NAME:________________________DATE:_____________PERIOD:________ Emission Spectra Lab Part 2 Each group will be called to the front of the room to observe the activity. Use Part One of this lab to answer the questions until your group is called. REVIEW: 1. What is an excited electron? _________________________________________________________ _________________________________________________________ _________________________________________________________ 2. How much energy is released when an electron decays? _________________________________________________________ _________________________________________________________ _________________________________________________________ 3. Why do elements give off different colors of light when they are burned? _________________________________________________________ _________________________________________________________ _________________________________________________________ _________________________________________________________ _________________________________________________________ 4. How would you determine the composition of an unknown substance with a spectrometer? _________________________________________________________ _________________________________________________________ _________________________________________________________ 1 5. List five safety rules you should follow when you are in the vicinity of a lit Bunsen burner. _________________________________________________________ _________________________________________________________ _________________________________________________________ _________________________________________________________ _________________________________________________________ _________________________________________________________ _________________________________________________________ 6. Read all the procedures thoroughly NOW so you are prepared. Then, name three accidents that could potentially happen if you do not follow safety rules. _________________________________________________________ _________________________________________________________ _________________________________________________________ _________________________________________________________ _________________________________________________________ _________________________________________________________ _________________________________________________________ MATERIALS: Safety equipment: Safety goggles Fire Blanket Fire Extinguisher Spectroscope Bunsen burner Dropper assemblies Copper Sulfate 2 Sodium Carbonate Lithium Chloride 2 unknown solutions PROCEDURES: 1. Put on your safety goggles when you are called to the front of the room. So, when you arrive, safety goggles should be on. Tie back long hair and loose clothing. Never touch the flame of the Bunsen burner. Never lean over the Bunsen burner. 2. Choose one person in your group who has excellent spectroscope skills. One person will view the flame through the spectroscope and determine the location of the emission lines. 3. Your teacher will light the Bunsen burner. Each dropper assembly contains some drops of a chemical solution with a wire loop protruding through the dropper. The wet loop will be held at a 45 degree angle to the flame. Note the color of the flame of five different solutions in the data table. 4. One person in the group will view the flame with a spectroscope. DO NOT BRING THE END OF THE SPECTROSCOPE TOO CLOSE TO THE FLAME. IT WILL MELT. That person will draw the emission lines in the data table and share the results with the group when they return to the table. 5. When you return to your table, put your safety goggles in the bucket of warm soapy water. Then dry them with paper towels and leave them in the bucket on the lab bench. 6. Answer the questions. 3 DATA TABLE: Name of Compound Flame Color Copper Sulfate Lithium Chloride Sodium Carbonate Unknown #1 Unknown #2 Emission Spectrum – Copper Sulfate 4 5 6 7 6 7 6 7 Emission Spectrum – Lithium Chloride 4 5 Emission Spectrum – Sodium Carbonate 4 5 4 Emission Spectrum – Unknown #1 4 5 6 7 6 7 Emission Spectrum – Unknown #2 4 5 Questions: 1. Compare the emission spectra and flame colors of the known and unknown substances. Is unknown #1 copper chloride, sodium chloride or lithium iodide? _____________________________________________________________ Why?________________________________________________________ 2. Compare the emission spectra and flame colors of the known and unknown substances. Is unknown #2 copper chloride, sodium chloride or lithium iodide? _____________________________________________________________ Why?_________________________________________________________ 3. What do you expect the emission spectrum of lithium iodide to look like? Why? _______________________________________________________________ _______________________________________________________________ 5 6