NZQA Expiring unit standard 2641 version 6 Page 1 of 6 Title Demonstrate knowledge of analytical measurement systems Level 4 Credits 6 Purpose People credited with this unit standard are able to demonstrate knowledge of: – pH measurement; – conductivity measurement; – dissolved oxygen measuring equipment; – stack and/or particulate monitoring equipment; – chromatography measuring equipment; – consistency and viscosity measuring equipment; – humidity measuring equipment; – density measuring equipment; and – analytical sampling systems. Classification Industrial Measurement and Control > Industrial Measurement and Control - Theory Available grade Achieved Explanatory notes This unit standard has been developed for learning and assessment off-job. Outcomes and evidence requirements Outcome 1 Demonstrate knowledge of pH measurement. Evidence requirements 1.1 The term pH and its associated scale are defined. Range 1.2 positive hydrogen ions, 14 alkaline, 3 acidic, 7 neutral, log scale. Components of a pH measuring system are identified and described. Range reference electrode, measuring electrode, temperature compensation, very high input impedance amplifier. 1.3 Operating principles of the pH measuring system are described. 1.4 Calibration methods for pH measuring systems are identified. The Skills Organisation SSB Code 100401 New Zealand Qualifications Authority 2016 NZQA Expiring unit standard Range 1.5 2641 version 6 Page 2 of 6 buffer solution, backing off unwanted e.m.f.s. Problems associated with pH measuring systems are identified. Range electrode cleaning, ultrasonic, mechanical wiping, lead wire connections, probe failure. Outcome 2 Demonstrate knowledge of conductivity measurement. Evidence requirements 2.1 Principles of conductivity measurement are described. Range 2.2 Factors taken into account when making conductivity measurements are defined. Range 2.3 siemens, micro mho, electrolyte. non-linear solution strengths, temperature compensation, probe constant. Calibration techniques are described. Range amplifier decade box injection, dedicated test equipment, standard solutions. Outcome 3 Demonstrate knowledge of dissolved oxygen measuring equipment. Evidence requirements 3.1 Principles of dissolved oxygen measurement are stated. Range galvanic cell, polarographic cell. 3.2 Air exposure at valve glands, and its prevention, is explained in relation to making dissolved oxygen measurements. 3.3 Calibration techniques are described. Range transmitter adjustment, sample 5% sodium sulphite, water saturated air. Outcome 4 Demonstrate knowledge of stack and/or particulate monitoring equipment. Evidence requirements The Skills Organisation SSB Code 100401 New Zealand Qualifications Authority 2016 NZQA Expiring unit standard 4.1 Principles of stack and/or particulate monitoring are stated. Range 4.2 dichotomous sampler particulate, infra red, zirconia probe, light attenuation/transmissiometer, Carbon Monoxide (CO), Carbon Dioxide (CO2), Nitrous Oxide (NO), particulate. Factors taken into account when making stack monitoring measurements are defined. Range 4.3 2641 version 6 Page 3 of 6 air dilution, water vapour, plant operating conditions, wet sample, dry sample. Calibration techniques are described. Range dedicated test equipment, sample. Outcome 5 Demonstrate knowledge of chromatography measuring equipment. Evidence requirements 5.1 Principles of chromatography and detectors are stated. Range 5.2 thermal conductivity, flame ionisation, carrier gas, packed column, measuring circuit. Typical measurement applications using chromatography are identified, and graphical read outs are described. Range liquid, gas, vapour samples. Outcome 6 Demonstrate knowledge of consistency and viscosity measuring equipment. Evidence requirements 6.1 Types and uses of consistency transmitters are described. Range 6.2 pulp stock, shear forces, force balance, blade type, rotating. Types and uses of viscosity transmitters are described. Range oil, liquid, rotational, capillary, float. Outcome 7 Demonstrate knowledge of humidity measuring equipment. Evidence requirements The Skills Organisation SSB Code 100401 New Zealand Qualifications Authority 2016 NZQA Expiring unit standard 7.1 Areas of application for humidity measurements are defined. Range 7.2 dew point, relative humidity, saturated solution, saturation pressure, specific humidity, hygrometer. Relative humidity is determined by using psychometric chart and hygrometer. Range 7.4 pulp and paper, powder plant. Principles and terms involved in humidity measurements are stated. Range 7.3 2641 version 6 Page 4 of 6 sling psychometer, wet-dry bulb hygrometer. Hygrometer types are described. Range chilled mirror type, surface conductivity type. Outcome 8 Demonstrate knowledge of density measuring equipment. Evidence requirements 8.1 Terms and units used in density measurement are defined, and examples are converted by calculations. Range 8.2 kilograms per cubic metre (kg/m³), relative density, specific gravity. Methods of density measurement using differential pressure transmitters are described and their applications stated. Range constant level over flow, reference wet leg, twin bubble tube. 8.3 Methods of density measurement using displacement transmitters are described and their applications stated. 8.4 Methods of density measurement using weighing of the fixed volume of product are described and their applications stated. 8.5 Methods of density measurement using nuclear radiation are described and their applications stated. 8.6 Methods of density measurement using refractometers and sonic measuring equipment are described and their applications stated. 8.7 Methods of density measurement using vibrating mass type measuring equipment are described and their applications stated. Outcome 9 Demonstrate knowledge of analytical sampling systems. The Skills Organisation SSB Code 100401 New Zealand Qualifications Authority 2016 NZQA Expiring unit standard 2641 version 6 Page 5 of 6 Evidence requirements 9.1 Steps to obtain and process an analytical sample are stated and shown in a block diagram. Range 9.2 sample taken, transport to analyser, condition sample, exhaust sample. Sampling system components are stated. Range pumps, filters, scrubbers, dryers, phase separating devices, vaporisers, heat exchangers. Replacement information This unit standard has been replaced by unit standard 28080 and unit standard 28081. This unit standard is expiring. Assessment against the standard must take place by the last date for assessment set out below. Status information and last date for assessment for superseded versions Process Version Date Last Date for Assessment Registration 1 31 October 1995 31 December 2013 Revision 2 30 October 1997 31 December 2013 Revision 3 3 April 2001 31 December 2013 Review 4 22 June 2001 31 December 2013 Review 5 19 May 2008 31 December 2017 Review 6 28 November 2013 31 December 2017 Consent and Moderation Requirements (CMR) reference 0003 This CMR can be accessed at http://www.nzqa.govt.nz/framework/search/index.do. Please note Providers must be granted consent to assess against standards (accredited) by NZQA, before they can report credits from assessment against unit standards or deliver courses of study leading to that assessment. Industry Training Organisations must be granted consent to assess against standards by NZQA before they can register credits from assessment against unit standards. Providers and Industry Training Organisations, which have been granted consent and which are assessing against unit standards must engage with the moderation system that applies to those standards. Requirements for consent to assess and an outline of the moderation system that applies to this standard are outlined in the Consent and Moderation Requirements (CMR). The The Skills Organisation SSB Code 100401 New Zealand Qualifications Authority 2016 NZQA Expiring unit standard 2641 version 6 Page 6 of 6 CMR also includes useful information about special requirements for organisations wishing to develop education and training programmes, such as minimum qualifications for tutors and assessors, and special resource requirements. The Skills Organisation SSB Code 100401 New Zealand Qualifications Authority 2016