Date: - 20-10 -2004 OM-GEN- Introduction To Cryogenic Instrumentation in SM18 Prepared by – Prashant K. Awale and Bangalore Arunkumar, BARC Department of Atomic Energy, India Operation Methods & other General Documents are used for testing the LHC Magnets in Cryogenic Conditions in building 2173 (SM18) and are the working documents produced for that purpose only. These Methods are step-by-step procedures that may be followed by the Shift Operators of SM 18 for carrying out different power- tests of the super-conducting magnets. Index / Contents Chapter No Chapter Name Page No. 1. Introduction to Cryogenic Instrumentation ………………03–06 2. Sensors used in SM18 Cryogenic system ………………07-09 3. Temperature Instrumentation ……………………………10-17 4. Flow Instruments ……………………………………….17-18 5. Level Instrumentation ……………………………………19 6. 13 KA Current lead Instrumentation ……………………..20 7. Cryo OK for 1.9K/4.2K/HV@ Cold ……………………...21 8. References ………………………………………………...21 9. Acknowledgement ………………………………………..21 2 Chapter 1 //Introduction to Cryogenic Instrumentation// Abstract: Cryogenic Instrumentation is the vast and unique filed of measurement and is one of the many challenges for the cryogenic system of SM18 magnet test facility as well as for LHC. This write-up/document is written in order to understand the cryogenic instrumentation aspects pertaining to SM18 magnet test facility and also addressed is some of the low temperature instrumentation aspects both for LHC as well as for SM18. Study of various low temperature instrumentation sensors conducted by the experts from CERN is also discussed here in brief. Also enclosed here is the list of various instruments and sensors (along with their range, make and location) that are being use in cryogenic system of SM18 magnet test facility. TT821 Cernox temperature sensor that is installed in each magnet is also discussed. Introduction: For testing of approximately 1800 superconducting magnets for the LHC machine at CERN prior to their installation inside LHC tunnel, an extensive Magnet testing set up is available in SM18. This set up comprises of total 6 test clusters with 2 test benches per cluster. i.e. overall 12 test benches are available in SM18 and all this test benches are in operation. Magnets are subjected to both warm as well as cold tests. For cold tests these magnets are cooled down to 1.9K. For the controlled cool down and warm up of these magnets, an extensive cryogenic system is installed and is in operation in SM18 (1) (Refer reference 1 “Cryogenic Infrastructure for Testing of LHC Series Superconducting Magnets” further details). This document/write-up is written in order to understand the Cryogenic Instrumentation aspects pertaining to SM18 Magnet test facility. Cryogenic instrumentation may be regarded as a unique field of measurement requiring the development of new techniques. It should be considered a separate field of effort because of increasingly higher accuracies required (like in case of cryogenic temperature control at 1.9K for LHC), the inherent remoteness of the measurements and the peculiarities of the cryogenic fluids themselves. The latter consideration is among the strongest in setting cryogenic instrumentation apart. In addition to the obvious characteristics of low boiling points, cryogenic fluids are characterized by extremely low heat of vaporisation. Cryogenic fluids like liquid helium require much less energy for vaporisation. The combination of low boiling point and low heat of vaporisation increases the possibility that the cryogenic fluid will become boiling, two phase system. The influence this has on pumping, liquid density and level determination is quite obvious. Any sensor adding energy to the system is in fact creating a vapour/liquid interface at the very point of measurement. An added consequence is that when the system is at equilibrium in the two phase region, the measurement of both temperature and pressure is redundant because the system has only one degree of freedom. (2) (e.g. TT 147 and PT147 in CFB / SSL test at 4.2K with helium pressure of 1350millibar). 