OPERATING PROCEDURES EVG 501 WAFER BONDING SYSTEM INCLUDING EVG 301 CLEANING STATION AN D EVG 620 WAFER ALIGNING STATION Rev. 2/9/2016 Material Restrictions: All materials allowed for use in this equipment are listed in PDF form on the WCAM My Web Space. To view the listing following these steps: A. Open the UW website https://mywebspace.wisc.edu for My WebSpace. B. Log on using your UW NetID and password. C. Click on the star in the upper left corner. D. Under Bookmarks click on Group Directories. E. Scroll down the list of organizations to WCAM. F. Click on WCAM. G. Double click on the first file folder to open “Approved Materials.” H. Double click on the WebsiteRpt to view the approved materials for equipment. I. Within the PDF you can perform a search. Overview The EV system is comprised of two units: the EVG301 wafer cleaning station, and the EVG501 wafer bonding station. The unit tooling is designed for 15 mm pieces, 50 mm (2 inch) 1 Document1 wafers, 75 mm (3 inch) wafers or 100 mm (4 inch) wafers. The substrate can be silicon, glass, or sapphire. A complementary tool is the EV 620 aligner. The EV 620 system is designed for waferto-wafer alignment of 100 mm (4 inch) wafers. This is a desktop system with a manual stage for backside alignment method. This method has a resolution of ± 2 µm. The aligned wafers are clamped in a special chuck, which is then transferred to the EV 501 system for the bond processing. Three types of bonding can occur with the EVG501 station: Direct bonding – Wafers with smooth, clean (preferably prime grade) surfaces are in direct contact without significant pressure. Bonding temperatures can range from less than 100 °C to 550 °C (maximum temp of heating unit on EVG501). Anodic bonding – Substrates are in contact and the bond is made by applying a large electric field with temperatures ranging 300 °C to 450 °C to increase mobility of mobile charges (e.g. Na+ ions). Typically, this type of bonding is used for permanent joining of a Na+ containing borosilicate glass substrate and some semiconductor wafer. Be sure to check your glass CTE to see how closely it matches your wafer CTE. Pyrex 7740 is a standard glass used for anodic bonding. PLEASE CONTACT THE STAFF MEMBER IN CHARGE IF YOU ARE DOING ANODIC BONDING. THERE ARE ADDITIONAL TOOLS AND STEPS THAT ARE USED WHICH MAY NOT BE DOCUMENTED IN THIS PROCEDURE. Intermediate-Layer bonding – This method requires a layer between the substrates for bonding. A metal layer can be used for eutectic bonding; or other layer types such as polymers, solders, low temperature glass or soft, thin metal films for thermo-compression bonding. Preparation for Bonding To prepare wafers for bonding the following basic steps are necessary: 1. Thickness measurement of the wafers, flags and field electrode (graphite or glass plate used only for eutectic (graphite) or anodic (glass) bonding). This thickness measurement is referred as the “stack height” and is needed to correctly adjust the pressure applied to the wafer bow piston at the center. 2. Cleaning of the wafers. This can be wet-chemical or by plasma or both. 3. Optional rotational alignment the wafers in the EVG620 system. This may not be necessary for most general users. 4. Check, with a bright light coming in at a small angle with respect to the wafer surface, or with a microscope, if there are any particles before bonding. If so, re-clean or replace the wafer. 2 Document1 5. The actual bonding process, which can be run manually, or automatically for more uniform control among a batch of wafers. Stack Height Preparation (Contact staff person to approve process parameters and correct tooling components before processing if you are unsure.) Stack thickness should be measured before bonding. Stack = field electrode + both wafers + flags (if used) (Field electrode is only used for anodic or eutectic bonding, and is the glass or graphite plate. Use less than 500 N (112 lbs) of force when using the glass plate or it will crack!) Wafers should be chemical and/or plasma cleaned before bonding. Start-Up 1. Log into CRESS 2. At the equipment computer, open two programs: EVG 501 for the bonding station, and EVG 301 for the cleaning station NEXT – GO TO WAFER CLEANING PROCEDURES OPERATING PROCEDURES EVG 301 WAFER CLEANING STATION Note: Deionized water is Fluid 0. No other chemical fluids are available with our system. Start-Up 1. Contact staff person to approve process parameters, wafer size file and correct tooling components if you are unsure of the procedure. 