Author O S yntheses rganic Procedure Checklist for Authors This checklist is designed to assist authors in providing procedures that meet the criteria for consideration by Organic Syntheses. A checked box should be used to indicate that your procedure conforms to the criteria detailed in the accompanying document "Instructions to Authors.” A completed checklist should be forwarded along with the procedure at the time of submission. Scale of Procedure The scale of the procedure conforms to criteria established by Organic Syntheses. Apparatus Description A detailed description of reaction apparatus is provided. Reagents Source and purity is indicated for all starting materials and reagents. Procedure The procedure, including temperature, amount of reagents, time, appearance, method for reaction monitoring, is clearly described. Reaction Work-up Detailed procedures for quenching, extracting, and isolating the products are provided. Purification Purification methods, including distillation, chromatography, and recrystallization, are described in detail as outlined in the Instructions to Authors. Characterization Physical properties and chromatographic and analytical data are provided to establish the identity, purity, and enantiomeric purity of the products in accord with the guidelines described in the Instructions to Authors. Discussion The discussion and reference sections conform to Organic Syntheses requirements, and include the clear identification of potential hazards and a clear statement(s) regarding the disposal of hazardous waste. 1