3 Instrumentation for the cryogenic system of LHC is one of the many challenges and most of these is overcome by rigorous research and development, proper design, selection of commercially available instruments and then tailoring it to meet the actual system requirements. Instrumentation plays a major role in terms of monitoring the healthiness of the process, measurements of various process parameters (like Temperature, Pressure, Flow, Level, Conductivity etc.), controlling the desired process parameter within the specified set limits and to take care of the safety aspects in case of control failure (e.g. Safety relief valves etc). For these type of critical cryogenic applications, a huge number of cryogenic probes are required and some of the important features these probes must have for the trouble free operation of the system are: Good accuracy, repeatability, long term stability (i.e. to keep the specifications over the lifetime of the equipment and under its environmental conditions), maintenance free with very very high MTBF so that the probe can last till the life time of the equipment, rugged as far as possible and most important is to withstand all the extreme process and ambient conditions like cryogenic temperature of around 1.8K, Magnetic field of the order of 9 tesla (wherever applicable), ionising radiation field and temperature and pressure cycling. Over and above this “Redundancy and Diversity” are the principles employed in instrumentation design, especially wherever accidents and failures are envisaged due to pressure build up etc. e.g. Multiple safety devices (for relieving the excess pressure build up) are installed in a single header where pressure build may take place due to quenching of magnets etc. From diversity point of view, Bursting Discs (Rupture discs) are also provided in parallel. Before going to instrumentation aspects, it is good to know the SM18 cryogenic process. (3) (refer to Basic Cryogenic Document- Cryogenics for LHC Dipole prepared by Mr Uttam Bhunia- Reference #3). Refer below the block diagram of the cryogenic system layout for SM18 (Fig#1) Liquid Super fluid helium is used to cool magnets to 1.9K as helium is the only gas that makes a good super-fluid due to its very weak intermolecular forces. Helium condenses to liquid at 4.2 K and turns into super-fluid at 2.17 K. Super-fluid helium has very high thermal conductivity and hence is a very good coolant, has very low coefficient of viscosity and can penetrate tiny cracks, deep inside the magnet coils to absorb any generated heat. As seen from the Cryogenic system layout below, total 12 CFB’s (Cryogenic Feed Box) are installed between Cooldown Warmup line (CWL) and Cryogenic Compound Line (CCL). This CFB is a system that enables a superconducting magnet to be completely connected up, cooled to 1.9K and maintained at that temperature whilst the magnet performance is being tested. As cryogenic Instrumentation is the vast field and therefore this write up/document talks mostly of low temperature measurement techniques that were studied and implemented in CERN for LHC / SM18 operations as well as the cryogenic system level and flow measurements. Also discussed in brief about the various instruments those are used in SM18 cryogenic system. 4 Fig#1: Block diagram of the cryogenic system layout for SM18: COMP 1 CWU 2 C only COMP 3 (2005) COMP 2 HP GHe Heater 30 kW LP GHe Heater 200 kW CWU 1 C only COOLDOWN-WARMUP SYSTEM (CWS) 2 GHe compressors 100g/s 2-12 bar LN2 distribution 2 Cooldown Units 120 g/s (2x140 kW) 1 LPGHe Heater 200 kW 1 HPGHe Heater 30 kW - Cooldown Warmup Line, 12 valve boxes (CWL) CFB CFB CFB CFB CFB CFB CFB CFB CFB CFB CFB CFB Cryogenic Compound Line, 12 valve boxes (CCL) WPU 1 Other Utilities required for Magnet Tests WPU 2 GHe Recovery GHe GHe 40 bar GN2 LN2 LHe GHe <90 K GHe INTERFACES WITH CRYOGENIC FACILITIES OF ZONE 18 Heater 1 30 kW Heater 2 30 kW CCU2 Linde CCU 1 (IHI) (2005) GHe PUMPING SYSTEM 5 Fig.2 Actual magnet cooling circuit for power test (Courtesy: Cryo-operation group, SM18) ……………………………………………………………… 6 Chapter 2 List of some of the important Sensors used in SM18 Cryogenic system: (Refer Figure# 2) Table#1 Temperature sensors Sl. Sensor Parameter Range Location Make No No. and Type 1 TT821 Temperature inside magnet 1.6 to 300K Inside magnet on SS collar In CFB on line M2 2 TE147 1.4 to 2.4K 3 TE148 Temp on line M2 (Temp. refered for Cryo OK of 1.9K) Temp. on line M2 0 to 20K In CFB on line M2 4 TE149 I/L temp of magnet in CFB 1.6 to 100K In CFB on line N 5 TE150A O/L temp. of magnet on line M2 in CFB 73K to 300K In CFB on line M2 6 TE150B O/L temp. of magnet on line M2 in CFB 1.6 to 100K In CFB on line M2 7 TE103 Temp in CFB on line E 73K to 300K In CFB on line E 8 TE161 He. Gas temp 73K to 300K 9 TE130A,B 20K to 300K 10 TE129 Temp of 13KA current leads Temp at the bottom of CL On line coming from CWS to CFB On CL 20K to 300K On CL CERNOX™ (CX) Helium 3 bulb Vapor Pressure, Ingovi make. Carbon Resistance (CRT), AB make Resistance carbon glass (Lake shore ref: CGR-11000-1). Pt100 Class#A RTD, Make ABB Automation Resistance carbon glass (Lake shore ref: CGR-11000-1). Pt100 Class#A RTD, Make ABB Automation -do- -do-do- 7 Pressure Instrumentation Sl. No Sensor No. Parameter Range Location Make and Type 1 PT147 0 to 300mbar 2 PT102 Pr. Of helium bulb on line M2 Helium pr. At CFB Top CFB (Refer TE147). CFB 3 PT121 Helium Guard Pressure 0 to 2 bar 4 PT142 0 to 60mbar 5 PT143 0 to 2 bar -do- -do- 6 PT151 0 to 5 bar CFB -do- 7 PT162 0 to 20 bar CFB -do- 8 PT181A Pr Upstream of FV142 Pr Upstream of FV143 On BP return line to CWS Helium pr. At CFB Top Pr. In Vacuum vessel Inside Helium gaurd -do- Druck LPX2380 SPL. Rosemount Model:3051 TA2A2B21 CQ4 -do- 9 PT181B -do- Vacuum (10-10 mbar to 1 bar) 0 to 1 bar Top platform of CFB -do- 10 PE126 Pr(Vacuum) downstream of valve FV126 0 to 1 bar -do- 11 PT127 0 to 1 bar -do- 12 PE182 Pr. (vacuum) upstream of FV127 Turbo Pump P002 suction pr.