2. Main power to the system and computer should be ON. 3. Open and/or maximize the following program window: EV 301 – the cleaning station 3 Document1 Operation 1. Operation is based on wafer size settings. To set the wafer size, download a settings file. INITIALIZING and PROGRAMMING the cleaning head parameters Objective: To download the correct INI file for the size wafers being bonded. There are INI files for 2-inch, 3-inch and 4-inch wafer size. Note: The download is performed in REMOTE control. The cleaning station is manually operated in LOCAL control. 1. Open “MY COMPUTER”/ C:\ EV301 folder INI folder. 2. Open the desired size wafer file folder. 3. Copy the appropriate INI file and paste it into the parent directory, OVERWRITING the file that is already there. 4. Close all recently opened folders. 5. Maximize the EV301 Engineer program. 6. Click on REMOTE ON/OFF. Note the REMOTE button on the bottom of screen changes to GREEN and ON. 7. Click on FUNCTIONS and then on the Maintenance button. 8. Click on “Download INI-file parameters.” 9. When download completed close Maintenance window. Click on EXIT FUNCTIONS. 10. Click REMOTE ON/OFF. Note the REMOTE button on the bottom of screen changes to RED and OFF. 11. Minimize the EV301 Engineer program. 12. Continue with EV 301 operating procedures. 2. Once the correct settings are downloaded, ensure that the REMOTE is OFF. This allows for the PRESETS to be used manually at the panel by pressing the buttons. 3. Measure thickness of the field electrode and wafers to be bonded. Use the Mitutoyo Digimatic Indicator located on the table near EVG system. Field electrode Wafer 1 Flags Wafer 2 ______ mm + ______ mm + 0.05 mm + ______ mm TOTAL STACK = ______ mm 4. You may want to replace the alignment arm for the appropriate sized wafer. The plastic arms can be found the ACCESSORIES or SPARE PARTS tub. Visual alignment can also be done. 5. At the clean station control panel, press ALIGN (top button) to move the arm in the down position. 6. Place first wafer on stage against the align arm. 4 Document1 7. At the cleaning station control panel, turn knob to desired preset 0 – 9. (only program 0 is currently active with parameters – contact the staff if you need to add other programs). 8. To begin the clean cycle, press: START – GREEN button on panel START ENTER – bottom button on panel ENTER 9. The program will automatically stop and alarm at completion and the wafer can be removed from chuck. Press ENTER stop alarm. ENTER Process Option A: Aligner Station before Bonding Station Process Option B: Bonding Station without aligning wafers Place first wafer into aligning tool. Repeat Steps 4-10 for second wafer. Place first wafer into bonding tool. Repeat Steps 4-10 for second wafer. 5 Document1 OPERATING PROCEDURES EVG 620 WAFER ALIGNING STATION You may skip this section if you are not doing any rotational alignment of your wafers or substrates. Components: This system is only for 100 mm (4-inch) wafers. The bonding method is anodic bonding. Components needed for manual aligning: Bond chuck top Bond chuck bottom Bond chuck ruler Carbon electrode Glass for anodic bonding 6 Document1 General Data on Substrate Alignment Range of X & Y alignment +/- 5mm Rotation +/- 3.5° Resolution 0.06µm Bond aligner accuracy 0.5µm for glass/silicon, 1µm silicon/silicon Separation Maximum 300µm adjustable in 1µm steps Resolution of Z-movement 0.033µm Alignment Mark Diagram Area where alignment marks may be seen 17.00 mm 12.00 mm 12.00 mm Flat of substrate Microscope Movement Switch between stage and optic selection with the button on the joystick Y direction move joystick front or back X direction move joystick left or right Theta/Z directions turn the joystick clockwise or counter-clockwise to move the optic in the Z-direction (focusing) or the stage in theta direction (PHI axis). 7 Document1 Manual Anodic Bonding Process The following presents a basic overview of anodic bonding two silicon substrates. The detailed process steps follow this section. 1. Load first substrate with bonding surface and alignment marks facing down. 2. Wait while the aligner performs wedge compensation (WEC) is between first substrate and tool. 3. Use joystick to adjust objectives to substrate alignment marks. 4. Use joystick to adjust crosshairs to alignment marks. 8 Document1 5. Load second substrate with bonding surface facing up and alignment marks facing down. 6. Use stage micrometers to align second substrate alignment marks to crosshairs. 7. Insert separation flags. 8. Wait while the aligner performs wedge compensation (WEC) is between first substrate and second substrate. 9 Document1 9. Use stage micrometers to do final alignment of second substrate to crosshairs. 10. Clamp the bond tool. 11. Remove bond top and proceed to EVG 501 for bonding process. 10 Document1 Start-Up 1. Log into CRESS. 