FIS 40100 Forensic Chemistry I Dr. John Goodpaster Assistant Professor-Forensic and Investigative Sciences Program jvgoodpa@iupui.edu Office: LD 326 H Phone: 274-6881 Prerequisites: FIS 20600. Chemistry C310, C311, C342, C344, C410, C411; FIS majors only Textbook (REQUIRED): Bell, Suzanne. Forensic Chemistry. Indianapolis: Pearson, 2013. Safety: You will need safety glasses. Course Description This course will cover the major techniques and instruments used in the analysis of chemical and pattern evidence commonly encountered at crime scenes. The techniques of gas chromatography, thin layer chromatography, and UV-visible, infrared and Raman spectroscopy will be studied and used extensively. There will be lecture and lab components for each type of instrumental analysis covered in the course. Principles of Undergraduate Learning covered within the course Integration & Application of Knowledge - Meet professional standards and competencies; enhance their personal lives Intellectual Depth, Breadth, & Adaptiveness - Intellectual depth describes the demonstration of substantial knowledge & understanding of at least one field of study; Intellectual breadth is demonstrated by the ability to compare & contrast approaches to knowledge in different disciplines Critical Thinking - Analyze complex issues & make informed decisions Course Content and Goals Module 1 will include 3 units. The overall goal of this module is to have a general understanding of commonly used lab procedures and statistics. Module 1: Unit 1 – General Forensic Laboratory Procedures Demonstrate good laboratory practices used in a forensic science laboratory Identify important techniques for the collection and preserving of evidence Dramatize and apply labeling and collection of different types of evidence 1 Forensic Chemistry I Syllabus J. Goodpaster Module 1: Unit 2 – Statistics Classify the use of statistics in forensic chemistry Select the correct statistical technique for different types of evidence and data Apply statistics in forensic data Module 1: Unit 3 – Sample Preparation Express how sample preparation is applied in forensic chemistry Generalize different types of sampling procedures for evidence Identify what preparation needs to be done for particular types of evidence Complete presumptive tests done in forensic science Module 2 will include 3 units. The overall goal of this module is to understand different types of commonly used instrumental techniques in forensic chemistry and to apply the techniques to evidence. Module 2: Unit 1 – Spectroscopy Classify different types of spectroscopy and their application to forensic evidence Illustrate the parts of a spectrophotometer and their application Produce data using spectrophotometers (e.g., FTIR, UV-Vis-NIR, Raman, and Fluorescence) on forensic evidence Compare and interpret different results from different instrumentation Module 2: Unit 2 – Chromatography Classify different types of chromatography and their application to forensic evidence Illustrate the parts of a chromatograph and their application Produce data using chromatographic systems (e.g., GC, HPLC, and TLC) on forensic evidence Compare and interpret different results from different instrumentation Module 2: Unit 3 – Mass Spectrometry Classify different types of mass spectrometry and their application to forensic evidence Illustrate the parts of a mass spectrometer and their application Produce data using mass spectrometers (e.g., GC/MS and LC/MS) on forensic evidence Compare and interpret different types of forensic evidence results from instrumentation Module 3 will contain one unit. The overall goal of this module is to become familiar with instrumental techniques that use microscopy for examination. This module will cover Phase Contrast microscope, FTIR, UV-Vis, and Raman microscopy. Module 3: Unit 1 – Instrumental Microscopy Explain general spectroscopy techniques that are applied with microscopy Forensic Chemistry I Syllabus J. Goodpaster Prepare samples for instrumental microscopy Differentiate when instrumental techniques are used and needed Identify fibers, paints, glass and inks using instrumental microscopy Class Procedures 1. Attendance and Class Participation: You are expected to be in every class and lab meeting. If you are unable to attend please talk to the instructor as soon as possible. 2. Lecture Material and Reading Assignments: You are responsible to review the section material including lecture material and reading assignments. Some power points will be available for review. You will not be graded on completing this material; however, you will need to learn the information and will be tested on the material. Most of this information will be kept in the Resource tool of OnCourse. 3. Exams: There will be three exams (all worth 100 points) which will cover material that has been discussed since the prior exam. Exams will be short answer and may contain multiple choice, matching, or fill in the blank questions. There will be more discussion about exams as the semester goes on. There will be no makeup exams, please see me if there is an issue with the scheduling. There will also be a final exam worth 200 points covering all the material from the semester as well as the techniques used throughout the semester in lab exercises. 4. Laboratory Grade: This is an important part of the course. Almost one half of your overall grade will come from laboratory work. Included in this are pre-lab exercises, laboratory reports, lab notebook pages, and unknown results. 5. Laboratory Coursework: Pre-lab exercises are due before the start of each lab exercise. Each exercise is worth 10 points and is to be turned into your TA at the beginning of the lab period. Late pre-labs will not be accepted. Laboratory reports and notebook pages are worth a total of 50 points and are due by 5:00 PM one week after completing the lab exercise. Please see the schedule in the lab manual. These are to be turned in to your course supervisor or TA along with copies of your lab notebook pages for that exercise. The late penalty is 3 points per day late. This includes the total grade on report and notebook pages. Unknown results should also be turned in with your report. Late unknown results will result in 1 point per day late. Weekends do not count towards this late penalty. Reports will have a cover sheet to be turned in with each report. These include a break-down of points for the report and unknown result. These cover sheets can be found on OnCourse. 