 10) actually is 4 times harder than corundum (hardness 9) and 6 times harder than topaz (hardness 8). Because it isn't made for that kind of precision, the Mohs scale uses half-numbers for in-between hardnesses. Dolomite, which scratches calcite but not fluorite, has a Mohs hardness of 3½ or 3.5. There are a few handy objects that also fit in this scale. A fingernail is 2½, a penny is 3, a knife blade is 5½, glass is 5½, and a steel file is 6½. The following is a range of the useful scale of common materials for the Mohs Hardness Scale: 1.0-2.5 Won’t scratch a fingernail 2.5-3.5 Scratches fingernail, but wont scratch copper 3.5-5.5 Scratches copper, but won’t scratch glass. 5.5-6.5 Scratches glass, but won’t scratch steel. 6.5+ Scratches steel Mohs hardness is just one aspect of identifying minerals. Along with hardness, you need to consider luster, cleavage, crystalline form, color, and rock type to zero in on an exact identification. Rock Number 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. Color & Luster Streak Color Hardness Cleavage Yes or No O of angle Specific Gravity > or < water Acid Test Fizz Yes or No Extra Tests Smell Magnetism Rock Sedimentary If Number Igneous or sedimentary Metamorphic Clastic, Chemical or Organic 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. If Igneous IntrusivePleutonic or ExtrusiveVolcanic If Igneous Felsic or Mafic If Name of Metamorphic Rock Foliated or Non Foliated Vocabulary: Rock Cycle: the process by which rocks are formed, altered, destroyed, and reformed by geological processes and which is recurrent, returning to a starting point. The rock cycle is made of the following types of rocks, each of which can change into the other: igneous rocks, metamorphic rocks, and sedimentary rocks. Igneous rocks http://www.cotf.edu/ete/modules/msese/earthsysflr/rock.html Igneous rocks (from the Greek word for fire) form from when hot, molten rock (magma) crystallizes and solidifies. The melt originates deep within the Earth near active plate boundaries or hot spots, and then rises toward the surface. Igneous rocks are divided into two groups, intrusive or extrusive, depending upon where the molten rock solidifies. Extrusive igneous rock Extrusive, or volcanic, igneous rock is produced when magma exits and cools outside of, or very near the Earth’s surface. These are the rocks that form at erupting volcanoes and oozing fissures. The magma, called lava when molten rock erupts on the surface, cools and solidifies almost instantly when it is exposed to the relatively cool temperature of the atmosphere. Quick cooling means that mineral crystals don't have much time to grow, so these rocks have a very fine-grained or even glassy texture. Hot gas bubbles are often trapped in the quenched lava, forming a bubbly, vesicular texture. Pumice, obsidian, and basalt are all extrusive igneous rocks. The cinder cone above and the close up at right are made of basalt. Intrusive igneous rock Intrusive, or plutonic igneous rock forms when magma is trapped deep inside the Earth. Great globs of molten rock rise toward the surface. Some of the magma may feed volcanoes on the Earth’s surface, but most remains trapped below, where it cools very slowly over many thousands or millions of years until it solidifies. Slow cooling means the individual mineral grains have a very long time to grow, so they grow to a relatively large size. Intrusive rocks have a coarse grained texture. The image at right shows granite, an intrusive igneous rock. Samples of Igneous rock Volcanic rock Igneous rock that cools and solidifies at or very near the Earth’s surface. Volcanoes produce volcanic rock. Granite A coarse-grained intrusive igneous rock with at least 65% silica. Quartz, plagioclase feldspar and potassium feldspar make up most of the rock and give it a fairly light color. Granite has more potassium feldspar than plagioclase feldspar. Usually with biotite, but also may have hornblende. Lava Magma that reaches the Earth’s surface through a volcanic eruption. When cooled and solidified, forms extrusive (volcanic) igneous rock. Pegmatite A very coarse-grained igneous rock, commonly with a granitic composition. Usually forms from molten rock rich in water or other volatiles that facilitate the growth of large crystals. Forms sills and dikes. Sedimentary Rocks Sedimentary rocks are formed from pre-existing rocks or pieces of once-living organisms. They form from deposits that accumulate on the Earth’s surface. Sedimentary rocks often have distinctive layering or bedding. Many of the picturesque views of the desert southwest show mesas and arches made of layered sedimentary rock. Clastic sedimentary rock Clastic sedimentary rocks are the group of rocks most people think of when they think of sedimentary rocks. Clastic sedimentary rocks are made up of pieces (clasts) of preexisting rocks. Pieces of rock are loosened by weathering, and then transported to some basin or depression where sediment is trapped. If the sediment is buried deeply, it becomes compacted and cemented, forming sedimentary rock. Clastic sedimentary rocks may have particles ranging in size from microscopic clay to huge boulders. Their names are based on their clast or grain size. The smallest grains are called clay, then silt, then sand. Grains larger that 2 millimeters are called pebbles. Shale is a rock made mostly of clay, siltstone is made up of silt-sized grains, sandstone is made of sand-sized clasts, and conglomerate is made of pebbles surrounded by a matrix of sand or mud. Biologic sedimentary rock Biologic sedimentary rocks form when large numbers of living things die, pile up, and are compressed and cemented to form rock. Accumulated carbon-rich plant material may form coal. Deposits made mostly of animal shells may form limestone, coquina, or chert. Chemical sedimentary rock Chemical sedimentary rocks are formed by chemical precipitation. The stalactites and stalagmites you see in caves form this way, so does the rock salt that table salt comes from. This process begins when water traveling through rock dissolves some of the minerals, carrying them away from their source. Eventually these minerals can be redeposited, or precipitated, when the water evaporates away or when the