2. Ensure that all controls to the EV 620 are powered ON 3. If not ON complete the powering up in the following sequence. a. The main power switch. b. The power control switch. c. The green on button. B C A 4. The EV Explorer window (not MS Windows) is automatically displayed. 5. Use the tracker ball to move the cursor. Use left button to double click on the application icon EVGXX Machine Software. 6. A blank log in window will be displayed. Click on Login. 11 Document1 7. A dialog window will appear requiring a user name and password. User name: User Password: EV User EV 8. Click Login 9. Wait while the tool automatically goes through initialization steps. You will be prompted to move the tray out. The message at the bottom will state: ! Tray – Move Tray Out 10. Gently rotate tray out. 11. After the tray is completely out, the initialization will continue. 12. Wait for initialization to complete. The message on bottom of screen will state: Initialization Okay 13. A blank align process application window will be displayed. 12 Document1 Recipes The alignment process is operated by recipes. Following are procedures for recipe operations: Creating a new recipe Saving a recipe Opening a recipe Starting a recipe Creating a new recipe 1. In the menu, click on File / New or click on the new document icon . 2. A recipe process window will open. 3. The following settings are standard for all recipes used in this EVG620 model. Process: Man. Anodic Bond Process mode: Crosshair Tool Name: 4 inch Bondtool, Size 4 inch Tool Name: 4 inch Chuck, Size 4 inch Separation: 30um Chuck: 1 Zone - Manual Process contact force: 1100 mbar WEC contact force: 500 4. Measure thickness of substrates and key value into 13 Document1 Saving a recipe 1. 2. 3. 4. In the menu, click on File / Save or click on the new document icon Or, File / Save As. Name the recipe Click OK. The file will be saved in the default directory. . Opening a recipe 1. 2. 3. 4. In the menu, click on File / Open or click on the new document icon The default directory will open. Double click on the selected recipe; or click on the recipe and then OK. The recipe process window will open with the selected recipe. . Starting a recipe 1. Click the green RUN arrow . 2. This is a manual alignment station. As the process recipe runs, the screen will prompt the user through the alignment steps. Typical Recipe Process Run NOTE: If the cursor is sitting on the bottom bar of a process screen, the EV Explorer Window will appear. Click on the EVG icon at the botton of the Explorer Window to return to the process recipe. 1. Open a recipe. 2. Check the recipe settings, including the substrate thickness. 3. Click on the green arrow Run to start the recipe. 4. WAIT several minutes for the process to begin 14 Document1 5. Screen will display each process step with illustrations and directions. Complete each process step directions and click Continue at the bottom of the screen. Begin process Click Continue Configure Optics (Skip – this option is not available) Click Continue Retrieve bond tool from storage rack 15 Document1 Insert Bond Tool Check placement of vacuum holes See following method for tool insertion Insert Bond Tool Check placement of bond tool. Align vacuum holes on bond tool to vacuum holes on stage. Insert Bond Tool 2 Insert front edge of bond tool first. This is a snug fit. Press front edge of bond tool against spring pin. Then insert back edge of bond tool. 1 Click Continue 16 Document1 Remove clamps Press down and turn each clamp until top line is vertical Click Continue 17 Document1 Remove flags Flags are not used in this process method Press each flag outward. Click Continue Insert chuck. This part has already been inserted vacuum connected. Click Continue Insert ruler with pins down and flat at 3:00 position 3 o’clock Ruler handle at 5:00 position Click Continue 18 Document1 Insert bond glass HANDLE GENTLY! The glass slides under ruler TOP pointing to the left TOP TOP Click Continue Insert wafer Position with flat to the right at 3:00 position 3 o’clock Bond surface DOWN ALIGNED TO the ruler ON TOP of glass NOTE: Placement of the top substrate is critical. No rotation of the top substrate is available. 