Jamison Brizendine Meg Streepey Senior Independent Project 18 April 2006 Mineralogy has been an important part of our everyday lives. We encounter rocks and minerals everywhere we go, where we work, and where we relax. Your house for example may have a cement roof, made up of the mineral gypsum. Your countertops may be composed of granite, formed from the inside of a giant volcano. You may work in an office building. That office building may have limestone facing which was the home to an extensive and ancient coral reef. When you go to a beach to relax chances are the beach is made up of quartz sand. Mineralogy exists everywhere and is a fundamental part of geology. In Physical Geology classes many students will learn how to identify minerals by their basic physical properties. The physical properties for minerals are: luster, color, heft, habit, cleavage, streak and hardness. Some minerals have a certain property which will stand out easily. Halite, for example, has a salty taste, sulfur has a bright yellow color and smells like rotten eggs, and magnetite is magnetic. Other minerals can be identified by using only one physical property. Talc has a hardness of one, biotite, a mica, has one perfect cleavage and its sheets can be peeled like an onion, and galena, is dense because it has lead in its structure. Unfortunately not all minerals can be identified with using one or even two physical properties. Pyroxenes and amphiboles, a single-chain silicate and a double chain silicate respectively can be difficult to identify in hand samples. They may share the same color, habit, luster, and even hardness. The way to tell those two minerals apart is that pyroxenes have ninety degree cleavage planes, while amphiboles have a sixty degrees and one hundred twenty degrees cleavage planes. Another interesting example of mineral confusion is the one between quartz and fluorite. Suppose someone finds a purple mineral, it can either be an amethyst, a variety of quartz, or a fluorite. Quartz can be identified by its superior hardness and its lack of cleavage. Additionally identifying plagioclase feldspars and orthoclase feldspars can be very difficult for some students. Both share all the same physical properties; however plagioclase feldspars are usually restricted to more mafic rocks and orthoclase can be easily identified in most felsic rocks. By learning about certain minerals the geology student can also learn about how they form from the different environments in which the mineral formations take place. A geologist would never find a diamond in central Indiana, just like limestone would not be found in the interior of a volcano. A student would be able to find calcite readily in a limestone, and quartz in sandstone. They may also learn that some minerals, like fluorite and gold, are formed in hydrothermal veins. They may also learn that some igneous rocks, like granites, would contain mostly plagioclase feldspar, quartz and orthoclase feldspars. What if the student was not interested in geology? Why should they care about mineralogy? The average person does not care about the effects that mineralogy has upon their lives. In the sixteenth century, finding mineral resources was the result of colonization, mining, warfare and the rise and fall of powerful empires. The Aztec empire, for example, was annihilated because of the Spanish Conquistadors looking for gold. After seizing all the gold, many of the Aztecs were slaughtered and a powerful empire was reduced to ashes. Mineralogy is used in many other sciences as well. Mineralogy contributes to the study of chemistry, biology, astronomy and physics. In chemistry, minerals are entirely elements and molecules. Elements have been successfully isolated from minerals. In physics, mineralogy is used for the study of chemical tracers, and the understanding of the origin of mineral phases. In astronomy, minerals have been used to calculate the age of the Solar System, the Earth and the other celestial bodies that orbit the sun. Without minerals, astronomers could only guess at the age of the earth, but with meteorites, astronomers can successfully find the age of the solar system. In forensics, geology and mineralogy is used to solve cases involving murders, rape and theft. A direct result of the study of mineralogy was the development of forensic geology. Forensic geology was first published as a method for solving cases in 1893 by Hans Gross. Gross was an Austrian criminal investigator who had stressed the need to use the microscope and mineralogy to examine the evidence left behind on shoes and other pieces of clothing. Another person to pioneer the use of forensic geology was the famous author who created Sherlock Holmes; Sir Arthur Conan Doyle. Doyle’s famous character used his spyglass to find evidence from mud and soil to help locate his suspects and solve the case. It would be only a matter of time before these methods would be put to use outside of a fictional novel. In 1904 Georg Popp, a German