Laboratories for CHM 508 – Analytical Chemistry III
Method Name
Lab #
Copper in Air by Flame AAS (air sample collected by filter in
cassette)
Method Source
Standard
Methods
Internet
EPA SW 846
Internet
EPA SW 846
Internet
NIOSH
Internet
NIOSH
Internet
NIOSH
Introduction to High Pressure Liquid Chromatography
Skoog (8th ed.)
7
Introduction to Gas Chromatography
Skoog (8th ed.)
8
Ethanol in Beverages by Gas Chromatography
Internet
9*
Sulfate, Nitrate and Chloride in Surface Waters by Ion
Chromatography
Standard
Methods
10*
Aspirin in Pharmaceuticals by HPLC
Internet
11*
Warfarin in Pharmaceuticals by HPLC (air sample collected
by impinger)
Volatile Organic Hydrocarbons by GC (air sample collected
by charcoal tube)
Internet
NIOSH
Internet
NIOSH
12*#
Data Reporting in the Analytical Laboratory II – Check Out
Lab Manual
14
Moisture Determination in Soils – Check In
Standard Preparation of Sediments, Sludges and Soils
Copper in Soil by Flame Atomic Absorption
Air Sampling by Indicator Tube, Sorbent Tube, Impinger and
Filter
Acid Digestion of Air Filters
1
2
3*
4
5
6*
13*#
These laboratories will be completed time permitting. See BlackBoard for current list.
* Denotes a laboratory with an unknown (student accuracy and precision testing).
# Denotes where unknowns are the same so that methodologies can be compared.
Laboratories to run simultaneously:
Lab #
7 and 8
9 and
10
12 and
13
Labs
Introduction to High Pressure Liquid Chromatography with Introduction to
Gas Chromatography
Ions by IC with Ethanol in Beverages by GC
Aspirin by HPLC with Volatile Organic Hydrocarbons by GC
1
Laboratories for CHM 408 - Analytical Chemistry II
Method Name
Method Source
Standard
Methods
Lab #
Chromium (III) in Aqueous Solution by Spectrophotometry
Internet
2
Chromium (III) in Aqueous Solution by Spectrophotometry
Internet
3*
Preparation of a Steel Sample for Spectrophotometric
Analysis of Manganese
Skoog (8th ed.)
4
Manganese in Steel by Spectrophotometry
Skoog (8th ed.)
5*#
Introduction to Spectrophotometry – Check In
Preparation of a Steel Sample for Flame Atomic Absorption
Analysis of Manganese
Manganese in Steel by Flame Atomic Absorption
Sulfate in Surface Waters by Turbidimetry
Sulfate in Surface Waters by Gravimetry
US EPA
SW 846
US EPA
SW 846
Standard
Methods
Standard
Methods
1
6
7*#
8*
9*
Skoog (8th ed.)
10
Analysis of Sulfide in Soil by Iodometric Titration
Standard
Methods
11*
Analysis of Vitamin C in Juice by Iodate Titration
Skoog (8th ed.)
12*
Analysis of Vitamin C in Pharmaceuticals by Iodine Titration
Skoog (8th ed.)
13*
Introduction to Water and Wastewater Treatment – Check Out
Standard
Methods
14
Production of Common Desk Reagents
These laboratories will be completed time permitting. See BlackBoard for current list.
* Denotes a laboratory with an unknown (student accuracy and precision testing).
# Denotes where unknowns are the same so that methodologies can be compared.
Laboratories to run simultaneously:
Lab #
4 and 5
7 and 8
10 and 11
Labs
Mn in Steel by UV-VIS Spec with Mn in Steel by FLAAS
Sulfate by Turbidimetry with Sulfide by Iodometric Titration
Total Chromium by FLAAS with Chromium (VI) by UV-VIS Spec
2
Laboratories for CHM 308 - Analytical Chemistry I
Method Name
Method Source
Lab #
Laboratory Tour – Check In
Lab Manual
1
Standardization/Production of Common Desk Reagents
Standardization/Production of Common Desk Reagents
Air Sampling for Alkaline Dust by Titration
Stan. Methods
Skoog (8th ed.)
Stan. Methods
Skoog (8th ed.)
Internet
NIOSH
2
3
4*
Hardness of Water by Chelation
Skoog (8th ed.)
5*
Chloride in Solution by Gravimetric Analysis
Skoog (8th ed.)
6*#
Chloride in Solution by Argentometric Titration
Skoog (8th ed.)
7*#
Chloride in Solution by ISE
Standard
Methods
8*#
Fluoride in Toothpaste by ISE
Skoog (8th ed.)
9*
Preparation of Common Desk Reagents
Skoog (8th ed.)
10
Dissolved Oxygen by Membrane Probe and
Azide Modification
Standard
Methods
Standard
Methods
Standard
Methods
Biochemical Oxygen Demand by Membrane Probe
Introduction to Water and Wastewater Treatment
Pharmaceuticals by TLC – Check Out
Internet
11*
12*
13*
14
These laboratories will be completed time permitting. See BlackBoard for current list.
* Denotes a laboratory with an unknown (student accuracy and precision testing).
# Denotes where unknowns are the same so that methodologies can be compared.
Laboratories to run simultaneously:
Lab #
10 and 11
Labs
Chloride by ISE with Fluoride in Toothpaste by ISE
3