Chemical Engineering Society Council of Student Organizations De La Salle University – Manila SEPAPRO QUIZ#4 REVIEWER Questionnaire:............................................................ I. Multiple Choice 1. The rate of leaching decreases as a. Pressure decreases b. Temperature decreases c. Temperature increases d. Both (A) and (C) 2. The unit operation by which soluble components of a liquid mixture are dissolved in a liquid immiscible with the insoluble components is a. Gas absorption b. Solvent extraction c. Leaching d. Adsorption 3. Which of the following factor influences the fraction of liquid retained in the underflow or slude? a. Boiling point of the solvent b. The type of pump used for transferring the underflow c. Fractional recovery of the solute d. None of the above 4. In ideal leaching operation, for constant underflow, the concentration of solute in the overflow is _____ the concentration of the solute in the solution adhering to the inert solid in the underflow. a. Equal to half b. Less than c. Equal to d. More than 5. If the solute concentration (on “solid free basis”) in the overflow and the overflow are not equal, the equilibrium (homogeneity) tie-lines are a. Vertical b. Horizontal c. Inclined to the right d. Inclined to the left 6. Hexane is the most popular solvent for oil extraction from seeds because a. It can be easily removed from the extract to recover the solvent b. It is non toxic c. d. It is miscibke with plabnt/vegetable oils in all proportion All of the above 7. The ideal leaching conditions exist if a. The solute is infinitely soluble in the solvent b. Sufficient contact time for the solvent to penetrate the solute completely is permitted c. The overflow streams contain some inert solids, either by entrainment or by partial solubility in the overflow solution d. Both (A) and (B) 8. Stage efficiency in leaching process depends on a. Vapor pressure of the solution b. Time of contact between the solid and the solution c. Rate of diffusion of the solute through the solid and into the liquid d. Both (B) and (C) 9. In a determination of the solution retention data, the mass fraction of the solute in the extract was determined to be 0.6. The corresponding underflow analysis showed a retention of 0.6 Kg solvent per Kg of the inert solid. The mass fraction of solute in the underflow is most likely a. 0.6 b. 0.47 c. 0.36 d. 0.27 In a salt recovery plant, rock salt is being leached to produce industrial salt in a continuous counter current system consisting of two ideal stages using water as leaching medium. The average composition of the rock salt is: inert = 70%, soluble salt = 25%, moisture =5%, all percentage by weight. The underflow from each stage contains 0.3 Kg of solution per Kg of inert. The plant leaches 50 MT/day of rock salt using 50 MT of water per day. The quantity of soluble salts recovered in MT/day is: a. 12.1 b. 13.1 c. 14 d. 15.2 1 II. Problem Solving Answers:…………............................................................ 1. Three hundred fifty Kg per hour of halibut liver is to be extracted in a counter-current cascade with ethyl ether to recover oil. The ether which has been partially purified contains 2% oil. The freshliver contains 20% oil and is to be extracted to a composition of 2% oil (on a solvent-free basis). Solvent used is 150 Kg per hour. All % are weight %. Use retention/drainage data from Geankoplis page 835, #12.10-4 (right triangular diagram at top of page and xA in a scale up to 0.6 will suffice to place all relevant points in the same graph). a. What % of oil entering with the fresh liver is recovered in the extract? b. How many ideal stages are required? I. Seeds, containing 20% by mass of oil, are extracted in a counter-current plant, and 90% of the oil is recovered in a solution containing 50% by mass of oil. If the seeds are extracted with fresh solvent and 1 Kg of solution in the underflow in association with every 2 Kg of insoluble matter, how many ideal stages are required? II. 2. 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. B B D C C D D D C A 1. Ma a. 92% b. 3.6 stages 2. 5 ideal stages Goodluck sa exam! Kaya niyo yan :) 2