19 Document1 Click Continue Remove ruler Carefully lift ruler away from glass and wafer. No vacuum is on Click Continue Move tray in Vacuum is on to hold glass and wafer Center stage Adjust 3 micrometers to center position 5.0 Click Continue 20 Document1 Check the positions of all three micrometers. The scribed line at 5.0 indicates the center position. Scribed line WEC Wait while the aligner makes adjustments to the first wafer 21 Document1 Adjust microscope Click on Position. Use cursor and button to select LEFT or RIGHT microscope objective button on bottom of screen Move objective with joystick to image alignment marks on wafer Zoom focus by rotating joystick knob. Adjust image by sliding controls. TIP: Microscope positions can be saved and stored for each recipe. Click Continue 22 Document1 Adjust crosshairs Click on CONTROLS to open crosshair control box TIP: Increase thickness to identify crosshair location Click on LEFT CROSS or RIGHT CROSS button on bottom of screen Move crosshair to image alignment marks on wafer by clicking directional arrows Slide controls to adjust crosshair image Click Continue 23 Document1 Move tray out The first wafer will be held in the tool by vacuum The tray will come out with only the glass to load the second wafer Click Continue Insert ruler TOP Reposition the glass and ruler Click Continue Insert wafer Position with flat to the right at 3:00 position 3 o’clock Bond surface UP ALIGNED TO the ruler ON TOP of glass Click Continue 24 Document1 Remove ruler Carefully lift ruler away from glass and wafer. No vacuum is on Click Continue Move tray in Vacuum is on to hold glass and wafer Click Continue Pre-align Use 3 micrometers to align second wafer to crosshairs Click Continue 25 Document1 WEC Wait while the aligner makes adjustments to the second wafer Final alignment Use 3 micrometers to align second wafer to crosshairs Click Continue 26 Document1 Before the clamps, make final align of second wafer. Use 3 micrometers to align second wafer to crosshairs Insert clamps Press down and turn each clamp until top line is horizontal Click Continue 27 Document1 Remove bond tool Wait while instrument releases bond tool Carefully lift bond tool out of the aligner Pull bond tool towards the front and lift out back to free bond tool The stack is clamped and ready for bonder Click Continue End of Process Exit out of aligner and continue to bonder DO NOT CLICK CONTINUE Click Exit 28 Document1 Exit returns to initial menu screen Click on the Park Tray icon. Click Continue You will be instructed to move the tray in Click File / Exit NEXT – GO TO WAFER BONDING PROCEDURES Check bonder for anodic setup before continuing Use only the carbon electrode with the aligner chuck. 29 Document1 OPERATING PROCEDURES EVG 501 WAFER BONDING STATION Pre-check 1. Measure thickness of the field electrode and wafers to be bonded before cleaning. Use the Mitutoyo Digimatic Indicator located on the table near EV system. Field electrode Wafer 1 Flags Wafer 2 ______ mm (only used for anodic bonding [Glass or graphite]) + ______ mm + 0.05 mm + ______ mm TOTAL STACK = ______ mm 2. Adjust the micrometer on the top to the TOTAL STACK measurement. 3. Clean the wafers. See CLEANING procedures. Start-Up 1. Main power of system and computer = ON. 2. Open and/or maximize the EV501 wafer bonder program window. 3. Maximize the Manual Setup Menu. 4. On the Activation Bar, ensure PUMP is OFF. If not, press PUMP and wait. 5. Check the top of the yellow Balzers valve. The center pin should be DOWN with the pump off. This indicates that the gate valve is closed for the turbo pump. 6. On the Activation Bar, press VENT to bring the bonding chamber to atmosphere. 7. When venting has completed, on the Activation Bar, press VENT. 8. Open the bonding tool by pressing and holding both GREEN buttons on bonding panel until bond chamber has fully opened. 30 Document1 9. Each bond chuck assembly is stored on the shelving unit near the bonder. 10. Check set-up for correct bonding tools. Contact staff person for correct setup if you are unsure or have any questions. See following diagrams for tooling setup. Top Electrode or Pressure Plate Top electrode setup has two components: 1. Top pressure plate For Anodic Bonding: you can use the quartz insert plate and contact finger: For Thermo-Compression Bonding: you should use the metal insert: Quartz insert with opening for piston and lip for metal finger. Stainless steel insert with opening for piston (in center) (Can be used for force > 2000 Newtons) Top Electrode or Pressure Plate 2. Anode electrical contact finger Contact metal (finger) installed on top of quartz insert (circled in red) Cross sectional assembly of field electrode, waferstack and bonding chuck Field electrode & Alignment ruler (if used) Second wafer Flags First wafer Bond Chuck 2-inch 3-inch 4-inch 31 Document1 Bonding Chucks Component 2-inch 3-inch 4-inch Bond chucks After placement - check the flag operation. Bottom Bonding Assembly Field electrodesFor use with: bow pin & 2-inch rulers bow pin & 3-inch rulers bow pin & pressure Electrode for force >2000N Electrode for force >2000N & rulers For uniform pressure across wafer Rulers: Electrode for force >2000 N 32 Document1 Example of Tooling Setup 1. Select correct tooling components. Install chuck to equipment. Check operation of flags. 