6. Communication: Announcements will be made on OnCourse if there are any changes in course content. To contact me with questions, concerns, or comments please email me directly. I will not use the messaging tool on OnCourse. I will respond to your email within 24 hours, with an exception to email sent Friday evening through Sunday, in which case I will respond to your email on Monday. Forensic Chemistry I Syllabus J. Goodpaster 7. Course Material: In order to read the various documents about this course, you must have Acrobat Reader installed on your computer. It is a free download from the Adobe website. I will also use the 2010 version of Windows. You can either download a patch for Windows 2003 or upgrade to the new version from UTIS website, which I recommend. You will need this to access word documents and power point slides that I post under resources. 8. Internet: YOU MUST HAVE ACCESS TO THE INTERNET USING A BROWSER. All of the course materials including the answers to exams, assignments, news and announcements, last minute changes outlines of my lectures will be kept in an OnCourse CL file for this class. In order to read the various documents about this course, you must have Acrobat Reader installed on your computer. It is a free download from the Adobe website. Grading Points 3 Exams at 100 points Final Exam 7 Pre-lab exercises at 10 points 7 Lab Reports at 50 points 4 Unknown Results at 10 points Total 300 200 70 350 40 960 Grading Scale Your grade will be based on a strict grading scale as outlined below. There will be no curving of final grades. A: 100 – 93% C: 76.9 – 73% A-: 92.9 – 90% C-: 72.9 – 70% B+: 89.9 – 87% D+: 69.9 – 67% B: 86.9 – 83% D: 66.9 – 63% B-: 82.9 – 80% D-: 62.9 – 60% C+: 79.9 – 77% F: less than 60% Forensic Chemistry I Syllabus J. Goodpaster Academic Misconduct (Taken from Academic Handbook, 2001and the Code of Student Rights, Responsibilities, and Conduct) http://www.indiana.edu/~deanfac/acadhbk/acad_handbk_2001.pdf http://www.life.iupui.edu/Who/Dean/Code The Academic Handbook states that faculty members have the responsibility of fostering the “intellectual honesty as well as the intellectual development of students....The faculty member should explain clearly the meaning of cheating and plagiarism as they apply to the course....Should the faculty member detect signs of plagiarism or cheating, it is his or her most serious obligation to investigate these thoroughly, to take appropriate action with respect to the grades of students, and in any event to report the matter to the Dean of Students. The necessity to report every case of cheating, whether or not further action is desirable, arises particularly because of the possibility that this is not the student’s first offense, or that other offenses may follow it. Equity also demands that a uniform reporting practice be enforced; otherwise, some students will be penalized while others guilty of the same actions will go free.” (p. 172). Academic Misconduct: (from the Code of Student Rights, Responsibilities, and Conduct) 1. Cheating: A student must not use or attempt to use unauthorized assistance, materials, information, or study aids in any academic exercise, including, but not limited to, the following: a. A student must not use external assistance on any "in-class" or "take-home" examination, unless the instructor specifically has authorized external assistance. This prohibition includes, but is not limited to, the use of tutors, books, notes, and calculators. b. A student must not use another person as a substitute in the taking of an examination or quiz. c. A student must not steal examinations or other course materials. d. A student must not allow others to conduct research or to prepare work for him or her without advance authorization from the instructor to whom the work is being submitted. Under this prohibition, a student must not make any unauthorized use of materials obtained from commercial term paper companies or from files of papers prepared by other persons. e. A student must not collaborate with other persons on a particular project and submit a copy of a written report which is represented explicitly or implicitly as the student's individual work. f. A student must not use any unauthorized assistance in a laboratory, at a computer terminal, or on field work. g. A student must not submit substantial portions of the same academic work for credit or honors more than once without permission of the instructor to whom the work is being submitted. h. A student must not alter a grade or score in any way. 2. Fabrication: A student must not falsify or invent any information or data in an academic exercise including, but not limited to, records or reports, laboratory results, and citations to the sources of information. 3. Plagiarism: A student must not adopt or reproduce ideas, words, or statements of another person without appropriate acknowledgment. A student must give credit to the originality of others and acknowledge indebtedness whenever he or she does any of the following: a. Quotes another person's actual words, either oral or written; b. Paraphrases another person's words, either oral or written; c. Uses another person's idea, opinion, or theory; or d. Borrows facts, statistics, or other illustrative material, unless the information is common knowledge. Forensic Chemistry I Syllabus J. Goodpaster 4. Interference a. A student must not steal, change, destroy, or impede another student's work. Impeding another student's work includes, but is not limited to, the theft, defacement, or mutilation of resources so as to deprive others of the information they contain. b. A student must not give or offer a bribe, promise favors, or make threats with the intention of affecting a grade or the evaluation of academic performance. Faculty Action If a faculty member has information that one of his/her students committed an act of academic misconduct, the faculty member is required to hold an informal conference with the student. The conference should be prompt and private. If the faculty member concludes that the student is responsible for the misconduct, then the faculty member is authorized to impose an appropriate academic sanction (i.e., lower or failing grade on the assignment, assessing a lower or failing grade for the course). After reporting the information to the Dean of Students, he/she will review the information to determine if additional sanctions should be applied. Sanctions are outlined in the Code of Student Rights, Responsibilities, and Conduct. This document appears on the web at the following address: http://www.life.iupui.edu/Who/Dean/Code/ Policy on Student Academic Misconduct Faculty are required to report all incidents of academic misconduct to the Dean of Students. For information about policies and procedures, including due process requirements, see the Code of Student Rights, Responsibilities, and Conduct, especially part III: Student Misconduct and Part IV: Student Disciplinary Procedures. The code is accessible on the internet at http://www.life.iupui.edu/Who/Dean/Code If you need any special accommodations due to a disability, please contact Adaptive Educational Services at (317)-274-3241. The office is located in CA 001E