water becomes over- saturated with minerals. Samples of sedimentary rock Sandstone Sedimentary rock made mostly of sand-sized grains. Shale Sedimentary rock derived from mud. Commonly finely laminated (bedded). Particles in shale are commonly clay minerals mixed with tiny grains of quartz eroded from preexisting rocks. Shaley means like a shale or having some shale component, as in shaley sandstone. Bedding Sedimentary layers in a rock. The beds are distinguished from each other by grain size and composition, such as in shale and sandstone. Subtle changes, such as beds richer in iron-oxide, help distinguish bedding. Most beds are deposited essentially horizontally. Chert A very fine-grained sedimentary rock made of quartz. Usually made of millions of globular siliceous skeletons of tiny marine plankton called radiolarians. Black chert is called flint. Metamorphic Rocks Metamorphic rocks started out as some other type of rock, but have been substantially changed from their original igneous, sedimentary, or earlier metamorphic form. Metamorphic rocks form when rocks are subjected to high heat, high pressure, hot, mineral-rich fluids or, more commonly, some combination of these factors. Conditions like these are found deep within the Earth or where tectonic plates meet. In metamorphic rocks some or all of the minerals in the original rock are replaced, atom by atom, to form new minerals. It’s not hard to see that this metamorphic rock, called gneiss, has been intensely folded! This rock had to have been under very high pressure and temperature to allow it to fold like this without breaking. Photo by Edward P. Klimasauskas, USGS. Metamorphic rocks are often squished, smeared out, and folded. Despite these uncomfortable conditions, metamorphic rocks do not get hot enough to melt, or they would become igneous rocks! Foliated metamorphic rock Foliation forms when pressure squeezes the flat or elongate minerals within a rock so they become aligned. These rocks develop a platy or sheet-like structure that reflects the direction that pressure was applied in. Slate, schist, and gneiss (pronounced 'nice') are all foliated metamorphic rocks. Non-foliated metamorphic rock Non-foliated metamorphic rocks do not have a platy or sheet-like structure. There are several ways that non-foliated rocks can be produced. Some rocks, such as limestone are made of minerals that are not flat or elongate. No matter how much pressure you apply, the grains will not align! Another type of metamorphism, contact metamorphism, occurs when hot igneous rock intrudes into some pre-existing rock. The pre-existing rock is essentially baked by the heat, changing the mineral structure of the rock without addition of pressure. Samples of metamorphic rocks Schist Metamorphic rock usually derived from fine-grained sedimentary rock such as shale. Individual minerals in schist have grown during metamorphism so that they are easily visible to the naked eye. Schists are named for their mineral constituents. For example, mica schist is conspicuously rich in mica such as biotite or muscovite. Source - US Geological Survey Western Earth Surface Processes Team and the National Park Service. http://www.desertusa.com/geofacts/rocks_igne.html Mineral - A mineral is a naturally occurring, inorganic, crytalline solid, that has a definite chemical composition, and is stable over a range of temperatures and pressures. Example - Quartz is a mineral, it is found in nature, it forms without the help of plants and animals, it is crystalline, and it has a definite chemical composition (SiO2, two oxygen atoms for every one silicon atom). It is stable, both at low and high temperatures, but is unstable at very high temperatures ( > 600 C). It is stable at low to moderate pressures and is unstable at high pressures (equivalent to burial many tens of kilometers deep). Another common mineral is feldspar. Rock - A rock is an aggregate (a combination) of one or more minerals. It may be igneous, sedimentary or metamorphic. Example - A mixture of crytals of quartz and feldspar is a rock called granite. Granite may also have other minerals such as micas, pyroxene, and amphiboles in lesser amounts, as well as many others in trace quantities. Although there are over 4000 different minerals and hundreds of rock types, there are only about 8 common minerals and 20 common rocks found at the Earth's surface. This makes it relatively easy to learn how to recognize the vast majority of minerals & rocks that you will ever see. All it takes is a little practice. The most common minerals are: quartz, potassium feldspar, plagioclase feldspar, olivine, pyroxene, amphibole, mica, and calcite. The most common igneous rocks are: rhyolite, granite, andesite, diorite, basalt, gabbro, peridotite, obsidian, pumice, and scoria. The most common sedimentary rocks are: shale, sandstone, conglomerate, limestone, and tillite. The most common metamorphic rocks are: slate, phyllite, schist, gneiss, marble, and quartzite. http://www.casdn.neu.edu/~geology/department/staff/colgan/iceland/rocks.htm Rocks and Minerals Id Lab Teacher Notes PA Standards: Science and Technology Standards 3.5 Earth Sciences: Describe earth features and processes 3.5.7 A Describe the processes involved in the creation of geologic features (rock cycle) Explain how the rock cycle affected rock formation in the state of PA. 3.5.10A Describe and identify major types of rocks and minerals 3.2 Inquiry and Design 3.2.7 B Apply process knowledge to make and interpret observations Measure materials using a variety of scales Design controlled experiments Lab Time: This laboratory assignment will usually take at least two days and up to four days. It can be broken into the different rock types such as igneous, sedimentary and metamorphic of three separate labs of one or two days each. Preparations: Students should wear eye protection (safety glasses) when dealing with chemicals. Surfaces will become dirty and dusty when dealing with rocks. Table tops should be cleaned routinely to avoid damage to clothing. Considerations/Students should already know: Students should be familiar with the rock cycle and the processes by which rocks are formed. Students should know the meaning of the vocabulary words.