(vacuum) Inficon, pirani/penni ng gauge Rosemount Model:3051 TA1A2B21 CQ4 Inficon (vacuum) Type:PSG 400 (ref: 350-000) -do- - -do- Ingovi, vacuum. 14 PDT239 0 to 80mbar -do- Rosemount Model; 3051CD2A0 2A1CS5Q4 15 PDT265 ΔP across FE239 (warm He gas flow from CWS) ΔP across FE265 (cold He gas flow from CWS) 0 to 300mbar -do- -do- 16 PT185 0 to 2 bar -do- 8 Flow Instrumentation 1 FT239 2 FT265 3 FT136A/B 4 5 FT160 FT145 Warm helium gas flow in CFB from CWS Cold helium gas flow in CFB from CWS He. Gas mass flow for cooling the resistive upper section of current leads 0 to 100gm/sec In CWS -do- -do- - On CFB top plarform Brooks mass flowmeter ref: 5863 -do -doNot in use Liquid He. Flow in the magnet for cooling to 1.9K Differential head type V- Cone meter -do- Level Instrumentation 1 LE100A Liquid Helium level in CFB Helium vessel Lact = 300mm Inside CFB AMI make, Superconducti ng Nb-Ti level sensor. Φ = 6.35mm 2 3 LE100B LE140 -doLact = 85mm -do-do- -do-do- 4 LE148 -doLiquid helium level in X+Y line. Liquid helium level in line M2. Lact = 40mm -do -do- Most of the Important Cryo Valves (e.g. CV145,CV150,CV103,CV104..) are of Velan make Model: SCGR-DN 6-32. Most of the security (safety valves- Pressure relief valves) are of Circle Seal controls Corona, California make. Helium gas leak detector used for detecting the helium leak if any from the system is of Pfeiffer make. ...................................................................................................... 9 Chapter 3 Temperature Instrumentation: Temperature measurement is a key issue in the Large Hadron Collider (LHC), as it will be used to regulate the cooling of the superconducting magnets. The compromise between available cooling power and the coil superconducting characteristics leads to a restricted temperature control band, around 1.9 K. The various components of the LHC cryogenic system work at temperatures from ambient down to 1.6 K. Depending on the actual temperature value, different accuracies are required on its measurement. Between 300 K and 25 K, an uncertainty of 5 K can be tolerated to monitor the warmer components and the general cooldown. However, at the nominal operation of superconducting magnets (below 2.2 K, i.e. at 1.9K) only 10 mK inaccuracy is allowed, to give enough room for the regulation band of the cryogenic controller, while avoiding magnet quench and minimizing the cooling effort of the cryogenic system. Table 2 below shows the allowed uncertainty on temperature measurement. The aimed resolution has to be ten times better than the overall accuracy (dT < 1mK, below 2.2 K temperature measurement on the LHC machine).(4) Table#2: Required overall Temp. accuracy and resolution: Temperature Span (K) Accuracy (mK) Resolution (mK) 1.6 to 2.2 10 1 2.2 to 4.0 20 2 4.0 to 6.0 30 3 6.0 to 25 1000 100 25 to 300 5000 500 Also, the accuracy budget is to be evenly shared between the sensor and the signal conditioning. CERN has done extensive and elaborate study of various temperature sensors available for cryogenic temperature measurements like CERNOX TM (CX), TVO, RhFe (Rhodium Iron Resistance Temperature Detector), AllenBradley(AB) carbon resistor, Pt100 (Platinum RTD with 100 Ω resistance at 0◦C) etc. Other temperature sensors that are available for low temperature measurements are Silicon diodes, germanium sensors, helium three isotope gas bulb vapor pressure measurement etc. The various guidelines for selection and usage were: 1. 2. 3. 4. 5. 6. 7. 8. 