forensic geologist was the first person to use mineralogy and forensics to solve a murder case. Inspired by both Gross and Doyle, Popp examined the evidence left behind from a scarf that was used to kill Eva Disch, a seamstress. The suspect, Karl Laubach, worked in a gasworks company and a gravel pit. The scarf had snuff, coal particles, and the mineral hornblende. Popp then used the suspect’s fingernails to try and find a match. Both the evidence from the scarf and the evidence from Laubach fingernails was enough proof to sentence the suspect. With the success of the Disch trial, other countries began to use forensic geology, including the United States. In 1935 the FBI had a large amount of soil samples and three years later had a large collection of metals and minerals to help solve more cases (Murray 2004). Today the FBI solves thousands of cases each year using metal and soil samples, sand samples, minerals and microscopes. Many forensic geologists today use mineralogy and soil science as a tool. They first tend to look for unusual or rare minerals. If they can identify these minerals, then they can usually find where they originated. They can also use soil grain sizes and combinations of minerals to help locate a source. Many times, forensic geologists are unsuccessful and are frequently disappointed in their findings. This may be due to the fact that there was no transfer that had taken place or soils may have been transferred, resulting in a composite sample. Sometimes the area has had rapid soil change or there was not enough soil to make an accurate conclusion. Suspects have been known to wash the evidence behind so that there may not be enough evidence for a conviction. Sometimes the suspect was not even at the crime scene, so in that case the soil sample would prove his innocence in a crime. The goal of the assignment was to create a forensic geology lab that would be interesting and scientifically relevant for students. In order to create such a lab, it was assumed that the students already knew basic mineralogy identification. The lab would be designed to fit the student; not too simple, but not so challenging that it would frustrate students who have trouble grasping basic mineralogy and science. The lab should also not take longer than the average lab time, but also should take longer than an hour to complete. The creation of a good lab also needed an interesting plot. The first idea for the lab was a murder case involving a deceased husband. The husband was the owner of a large mineral collection and had been murdered so that one of the suspects would inherit his collection. The story involved fifteen suspects and an inspector who had three hours to solve the case before it leaked to the press. The story while cute had its own set of problems: The first problem was the story was not serious enough for the students. The second was finding fifteen samples that could be used in finding the murderer and the last problem was that chances are the lab would have taken longer than three hours to complete. The lab had to be rewritten and a new approach was taken. So the new lab would also be a murder case, but a case that was documented and could be used for a case study and good introduction for the lab. The murder of Adolph Coors III was such a case. The Gravel Page, by John McPhee, was used to given the overall background for the murder case. Adolph Coors was the grandson of the founder of the Coors Brewery Company. One day, no one knows for sure, he had disappeared from his ranch near Morrison, Colorado. Morrison is near Denver, Colorado close to the foothills of the Rocky Mountains. His car was found with the motor still running. Investigators also found glass and blood around the car. A suspect’s vehicle was found near a dump site in Atlantic City, New Jersey and showed four layers of earth material. The first, outermost, layer was obviously soil from the dump. The three other layers matched the geology of the Rocky Mountains. The sharp pink potassium feldspars came from the Pikes Peak granite, and pink feldspars from other Front Range granites. Other samples were quartzose sands from the Dakota Group and limes and clays from the Morrison Formation. One layer was where the victim was found, which had contained the feldspars from Pikes Peak and Front Range. The second layer of the three was the quartzose sands where Coors’s Ranch was located. The final and third layer from the Denver area that had contained the clays, sands and limes (Murray 95-96). The suspect, Walter Osborne, his alias name, was then found guilty of kidnapping and murder because the suspect’s automobile was directly tied to the crime scene and sentenced to life imprisonment. The lab involved an event similar to this case. A truck was found in a parking lot in Las Vegas, Nevada. Sand and gravel had accumulated on the tires of a vehicle and then was sent to a lab for investigation. As the forensic geologist the student would have to examine six samples