Advanced Composites Processing Exercise no. 3 Spring Semester 2012 Exercise no. 3: Liquid Composite Molding – RTM & VARI Model Solution Injection strategies 1. The geometry shown in figure 1 has to be impregnated without dry spots by setting one position for the inlet and another position for the outlet. It was defined, that in this geometry, the inlet and the outlet have to be placed at the outer circle in opponent locations. The challenge is to set the points in such a manner that different flow fronts are meeting in the nodes of the 1D-grid and finally in the position of the vent. Therefore it has to be avoided, that flow fronts will meet between two nodes. For learning purposes, two trials were provided to the students. 2. The main idea is that if two cross sections of different cross sectional area are meeting in one node, the fluid velocity is higher in the thin cross section than in the thick cross section. If an injection is directly at a node, the outflows of this node are decoupled, meaning, the flow velocity in the adjacent 1D-channels is the same. Regarding this information, due to symmetry reasons, the best position for an injection is at the node at the ring adjacent with the 80mm wide domain (see Figure 2). The flow will have approximately the same velocity during the first filling phase. As the distances between the nodes is approximately the same, the flow fronts might meet in the nodes of the ring and the 40 mm domain and 20 mm respectively. A possible problem might appear in the node of the 20 mm domain and the outer ring: As the ratio of widths from 80 to 20 mm is quite high, there is a high risk, that the flow front in the 20 mm wide domain reaches the node adjacent to the circle faster than the outer circle. This problem could be addressed by moving the injection gate a small amount lower than it is displayed in Figure 2. 3. The continuity equation for RTM-processes states, that in a representative volume the sum of inflows is equal to the sum of outflows: 𝑄1 − 𝑄2 = 0. Assuming the same permeability 𝐾1 in the two domains, applying Darcy’s Law at the node leads to − 𝐾1 𝐴1 𝐾2 𝐴2 ∇𝑝1 + ∇𝑝2 = 0 𝜂 𝜂 𝐴 ∇𝑝 ⇔ 𝐴2 = ∇𝑝1. 1 2 which shows that the pressure gradient is higher, if the cross section is lower, therefore also the volume averaged velocity, which is 𝑣𝑖 = 𝑄𝑖 /𝐴𝑖 = − ETH Zurich, Centre of Structure Technology 𝐾1 𝜂 ∇𝑝𝑖 , 𝑖 = {1,2}. C. Di Fratta, B. Louis, F. Klunker Page 1 Advanced Composites Processing Exercise no. 3 Spring Semester 2012 4. The part itself usually showed a flow front pattern as it was expected in the discussions. The challenge, that the flow fronts meet in the node, was not successfully reached in reality. There were minor deviations which can be also due to a)modeling problems (RTM vs VARI) and b) possible edge effects appearing, due to the complex setup. Figure 1. Part geometry. Lengths are in millimeters. ETH Zurich, Centre of Structure Technology C. Di Fratta, B. Louis, F. Klunker Page 2 Advanced Composites Processing Exercise no. 3 Spring Semester 2012 Figure 2: Example of an RTM-flow simulation, where colors represent the fluid pressure and the flow fronts are meeting in the nodes, the injection point is on the right side Material and process parameters sensitivity 1. Sketches will vary. An approximate sketch is as follows: 2. In the lab demonstration experiment, fluid fully impregnates the distribution media (mesh) first. Then the fluid (silicone oil in the lab, resin in real composite processing) flows from the distribution mesh into the fiber perform. This occurs predominantly occurs in the through-thickness direction from the wetted distribution mesh. ETH Zurich, Centre of Structure Technology C. Di Fratta, B. Louis, F. Klunker Page 3 Advanced Composites Processing Exercise no. 3 Spring Semester 2012 3. Sample numbers are provided. Velocities will vary from experiment to experiment. Apparent Flow Front Velocity Injection stage No mesh Mesh (top) Mesh (bottom) Start 5s (0.45cm/s) 3s (2.50cm/s) 4s (1.67/s) Middle 45s (0.11cm/s) 8s (0.50cm/s) 10s (0.31cm/s) End 150s (0.06cm/s) 31s (0.26cm/s) 36s (0.36cm/s) 4. Because fiber wetting occurs predominantly in the through-thickness direction, air entrapment may occur in the corners. This occurs under the following conditions: The top portion of the fiber (or distribution mesh) is wetted out on both the horizontal and vertical flange prior to the in-plane of the fiber being fully impregnated. The progressing flow front (partial saturation) passes from the horizontal flange to the vertical flange, without the fiber being fully saturated. The result is any entrapped air in this region effectively becomes entrapped now by two converging flow fronts: vertical flange, and horizontal flange. Figure 3. Actual in-plane impregnation progress as a result of using distribution media (mesh) in a 90° corner. Effectively, two flow fronts form, and converge at the corner (gravity effect is also present in the vertical flange impregnation). ETH Zurich, Centre of Structure Technology C. Di Fratta, B. Louis, F. Klunker Page 4 Advanced Composites Processing Exercise no. 3 Spring Semester 2012 Figure 4. Resulting air entrapment at 90° corner due to converging flow fronts. Possible strategies to avoid this are as follows: a. Stop the distribution mesh prior to the 90° corner, and let the flow front progress fully impregnate the fiber in the through-thickness direction. This is followed by letting the flow front progress in-plane up the vertical flange. This can be achieved by leaving the vertical flange bare of distribution media. b. Again stop the distribution mesh prior to the corner. However, the distribution mesh may begin again on the vertical flange at some distance away from the corner region. Process monitoring 1. The LCM processes in closed molds (e.g. RTM) can be monitored by suitable a sensing system, using for example cameras, electric sensors, pressure transducers, ultrasound sensors, thermocouples, etc. In this experiment, pressure sensors are used to track the flowfront during the process: when the fluid reach the pressure sensors, their output signals increase; analyzing the pressure values by the sensors and comparing them to value from simulations it is possible to estimate the position of the flow-front. Possible “flow irregularities” can be monitored by an irregular signal from the sensor, in respect to the ideal response. Variations in the flow pattern can be detrimental to the final composite parts, since they can lead to voids or dry spots, resulting in a diminishment of the mechanical qualit: this is why a process should be monitored. 2. “Runners” are flow channels occurring close to edges or boundary of the cavity, usually because a bad alignment of the fabrics inside the mold; this fact leads to a local lack of “material” and so creates channels where the resin can flow faster. If runners are present, they will disturb the flow pattern (the flow is uneven and for example the resin can reach the vent before a full wet-out of the fabrics) and therefore dry spots can arise. Pressure sensors close to a runner will ETH Zurich, Centre of Structure Technology C. Di Fratta, B. Louis, F. Klunker Page 5 Advanced Composites Processing Exercise no. 3 Spring Semester 2012 sense these disturbances by an abnormal increase of fluid pressure, in comparison with other sensors or with ideal flow conditions. 3. At the beginning, the sensor measures only a constant value equal to the fabric compaction pressure in dry state. Then the flow arrives and the pressure decreases initially because the fabric wet compaction pressure is lower than the dry compaction one. In the same time the pressure starts to increase again because of the increasing resin content in the cavity. The actual fluid pressure is equal to zero before the resin arrival, at roughly 100 s, and then, after that point, it can be obtained subtracting dotted line (fabric compaction pressure in wet condition) from the sensor output pressure. Figure 5. Sensor typical response 4. Since it is a 1D (constant) vacuum driven injection, the pressure distribution in the cavity is always linear at any time (see graphics below, with Pi = 1 bar, ΔP = Pi – Pf = 1 bar and xs = 0.55 m). Therefore the following formula can be used to find the flow front xf and approximated values are listed in the table below: PS = Pi − (Pi − Pf ) ETH Zurich, Centre of Structure Technology xs ⇒ xf xf = xs C. Di Fratta, B. Louis, F. Klunker Pi − Pf Pi − Ps Page 6 Advanced Composites Processing Exercise no. 3 Spring Semester 2012 Pi Ps Pf = 0 xi = 0 xs xf Figure 6. Pressure Distribution for each time Time Sensor output pressure Resin pressure Flow-front position 150 s ~0.42 bar 0.37 bar 0.87 m 200 s ~0.50 bar 0.45 bar 1m 250 s ~0.54 bar 0.49 bar 1.12 m 5. In Figure 7, the blue curve corresponds to the constant injection pressure, while the red one is for constant flow rate. These trends can be deducted by the 1D flow solution. Leaving out mathematical formulas, when just looking at Figure 8 (pressure distribution along the laminate at different time), it is noticeable that constant flow rate injection imply a linear growth of pressure in each points of the laminate (and thus also at sensor point), because the injection pressure is linearly increasing with time. In case of constant pressure of injection, instead, it is clear that the more the resin advances, the less will be the increment of pressure at the sensor position. ETH Zurich, Centre of Structure Technology C. Di Fratta, B. Louis, F. Klunker Page 7 Advanced Composites Processing Exercise no. 3 Spring Semester 2012 Figure 7. Resin pressure at sensor location for constant flow/pressure injection Figure 8. Constant injection pressure vs. flow rate ETH Zurich, Centre of Structure Technology C. Di Fratta, B. Louis, F. Klunker Page 8