9. Single sensor covering full temperature range from 1.6K to 300K. Sensor should be able to withstand the thermal and pressure cycling. High magnetic field environment ( around 9 teslas). Radiation field. Accuracy (inclusive of signal conditioning electronics and hardware) shall be better then the required specification as mentioned in Table#1 above. very good long term stability and very very low long term drifts. Maintenance free as most of these sensors will be inaccessible while the system is in operation. Very good sensitivity specifically at low temperatures (around 1.9K). self heating effect… 10 CERNOX™ (CX), TVO® and RhFe listed above cover the full temperature range with a single sensor. AllenBradley® (AB) and Pt100 can be combined to cover respectively low and high temperature scales, or used alone in applications not requiring full range measurements. In terms of resistive values, CERNOX (CX’s) span is the largest among all sensors (3 decades), requiring wide dynamic range signal conditioning. Also covering the whole temperature range, RhFe spans over only 2 decades of resistance, with the advantage of less demanding dynamic range, but with the consequence of limited sensitivity. Sensors with negative dR/dT, like CX, TVO® and AB, show high resistance and high sensitivity (dR/R / dT/T) at low temperatures, where measurement accuracy has to be at its best. This semiconductor behavior relaxes the constraints on signal conditioner accuracy for low temperature measurement. On the other hand, at low temperature metallic sensors like RhFe exhibit a sensitivity one order of magnitude worse, demanding much more accurate signal conditioning. Typical characteristics of cryogenic temperature sensors Sensor type T Span (K) R Span (Ω) dR/dT (Ω/K) (dR/dT)/(dT/T) CERNOX(CX) 1.6 to 300 30000 to 30 -40000 to -0.1 -2.7 to -1.0 TVO 1.6 to 300 9000 to 900 -7000 to -0.7 -1.3 to -0.2 RhFe 1.6 to 300 6 to 110 +0.7 to +0.4 +0.2 to +1.0 AB 1.6 to 100 10000 to 100 -12000 to -0.3 -3.0 to -0.2 Pt100 73 to 300 18 to 110 + 0.4 to +0.4 +2.0 to +1.0 Of almost all the sensors mentioned above, CERNOX™ (CX) is the sensor best suited for LHC application. CERNOX™ (CX) temperature sensor possess many attributes desirable in a temperature sensor for LHC type of project application including high sensitivity, excellent short- term and long term stability, small physical size, fast thermal response and very very low calibration drifts (almost negligible) when exposed to magnetic fields and ionizing radiation. Details of this sensor is discussed in following sections: TT821: TT821 is CERNOX TM (CX) temperature sensor manufactured by M/s Lakeshore. Sensor Model No: XCX-1050-SD-30 and is referred as Short Thermometer. This sensor is used to monitor magnets internal temperature and same is mounted inside the magnet on the SS nonmagnetic collars. For proper mounting of the sensor, a support block made out of PCB (developed by CERN) is used. CERNOX sensor is push fit mounted in a groove provided in this short thermometer block. The 4 lead wires of the CERNOX sensor are soldered to the 4 soldering points provided on the block. This block is then screwed on the SS collar inside magnet and a polymide foil is sandwiched between thermometer and mounting surface to avoid electrical damage of the sensor in case the surface is under high electrical potential. (5). 11 There is one drawback of this sensor.i.e. these sensors are not directly interchangeable. Because each individual sensor has it’s own specific calibration curve, it is strictly forbidden to interchange thermometers. Each thermometer has got its own fit and coefficients and same is available in MTF for the corresponding magnets. The resistance of this temperature sensor is measured by four wire technique in order to get rid of lead wire resistances. Therefore, a 4 –wire twisted thermometer cable is soldered to the thermometer. To minimalise heat flow from ambient environment to the sensor by conduction of electrical leads, thin wires are used ( silver plated copper wires of AWG30 with polyimide insulation with ρ(300K) of 0.32 Ω/m is used). Stress on these thin wires is avoided by more robust extension wires, which are mechanically fixed (i.e. by a knot) close to the connector. Extension wires are also silver plated copper wires of AWG24 with polyolefine insulation and ρ(300K) of 0.07Ω/m. Fig#4: installation of TT821 (Cernox) inside magnet- wiring methodology. What is CERNOX™ (CX) ? (8) The “CERNOX™ (CX)” temperature-sensing element is used in the magnet assembly (TT821). “CERNOX™ (CX)” (short for Ceramic Nitride-Oxide) is a thin film resistance temperature sensor commercialized by M/s Lakeshore Cryotronics,Inc. The sensor is fabricated from zirconium reactively sputtered in a nitrogen-oxygen atmosphere. The resulting thin film is comprised of conducting zirconium nitride embedded within a zirconium oxide non conducting matrix. This material has a negative temperature coefficient of resistance making it useful as a temperature sensor. To tailor the sensor to a given temperature range the ratio of conducting to non conducting material is varied. The main advantage is a single device can be fabricated for use from below 