given to him or her. Then the student was given an unknown sample to look at, this unknown sample was a combination of three samples, and this was the sample found on the truck tire. Originally I had asked the students to identify the minerals in each sample, the overall sorting of the sample, the average roundness of the grains, the average sphericity of the grains, if there were foreign objects in the grains and to find fossils if there were any. I had used six samples: The Sleeping Bear Dune from Traverse City, Michigan, The Petroglyph Beach from Arizona, The Morrison Shale Formation from Arches National Park, Arizona, Hilton Head Island Beach Sand, South Carolina, sand from the AuSable River in the Adirondack Mountains of New York and sand from the Cove Creek in Magnet Cove, Arkansas. All the samples were unique in appearance and had different enough properties that the student could enjoy and not become easily frustrated. The Hilton Head Island Beach sand had clear quartz, while the Petroglyph Beach sand had iron-stained quartz grains. The Cove Creek sand had pyrite and magnetite in the sample while the river sand from the AuSable River contained black hornblende grains and bright red garnets in the sample. The Morrison Formation sample had green shale and clays in the sample, while the final sample from Sleeping Bear Dune had iron stained quartz, basalts and chert. Doing the preliminary tests for the lab proved to be a little difficult for a student’s level. It would be assumed that if this was done late enough in the year, and this time it was, the knowledge of mineralogy would be a difficulty. I had created a Power Point to demonstrate how to identify roundness, sphericity and sorting to the class. It was quickly discovered that the students would have had a difficult time trying to figure out a grain’s sphericity or overall shape. Additionally there were not enough fossils or even foreign objects in the samples to make an accurate answer. To make the lab easier, the students were asked to identify the overall colors in a sample, and then identify the average roundness in a sample. The student was then asked to complete the sorting of the sample and then finally the overall character of the sample. These questions were asked for all six samples. Finally the student was to look at the unknown sample, and try to identify the three samples found on the tire truck. He or she then had to plot the points on a map to the possible route the truck had taken. These questions were sufficient enough to challenge the student, but not to make it too challenging and it was thought that the student would be able to complete the lab in less than three hours. Appendix 1: Jamison Brizendine Meg Streepey Physical Geology Lab and Independent Senior Project. Everyone is quite familiar with Sherlock Holmes. Sir Arthur Conan Doyle created a character that everyone would idolize. Holmes and his assistant worked for Scotland Yard. They would go to scenes of crimes looking for evidence such as soil samples, paint chips, wool and other material that would transfer or leave a presence. Forensic scientists today are much like Doyle’s imaginary character. When they are called in to crime scenes, they investigate reports and evidence. Today forensic geologists study material that is transferred from one thing to another. Minerals, soils, glass, cement, asphalt, and other foreign objects are used in their investigations. Forensic geologists are called in for a variety of different crimes including theft, murder, hit-and-run accidents, larceny, and kidnapping. Forensic geologists have worked on cases ranging from rape trials, to finding thieves who have stolen thousands of dollars worth of palm trees. Some forensic geologists even try to solve cases that involved swapping traded goods. A famous example that many forensic geologists are familiar with is the one that involved the murder of Adolph Coors III. Adolph Coors was the grandson of the founder of the Coors Brewery Company. One day, no one knows for sure, he had disappeared from his ranch near Morrison, Colorado. Morrison is near Denver, Colorado near the foothills of the Rocky Mountains. His car was found with the motor still running. Investigators had also found glass and blood around the car. A suspect’s vehicle was found near a dump site in Atlantic City, New Jersey and showed four layers of earth material. The first, outermost, layer was obviously soil from the dump. The three other layers matched the geology of the Rocky Mountains. The sharp pink potassium feldspars came from the Pikes Peak granite, and pink feldspars from other Front Range granites. Other samples were quartzose sands from the Dakota Group and limes and clays from the Morrison Formation. One layer was where the victim was found, which had contained the feldspars from Pikes Peak and Front Range. The second layer of the three was the quartzose sands where Coors’s Ranch was located. The final and third layer from the Denver area that