Form 20 Version 3.0 (2007/2008) Heriot-Watt University - Module Descriptor Template (RAY) Module Title Forensic Analysis School Engineering and Physical Sciences Module Co-ordinator Dr J.H. Cameron SCQF Level 9 Module Code 1. Pre-requisites Minimum D grade in Stage 2 core Chemistry modules, or the equivalent 2. Linked Modules (specify if synoptic) 3. Excluded Modules Analytical Chemistry 4. Replacement Module Code: 6. Degrees for which this is a core module 7. Aims Date Of Replacement: MChem Chemistry with Forensic Science 5. B19FA Availability as an Elective Semester Yes On or OffCampus Credits 2 No On 15 The module aims to provide : an introduction to the theory and practice of some modern techniques of chemical instrumental quantitative analysis of particular relevance to the practising forensic analytical chemist 8. Syllabus Reproducibility, Reliability, Calibration, Internal Standards Mass Spectrometry - qualitative and quantitative methods of analysis using mass spectrometry ; descriptions of specific examples of forensic interest such as drugs, alcohol, explosives Separation Techniques - Gas chromatography, high performance liquid chromatography Forensic Microscopy - Atomic Force Microscopy and Scanning Electron Microscopy for the analysis of surfaces Forensic Spectroscopy - analysis of samples for metals by Atomic Absorption and Atomic Emission spectroscopy ; application of fluorescence spectroscopy to quantitative analysis ; sensitivity gains obtained using emission methods in general Powder and Fibre Diffraction – basic principles of diffraction of X-rays, Miller indices, indexing powder patterns, applications of powder diffraction, orientation effects in liquid crystals and fibres 1/2 Form 20 Version 3.0 (2007/2008) Heriot-Watt University - Module Descriptor Template (RAY) Module Title Forensic Analysis School Engineering and Physical Sciences Module Co-ordinator Dr J.H. Cameron SCQF Level 9 Module Code B19FA Semester 2 On or OffCampus Credits On 15 9. Learning Outcomes (HWU Core Skills: Employability and Professional Career Readiness) Subject Mastery Understanding, Knowledge and Cognitive Skills Scholarship, Enquiry and Research (Research-Informed Learning) On completion of this module, the learner will be able to: Discuss critically the importance of reproducibility and reliability in quantitative analytical chemistry Define and discuss the various contributions to chromatographic separation bandwidth Design the correct methods and experimental components required for chromatographic separation of a given mixture Interpret simple chromatographic data Design the correct mass spectrometric inlet system, ion source and ion analysis for complex forensic analytical mixtures Use isotope-ratio mass spectrometry, and selected ion and reaction monitoring, to solve forensic problems Demonstrate an understanding of the background to the AFM and SEM techniques, and a knowledge of their applications Discuss the theory and application of AA, AE and fluorescence spectroscopies in the analysis of chemical samples Describe the application of powder diffraction to the analysis of unknown materials Display a critical understanding of the concepts, theories and principles discussed in the module Personal Abilities Industrial, Commercial & Professional Practice Autonomy, Accountability & Working with Others Communication, Numeracy & ICT Personal abilities are embedded in the module. The module provides the opportunity to : Critically use mathematical methods to solve problems in forensic analysis Interpret, use and evaluate a wide range of data to solve problems of both a familiar and unfamiliar nature Manage time effectively, work to deadlines and prioritise workloads Use ICT skills with on-line materials, assessments (formative and summative) and web links to support the learning process Exercise autonomy and initiative in carrying out defined activities Work with a group of peers to discuss problems in analytical chemistry, sometimes taking the lead role 10. Assessment Methods 11. Re-assessment Methods Method Duration of Exam Weighting (%) Synoptic modules? Method Duration of Exam (if applicable) Examination Continuous Assessment 12. Date and Version Date of Proposal 27 August, 2007 2h Date of Approval by School Committee (if applicable) 70% 30% Examination (100%) Date of Implementation 15 September, 2008 2h Version Number 1.0 2/2