0.3 K to 420 K. Cernox temperature sensors also possess many attributes desirable in a temperature sensor including high sensitivity, excellent short-term and long-term stability, small physical size, fast thermal response and small calibration shifts when exposed to magnetic fields or ionizing radiation. It should be noted that each fabricated sensor has a typical characteristic polynomial curve. The typical resistance values are around 45000 Ohms at 1.6K and around 60 Ohms at Room temperature (300K). Each sensor that is used in magnet is independently and individually calibrated in a lab. and its coefficients (fit) are made available for future reference. Coefficients are normally stored in MTF in components folder under the corresponding magnet in 12 which this particular sensor is going to be used. Typical curve fit equation for a Cernox sensor is: T = 10 ^∑{A(i) x [1/log10I] ^i }, where i = 0,…..,9 and A(i) are coefficients. R is resistance in Ohms and T is temperature in K. e.g.: For a Cernox thermometer calibrated in a lab following are the typical observations: Thermometer CX_LS_X09273. Range: 1.615725 to 290.5813K. (Table# 6) Coefficients: A(0) 41.44669 A(1) -1192.59 A(2) 14621.59 A(3) -101618 A(4) 443679.2 A(5) -1262277 A(6) 2342678 A(7) -2739332 A(8) 1834192 A(9) -536570 Fig# 5: Resistance as a function of temperature for CERNOX family of temperature sensors: Stability: Stability is one of the most important characteristics for a temperature sensor. Short term stability for Cernox sensors is tested during manufacturing and is found to be better than ± 3 mK repeatability at 4.2 k upon repeated thermal cycling. Long term stability data is available in terms of “ Mean deviation from original calibration after 5.8 years as a function of temperature for 39 Cernox sensors chosen. At temperature of 1.4 K, the mean deviation was + 0.05 milliKelvin and at 4.2K temperature the mean deviation observed was -0.17K. For checking the effects of radiation effects on these Cernox sensors (Prior to their selection for LHC Project), experts and researchers at CERN has thoroughly investigated the radiation tolerance of Cernox temperature sensors. In one study, 66 Cernox sensors at 1.8 K were irradiated with neutrons to total fluences of 3 x 1014 13 n/cm2 to 1 x 1015 n/cm2. The mean calibration shift at 1.8K was +1mK. No signs of thermal annealing were observed. In a second experiment, cernox temperature sensors from two different lots were irradiated at 4.2 K by a neutron source to a total fluence of normally 1 x 1015 n/cm2. Sensors within each lot behaved in a similar manner. The first set had the lower sensitivity and showed a continually decreasing resistance throughout the irradiation with an equivalent temperature variation of 4mK. At 4.2K. The resistance of the second set initially increased slightly and then decreased showing an equivalent temperature variation of about 2.5mK. These data evidence the cernox’s insensitivity to radiation. Signal Conditioning for Cernox Temeprature sensor: In order to meet the stringent accuracy requirements, experts at CERN had explored all the possibilities of various signal conditioning circuits that can be used like Logarthmic conditioner, Linear Multirange conditioner etc. The Linear multi-range conditioner was found to be satisfying all the accuracy requirements. Figure #7 below shows the front end block diagram of this signal conditioning circuit.. It is well known that self heating effects cannot be neglected when using resistive type sensors at low temperatures and hence they impose the use of relatively low exitation currents. Therefore, the input span of 30 Ohms to 30 Kohms for this cernox sensor is divided into three parts (3 decades) so that the sensing current is kept lower for high R values therby reducing the self heating of the sensor, and higher for small R values, increasing the voltage developed at the sensor and its signal to noise ratio. Refer Table# 7 . (4) Table# 7 Resistance (Ω) Current (µA) Typical Temperature (K) 30 to 300 100 50 to 300 290 to 3000 10 5 to 50 2900 to 30000 1 1.5 to 6 The front end design is based on comparison bridges in which the comparison signal is generated by means of a radiation hard reference resistor. This reference resistor is a high accuracy (0.01%) and low thermal drift (10ppm/K) thick film NiCr metallic resistor. Refer figure below. This comparison bridge permits to compensate variations in excitation current supply and variations in amplifier gain. In order to get rid of thermoelectric/thermocouple voltages AC measuring technique (current inversion – bipolar sensing current, oscillating at 2 Hz) is used. Amplifier offset is compensated by means of the inverting switch at the front end amplifier input. Voltage developed across the reference resistor and the Cernox temperature sensor is measured in order to compute the R value and thereby the temperature as sensed by Cernox sensor. { R = (V/Vref) * Rref.