Determination of Wet Film Thickness of Waterborne Road Marking

advertisement
Department of Planning, Transport & Infrastructure
Field Services Section
Technical Services Group
Procedure
Determination of Wet Film Thickness of Waterborne Road Making Paint / Glass Bead
Application Rate, Test Panels
TP908
Revision: 3.5
1.0
Date: May 2012
Page 1 of 3
SCOPE
This procedure describes a method for determining the average wet film thickness of paint and glass
bead application rate from test panels.
2.0
REFERENCES
AS/NZS 2009, Glass beads for pavement-marking materials
AS 1580, 202.1, Density.
AS 1580, 202.2, Density of Water Dispersed Paint Subject to Foaming.
AS 1580.301.1, Non Volatile Content
AS 1140.11, Particle Size Distribution by Dry Sieving
3.0
DEFINITIONS
Nil.
4.0
APPARATUS AND MATERIALS
4.1
Apparatus

2x Aluminium panels, nominally 200x100x1.5mm

2x Buckets with sealable lid

Sieve 200mm diameter 75µm mesh, full stainless steel

Plastic funnel 200mm diameter, with stand

Drying oven, 105 ± 3°C

Desiccator

Balance, >500g capacity, readable to 0.01g

Steel rule 300mm

Lacquer thinners
5.0
SAMPLING AND SAMPLE PREPARATION
5.1
Sampling
Duplicate 200x100mm panels are placed adjacent to one another, in the path of the machine.
PRINTED COPIES ARE UNCONTROLLED DOCUMENTS
File Location: Q:/Quality Management
Department of Planning, Transport & Infrastructure
Field Services Section
Technical Services Group
Procedure
Determination of Wet Film Thickness of Waterborne Road Making Paint / Glass Bead
Application Rate, Test Panels
TP908
Revision: 3.5
5.2
Date: May 2012
Page 2 of 3
Sample Preparation
Retained panels must be allowed to dry overnight prior to testing. Where testing is urgent, panels
may be dried in an oven at 105°C for 2 hours.
6.0
PROCEDURE TO BE FOLLOWED
The following procedures utilize duplicate panels, placed on the road adjacent to one another, in the
path of the line marking machine. One of the panels is placed in a bucket immediately after
application on site to remove beads, whilst the other is dried.
6.1
On site, Place the panel to be washed in a plastic bucket with sufficient water to cover the
panel, press the lid into place and mark the number of the retained panel on the bucket lid.
Place the retained panel off to the side where it will be protected from contamination.
6.2
Record the number of the panel, together with information regarding location etc, on the
worksheet.
6.3
On return to the laboratory, Remove the lid from the plastic bucket, and wash the paint and
beads from the panel into the bucket.
6.4
Place the 200mm 75µm mesh sieve in the plastic funnel.
6.5
Rinse the contents of the bucket through a sieve and then place the sieve into the oven at
105°C to dry.
6.6
Allow to cool in a desiccator, then brush beads into a container and weigh to the nearest 0.01g
(m3).
6.7
Measure the width (W) of the line on the Dry duplicate panel, to the nearest 1mm.
6.8
Weigh panels to the nearest 0.01g, and record (m1).
6.9
Scrape the panel clean and rinse with thinners. Then weigh to the nearest 0.01g, and record
(m2).
Note: All of this work shall be performed in a fume cupboard, with appropriate personal protective
equipment.
6.10 If the density (D) and non-volatile content (N) are not known, these shall be determined in
accordance with AS1580 test methods.
PRINTED COPIES ARE UNCONTROLLED DOCUMENTS
File Location: Q:/Quality Management
Department of Planning, Transport & Infrastructure
Field Services Section
Technical Services Group
Procedure
Determination of Wet Film Thickness of Waterborne Road Making Paint / Glass Bead
Application Rate, Test Panels
TP908
Revision: 3.5
Date: May 2012
7.0
CALCULATIONS
7.1
Wet Paint Film Thickness
Page 3 of 3
Calculate the wet film thickness of paint using the following formula:
Wet Film Thickness (m) =
Where
7.2
m1
m2
m3
N
D
W
=
=
=
=
=
=
(m1 – m2 – m3) x 106
NxDxW
panel + mass of dry paint + glass bead (g)
mass of panel (g)
mass of glass bead (g)
non-volatile content (%)
density of paint (kg/l)
width of line (mm)
Glass Bead Application Rate
Calculate the bead application rate using the following formula:
Glass Bead Application Rate (g/ m2) =
Where
8.0
m3
W
=
=
m3 x 104
W
mass of glass bead (g)
width of line (mm)
PRECISION
Uncertainty of measurement has been determined as ± 4% for wet film thickness and ± 3% for glass
bead application rate.
Uncertainty of Measurement determined by and for DPTI Technical Services Group, Field Services
Section.
9.0
DOCUMENTATION
Complete form TP908-1
PRINTED COPIES ARE UNCONTROLLED DOCUMENTS
File Location: Q:/Quality Management
Department of Planning, Transport & Infrastructure
19 Bridge Rd Walkley Heights Ph (08) 8260 0230, GPO Box 1533, Adelaide SA 5001
Technical Services Group
Procedure
Determination of Wet Film Thickness of Road Marking Paint / Glass Bead
Application Rate, Test Panels
TP908
Contractor
Test Location
Date of Test
DATA
Density of Paint,
Kg/L
D
Non-Volatiles, %
N
WET FILM THICKNESS
Line No.
Panel no.
Washed Panel Area cm²
Bead mass,g
Panel no.
Area cm²
Mass panel + paint +
bead, g
Retained Panel
Mass panel, g
Mass paint + bead, g
Mass bead, g
Mass paint, g
Paint wet film thickness, µm
Glass bead rate, g/m2
Tested by: …………………………..….........................
Date:……………………
Calculated by: …………………...................................
Date:……………………
Checked by: ……………………..………………………
Date:……………………
Form TP908-1, Revn. 3.5
PRINTED COPIES ARE UNCONTROLLED DOCUMENTS
File Location: Q:/Quality Management
Download