Changes in volatile compounds produced during thua nao production Arunsri Leejeerajumnean Department of Food Science and Technology, Faculty of Engineering and Industrial Technology, Silpakorn University, Nakorn Pathom, 73000 Thailand Email: arunsri@su.ac.th Abstract Thua nao, a traditional proteolytic fermented soybean condiment in northern Thailand, was prepared from whole soybeans by natural flora fermentation. The formation of volatile compounds in thua nao during fermentation of cooked soybeans by mix culture of Bacillus was studied. Hexanal and 2pentyl furan were the main volatile compounds in cooked soybeans. After 12 h of fermentation, 3-hydroxy-2-butanone was the main volatile compound and after 24 h, butanone and 3-hydroxy-2-butanone were the most abundant volatile compounds. Following 72 h of fermentation, acids and esters (2methyl butanoate), dimethyl disulphide, pyrazines, butanone and benzaldehyde were the volatiles produced in the greatest quantities. The volatile compound in dry thua nao was a mixture of many compounds, not mainly only ketones, pyrazines and sulphur containing compounds, but also acids and esters, alsohols and aldehydes and furans. The volatlies in thua nao were different from those in natto (used in this experiment), which were mainly only pyrazines and ketones.