} where V is the voltage measured across the sensor, Vref is the voltage developed across the reference resistor, Rref is the value of reference resistance and is a known constant and R is the sensor resistance. The actual temperature value is computed by inserting this R value in the Curve fit equation for the cernox sensor (for which coefficients were obtained at the time actual temperature calibration). 14 Fig: 7. Signal conditioning front end for Cernox tempetaure sensor. The signal conditioning circuit shown above is the one that will be used for LHC. One which is used in SM 18 Magnet test set up is more or less same but with minor differences. Instead of field bus output, the one used in SM18 has two types of out puts, i.e. 1)0 to 10V DC analog output as the signal corresponding to the resistance value and 0 to 6V DC as the out put corresponding to Range of resistance that is being measured. 2) 4 to 20mA DC analog output as the signal corresponding to the resistance value and 2 bit digital value indicating the Range of resistance that is being measured. Out of these two available options, the second one is used in SM18. The 0 to 10V DC output and 0 to 6V values for indicating range is fed to a LF data acquisition system for further computations and indication of the actual temperature value. Redundancy of TT821: Each magnet is provided with only one TT821 Cernox temperature sensor. The total cost for each Cernox sensor inclusive of the calibration cost works out to be much higher and hence its not economical to have back up sensor in the magnet. Then how about redundancy? What happens when this sensor fails? If sensor fails when in use in LHC, the back up to this will be available from the adjacent (previous or next) magnets TT821 (cernox) temperature indication. Thus the redundancy aspect is taken care of. TE147 is a Helium 3 bulb Vapor Pressure temperature sensor. The pressure exerted by a saturated helium vapor in equilibrium with its liquid is a very definite function of temperature and same principle is used to measure the temperature of the liquid helium in line M2. This temperature indication is also used to check whether the 1.9K cryo OK condition has come or not. The most common form of vapor pressure equation are : LogP = A + B/(C + T) where A, B and C are the coefficients and are constant. T is the temperature and P is the pressure. For temperature measurement, this helium vapor pressure bulb is inserted in the helium line whose temp is to be monitored and 15 the pressure generated by this filled bulb system is monitored in order to compute the corresponding temperature. This helium vapor pressure is monitored by using Druck make absolute pressure transmitter LPX2380 SPL. TE-149 and TE150B: Sensor :Resistance Carbon Glass manufacturd by M/s LakeshoreRef:CGR-1-1000-1. Carbon-Glass RTDs (CGRs) have the longest history of use of any sensor suitable for high magnetic fields and wide range temperature sensing. These resistance temperature sensors are highly reproducible and can be used from 1.4 K to 100 K and in magnetic fields up to 20 tesla. Their extremely high sensitivity at liquid helium temperatures makes them very useful for submillikelvin control below 10 K. CGR sensors are monotonic in resistance temperature characteristic between 1.4 K and 325 K, but their reduced sensitivity (≈0.01 /K) above 100 K limits their usage at higher temperatures. Features: Low magnetic field induced errors For use in magnetic fields up to 20 tesla Reproducible in the 1.4 K to 100 K range Monotonic R vs. T and dR/dT vs. T response curves High sensitivity provides submillikelvin control at 4.2 K and below Usable sensitivity over the broad range of 1.4 K to 325 K Good resistance to ionizing radiation at low temperatures Typical Carbon-Glass Resistance Values Typical Carbon-Glass Sensitivity Values Typical Carbon-Glass Dimensionless Sensitivity Values Fig# 8 TE 148: (Carbon Resistance Thermometer- CRT): This is the Carbon resistance thermometer and is referred as CRT. The one used here and for LHC is “AllenBradley (AB) make” Model CRT_AB(100 Ω, 1/8 watt). CRT has high sensitivity at 16 low temperatures and it is one of the low cost sensor. This particular sensor is most suitable for temperature range below 20K. At higher temperature it has decreasing sensitivity, stability problems and also competition with the metallic resistors like platinum(Pt) etc. The CRT sensors have NTC. The typical interpolation equation that fits the data in 2K to 20K range is: [(LogR)/T]1/2 = A + BLogR, Where, R is the resistance at temperature “T” and A,B are the experimentally determined constants. {e.g.: A typical 0.5Watt, 220Ω resistance will measure roughly 1KΩ at 1K, 20KΩ at 0.1k and 300KΩ at 0.015K.