had contained the clays, sands and limes (Murray 95-96). The suspect, Walter Osborne, his alias name, was then found guilty of kidnapping and murder because the suspect’s automobile was directly tied to the crime scene and sentenced to life imprisonment. A more detailed reading to the Adolph Coors kidnapping and murder is found on pages 91 to 102 in The Gravel Page, which you will be required to read before coming to lab. This lab will be very similar to solving the murder of the Adolph Coors case. The FBI field office in Las Vegas, Nevada currently has a suspect with a warrant for the arrest of a man who had recently shot and killed someone. The forensic geologist in charge of the case is currently on vacation in his penthouse in Palm Springs, California and has asked you to solve the case. The FBI has also found a car that was found in a parking lot in Nevada that contained sediment from its tires and tailpipe. Your lab has received six samples of various different locations and they want to know where the vehicle has traveled. You are a given an unknown with three different sediment locations which you will receive after analyzing the initial six samples. A. References needed for lab: 1. The handout from Sedimentary Geology (Prothero and Schwab, 2004) 2. The Gravel Page by John McPhee 3. A handout from Ron Parker’s Sedimentology class, August 2004. B. Please answer the following questions for the initial six samples: 1. What are the average mineral percentages in each sample? For example a sample may have 50% of a reddish mineral and 50% of a clear mineral. 2. What is the overall general character or appearance of each sample 3. The average roundness: The roundness or angularity of grains. 4. Sorting: Are the grains well sorted or poorly sorted? 5. For extra credit: Name the minerals present in each sample. Procedure: 1. Make groups of two to three people to share microscopes. There are six initial samples available that were collected by your lab. Answer the above questions on the worksheet. I will show you in class a step by step approach if you have trouble answering the questions. 2. Take a small clear dish, and then take a very, very small portion of the sample, about the size of you fingernail. Any larger and you will not be able to see the samples because the grains will be to close together to see any detail. 3. After finishing with the sample you have looked at, dump the sample back into the containers where they were found, this is so that they can be used later. Then clean the dish with a damp tissue rag so that your new sample is not contaminated. 4. The samples come from the following sources: Sample A: Dune Sand, Sleeping Bear Dune, Traverse City, Michigan. Sample C: AuSable River, Adirondack Mountains, New York Sample D: Petrograph Beach, Glen Canyon, Arizona Sample F: Arches National Park, Morrison Formation, Utah Sample G: Cove Creek, Magnet Cove, Arkansas Sample I: Beach Sand, Hilton Head Island, South Carolina 5. Conclusion: In order to finish the lab, please write on a separate piece of paper of which three samples were found on the truck tire. Explain how you came to this conclusion using the data you collected. On the map of the United States, trace the route the vehicle took from its origin to its final location in Nevada. Please turn this in with the data you collected from your initial six samples. The lab proved to be a large success and both lab classes thoroughly enjoyed it. The students learned a variety of skills after completing the lab. One of these skills was identifying minerals in a variety of sediments. Students were asked to identify various shades of colored minerals, and then were asked to identify them. The purpose was that if students could identify two physical properties: Luster and color. After these properties are identified then finding the correct mineral would not be a challenge. Quartz, for example is prevalent in beach environments, is non-metallic and it is a clear or orange color. Students were also asked to find the general character of a sample. If a student looked at sediment from Hawaii and then looked at sediment from South Carolina, there are many differences. The Hawaiian sediment contains olivine, pyroxene, hornblende and perhaps some quartz. The South Carolina sand is much more mature, it only contains quartz and maybe bits of asphalt from a beach road nearby. Students would learn that all sand, soils and sediments are not homogenous, but reflect on the depositional environment. Students also learned about the sorting, maturity and roundness of grains in sediments. They found out that if the grains were angular and poorly sorted, then the sediment must be near the source of original deposition. A sediment that contains grains that are fairly well rounded and well sorted means that erosion processes are more vigorous in that location. Some students also reviewed how some minerals are more prevalent and resistant than other minerals. Olivine which forms first from Bowen’s