2. Position first wafer onto the bond chuck. (thinnest wafer recommended to be on the bottom) a. Make sure the bond side of wafer facing up (especially for double polished wafers). b. Align against the three (quartz) alignment pins – 2 pins at the wafer flat and 1 pin at wafer side. The quartz alignment pins should not be taller than the bottom wafer. 3. Ensure the separation flags are positioned over the first wafer. 4. Position desired ruler on the chuck by aligning the ruler holes onto the chuck metal pins. The alignment rule is for positioning the second wafer. Adjust set screws to level the ruler. 5. Position the second wafer onto the bond chuck using the appropriate vacuum wand. a. Bond side of wafer down. b. On top of the separation flags. c. Align to the ruler, if alignment ruler is used. 6. Place field electrode on top of wafer stack. Ensure that the field electrode sits flat and is not resting on top of the ruler or separation flags. 7. Go to bonding modes and procedures. Bonding Modes Manual Setup Menu has individual sections for the bonding processes that must be set. Buttons on the Activation Bar activates the functions. Heating time and temperature – Electrode force – Voltage – Bonding time – Cooling time and temperature– h:mm:ss h:mm:ss h:mm:ss 0-550C 1-7000 N 0-1200 V TIP: Heating time set at 0:00:00 heats unit as fast as possible. 0-550C Automatic Setup Menu enables you to select a written program or create a new program of bonding processes. RUN on the main menu bar activates a loaded program. TIP: Close chamber before proceeding to second wafer to prevent DI water splashing into chamber. Bonding Procedures 1. Position first clean wafer with bonding side facing up on the stage. Use the alignment pegs to center the wafer. 2. On the Activation Bar press FLAGS IN. 3. Close the chamber by pressing and holding both GREEN buttons on bonding panel until chamber has fully closed. 4. Clean second wafer, then open chamber again using the GREEN buttons and place the second wafer facing down using the alignment pegs to position. The flags will keep the wafers separated until the bonding process has been activated. 5. Close the chamber by pressing the GREEN buttons. 6. Log off of CRESS. 33 Document1 Example Of Process Steps For Operation Modes (look at either the Manual column OR the Automatic column for step by step operation. There is no relation between the adjacent blocks in the manual and automatic steps.) Step 1 2 3 4 5 6 7 8 9 10 Manual SETUP Mode Minimize the Automatic Setup Mode submenu Maximize the Manual Setup Mode submenu. Click the PUMP button on Activation Bar. The pump should be on and the Balzers valve pin up. Set parameters on menu: Heating top & bottom time & temperature 0-550C Electrode 1-7000N Voltage 0-1200V Bonding time Cooling top & bottom time & temperature Click H button on Activation Bar to start heating process. If the field electrode has the spring center for the bow pin movement then click WAFER BOW button to move down the pin. Click F button to pull out flags. Click E button on Activation Bar and a submenu will show. (E corresponds to Electrode FORCE) Verify the correct tooling configuration At end of bonding time, click E to release force. (E = Electrode FORCE) Click C button on Activation Bar to start cooling process. Click PUMP button on Activation Bar to turn off the pump The pump should be off and the Balzers valve pin down. 34 Document1 Automatic SETUP Mode Minimize Manual Setup Mode submenu Maximize the Automatic Setup Mode submenu. The process recipe file can be edited or a new process created and named. Click on FILE, select desired process file and click OK. Click RUN and allow the program to complete process View process steps on the PROCESS MONITOR submenu View the processing graph on the RECORDER submenu At the end of the process recipe, minimize AUTOMATIC SETUP submenu. Maximize MANUAL submenu Click PUMP button on Activation Bar to turn off the pump. The pump should be off and the Balzers valve pin down. Do not vent until pin position is verified. Click V button on Activation Bar to vent the bonding chamber. Hold down both GREEN buttons on bonding panel to open chamber. Hold down both GREEN buttons on bonding panel to closed chamber. Do not vent until pin position is verified. 11 12 13 14 15 Click P button on Activation Bar to start nitrogen purge process. Click V button on Activation Bar to vent the bonding chamber Hold down both GREEN buttons on bonding panel to open chamber Remove bonded wafers Hold down both GREEN buttons on bonding panel to close chamber Record use in logbook Remove bonded wafers Record use in logbook For help on automatic scripts and commend definitions, please contact the staff for more details. 35 Document1