} ………………………………………………………………………………………….. Chapter 4 Flow instruments— a) Thermal mass flow meter is mainly used for low gases flow rates at ambient temperature. (Brooks make mass flow meter) b) Large liquid flows at very cold temperature are measured by drop in level method by “Hot Superconductor Wire”. The principle of level measurement is described under level heading. c) Large gas flows are measured by V-cone meters. The differential head developed in the V- cone is measured by standard industrial differential pressure transmitter. FT239 (Warm helium gas flow in CFB from CWS) and FT265 (Cold helium gas flow in CFB from CWS): (Fig# 9). These flows are measured by V- Cone (√CONE) meters Model VB. V – Cone meter is a differential pressure type flow measurement device. A SS cone is positioned in the center of the pipe to increase the velocity of the flowing fluid and create a differential pressure across the two taps (P1 and P2 as shown in fig below). This differential pressure generated is measured using “FisherRosemount make, Model 3051TA2A2B21CQ4, smart differential pressure transmitter. The output of this transmitter is 4 to 20mA DC linear output and is fed to PLC for further computation of the flow. The flow ‘Q’ and ‘∆P’ has a square root relationship, i.e. Q = K √∆P. (PT239 and PT265). The accuracy for this V cone meter is ± 0.5% of flow rate and repeatability is of the order of ±0.1%. The turn down ratio is 10:1. It may be noted that like other differential pressure flow measuring instruments ( Orifice plates, Venturies etc), this V-cone is also sized for the intended application. The V-Cone meters has many advantages as compared to other traditional instruments like Orifice plates and those are: 1) V cone can measure almost all process fluids like liquids, slurries, gases and steam. 2) Short straight run requirements hence making it much effective from space utilization point of view as well as from cost saving point of view for the 17 3) 4) entire plant. (Typically 0 to 3 diameters upstream and 0 to 1 diameters downstream). Low permanent pressure loss. Durable against wear and sticking as the V-cone because of its design has a unique self cleaning capability as the fluid runs of from the beta edge of the cone. Fig:9 :V-cone flow meter. Flow Instrumentation for Water cooled cables: Flow through water cooled High current power cables is monitored by Eletta (Sweden) make Differential pressure type Indicator cum flow switch. This flowmeter is mounted on the return line. The Eletta Flow Monitor is based on the proven and dependable differential pressure principle, using interchangeable orifice plates for different measuring ranges. The Flow Monitors are working with differential pressure ranges, i.e. 50 – 200 mbar for Type S2-FSS26 and the accuracy specified is ± 5% of FS. The Instrument consists of two parts mainly i.e. the Pipe Section and the Control Unit. The Pipe Section is the part that is mounted in the process pipe and the Control Unit is mounted directly (standard) or remote on/to the Pipe Section. The Control Unit is gives the Flow information and also contains the SPDT contacts. The Control Units S02 have a local readout and is equipped with two independent adjustable alarms (micro switches) which can be set for low and high flow alarm. The readout has a scale, which shows the ordered flow range with a multiplier. The differential pressure signal generated by the orifice plate is sensed by the diaphragm and in turn moves the diaphragm linearly. This diaphragm movement is transmitted by linkages and gearing mechanism to the indicator (pointer) inside the control unit. …………………………………………………………………………………….. 18 Chapter 5 Level Instrumentation (LE100A/B, LE140, LE148): Principle of Liquid helium level measurement: This is based on “Hot wire” method of detecting the depth of the liquid. The active element of the probe is a Niobium-Titanium (NbTi) wire, whose superconductivity transition temperature is above the boiling point of liquid helium. At the start of measurement the probe is excited by a boost current, which is in excess of measuring current. This heats the top of the element & causes the normal / superconducting interface to propagate down the element. When this interface reaches the surface of the liquid, the much greater cooling power available causes the propagation to cease. This is detected & the booster current is reduced to normal measuring current. The voltage drop across the probe is a function of the depth of immersion as the effective resistive length of this NbTi wire probe changes with the depth of its immersion in liquid helium. With suitable lookup table & electronics the actual height / depth of liquid is found. LE100A/B, LE140, LE148 level elements are AMI (American Magnetics,Inc) make liquid helium level sensors. The diameter of the NbTi probe is 6.35mm and the active length for each sensor/probe depends on the application (refer Table#1). The overall length is usually 1 inch longer than the active length (0.5 inch at top and 0.5 inch at bottom).