Reaction Series, typically is the first mineral to be destroyed by weathering processes because it is unstable at the surface. Quartz on the other hand is highly resistant to erosion. Quartz is harder than olivine and has no weak spots in its structure. The lab was also intended for students to refresh themselves to identify minerals that may have been tricky to identify earlier in the semester. After completing the lab, students were asked to complete a survey and then asked for questions or comments to help make the lab more enjoyable. The first question asked the degree of difficulty of the lab. One hundred percent had commented that the lab was just right for the skill level for physical geology. Other comments included that the difficulty was well explained, challenging, and fun. Some students commented that the lab was too simple because the samples were so different, and others thought it was a little overwhelming to identify colors. The next question on the survey asked the classes if the time of the lab was too short, too long, or just about right. Ninety seven percent of the class said the lab was just about right and only three percent of the lab group said it was too short. Other comments included was that the lab did not have the feeling of being rushed and “didn’t eat away my sunny afternoon”. Others felt that the outside reading of John McPhee’s article was taken into account on the length of the lab. One comment was that long labs tended to be redundant and that it would be hard focusing on the tasks at hand. This lab was short and the questions were clear and concise. Another comment was that the lab could have asked for more samples, but this one had shown enough differences in the different deposition environments in the United States. The majority students had felt that the lab was a little too short, but that if it had taken any longer than it would have become redundant. The third question asked if the introduction and the explanation of the lab was too brief and contained not enough detail, or it was too long and contained too much detail or if the lab was just fine. The numbers had more variety here. Five percent of the students felt that the introduction and explanation was too brief, eight percent thought it was too long, and eighty five percent felt it was just right. Other comments included that there was too much background information, such as the handouts, others felt that the example in class was good, it was doable and straight forward, and that the case study was an overall good introduction to the lab. The final question asked if the lab furthered the student’s interest in forensic geology, had no change on the interest in forensic geology or made the student wish they had never heard of forensic geology. Fifty seven percent said that after doing the lab the students were further interested in the study of forensic geology and twenty six percent of the students answered that it had no change on the study of forensic geology. One person commented that they thought about pursuing forensic geology as a possible career path. An interesting question that was given to me was how one would know the order of the places traveled. In the case of the current lab, this could not be done, because samples were mixed with other samples to obtain an unknown sample. One way to solve this question would be to have two unknowns. One unknown would have a mixture of two samples and another unknown would have a mixture of the same two samples, plus another sample to yield a final mixed sample. If that process were done, than the student could draw a possible route on a map that the “vehicle” might have taken. The overall results from the lab proved to be positive and beneficial for the students, lab assistants and the professor. There should be no need to make any large scale changes to the lab, since the students felt it was just right for the skill level. The background reading for the class I felt was essential because it set the student up for the lab. Without the background reading and case study, the lab would not be as interesting or stimulating to students. If any changes were to be made I would make the following changes: The first change would be to increase the initial samples from six to eight. The two additional samples could be similar to each other, similar to the original samples, or even very different from the original six. Making eight original samples and one unknown would make the lab a little longer, but not make it so long that it becomes redundant. The forensic geology lab was a great choice for teaching students about possible career paths, and a good introduction into sedimentology. It also engages the students to identify minerals and look for objects they would not initially find in sediment, such as cement, wool or asphalt. Using this lab is a great way for students to refresh themselves on how to identify minerals and to teach students how geology is used in other applications besides academia.