(6). The typical value of the boost current is of the order of 200mA and the measuring/sensor current is of the order of 75mA. The maximum magnetic field for which this sensor can function is 10 Tesla. Nominal sensor resistance is 4.5 ohms/cm at 20K and 5.4ohms/cm at 300K. Normally this NbTi wire has a small heater attached to initiate a resistive zone. The selection of the boost current and the measuring current is very tricky affair as large helium losses can occur if high current is left on continuously. It may please be noted that the installation of this sensor probe should be avoided where icing (frozen water ..) may occur since ice formations may cause erratic operation as ice formation may stop the propagation of the normal (resistive) zone before it actually reaches the liquid/gas interface. This may result in giving the indication of a higher helium level than it actually exists. ……………………………………………………………………………………… 19 Chapter 6 13kA Current Lead Instrumentation Fig:3: Instrumentation associated with Gaseous Helium cooling circuit for 13KA and 600Amps Current Leads. Connections of voltage taps and temperature sensors is done by Fisher connectors. (Lead body isolation voltage to earth is 2KV in helium atmosphere). The room temperature terminals are nickel plated for good electrical contact and the cold terminals are silver plated for good electrical contacts. 20 Chapter 7 Cryo O.K. For 1.9K, 4.2K and for HV @Cold: All the cryo sensor signals for Cryo O.K. at 1.9K, 4.2K and HV@Cold are highlighted in blue colour in the instruments table (Table#1). Cryo O.K. at 1.9K: Following Process conditions must be fulfilled in order to have Cryo O.K. at 1.9K: Table # 3 SL. Sensor Parameter Condition No. 1 2 TT147 LT100A 3 4 TT130 A/B LT140 5 FT136 Temp on line M2 Liquid Helium level in CFB Helium vessel 13KA current lead Liquid helium level in X+Y line He. Gas mass flow for cooling the resistive upper section of current leads <1.94K > 40% level < 300K < 20% >580mg/sec Cryo O.K. at 4.2K: Following Process conditions must be fulfilled in order to have Cryo O.K. at 4.2K: Table # 4 SL. Sensor Parameter Condition No. 1 LT100A 2 3 TT130 A/B LT148 4 FT136 Liquid Helium level in CFB Helium vessel 13KA current lead Liquid helium level in line M2 He. Gas mass flow for cooling the resistive upper section of current leads > 40% level < 300K >76% >580mg/sec Cryo O.K. for HV@ Cold : Following Process conditions must be fulfilled in order to have Cryo O.K. for HV@Cold: Table # 5 SL. Sensor Parameter Condition No. 1 2 TT130 A/B LT148 13KA current lead < 155K Liquid helium level in >76% line M2 21 Conclusion: This write up is an effort to understand some of the instrumentation aspects of the Cryogenic Instrumentation in SM18 Magnet test facility. Working principles of various instruments were also discussed. The HF/LF data acquisition system and the control philosophy is not discussed here. References: 1. Cryogenic Infrastructure for Testing of LHC Series Superconducting Magnets by J. Axensalva, V. Benda, L. Herblin, JP. Lamboy, A. Tovar-Gonzalez and B. Vullierme 2. Cryogenic Engineering by Thomas M. Flynn. 3. Basic Cryogenic document- Cryogenics for LHC dipole by Uttam Bhunia, VECC. 4. Signal Conditioning for cryogenic thermometry in LHC by J. Casas, M.A.Rodriguez Ruiz…(CERN) 5. Installation guide for LHC cryogenic Thermometers prepared by Ch. Balle, LHC/ACR. 6. Installation,Operation and maintenance Instructions for the AMI (American Magnetics Inc) liquid helium level sensor. 7. CFB Operator guide by Antonio Tovar- Gonzalez, CERN 8. Review of Cernox Thin-Film Resistance temperature sensor by S. Scott Courts and Philip R. (lake shore cryotonic Inc). Acknowledgements: We wish to extend our gratitude and thanks to Dr. Vinod Chohan for his encouragement in preparing this document. Thanks also to Shri Bruno Vullierme, Shri Jean Paul Lamboy, Shri Christoph Balle, Giorgio D’Angelo & our other colleagues who have shared valuable technical information and for their advice and guidance. 22