COE Chemical and Biological Engineering Course Description Page CBE 250 - Process Synthesis Catalog Description Textbook(s) and/or other required material R. M. Murphy, Introduction to Chemical Processes: Principles, Analysis, Synthesis, McGraw-Hill, 2005. In-class handouts and readings. Course objectives Students will have: Familiarity with chemical process flowsheeting and common unit operations Ability to apply Mass and Energy Balances to chemical processes and unit operations Understanding of factors involved in a successful chemical process, and ability to suggest possible new processes Topics covered Units, dimensions Flow charts Material balances Recycle, bypass, purge Material balances on reacting systems Combustion processes Elementary phase equilibrium Staged separations - extraction Energy balances - non-reactive and reactive systems Enthalpy contributions - sensible heats, latent heats, heats of reaction Combined mass and energy balances Basic heat exchanger design and application strategies Basic process synthesis (class project) Class/laboratory schedule Meets twice weekly, in 75 minute lectures on Tuesday and Thursday mornings. Section 1: 8:00-9:15; Section 2: 11:00-12:15 Office hours conducted in tutorial mode Monday, Tuesday, Wednesday afternoons modified from CBE 2006 ABET Self-Study B-3 COE Chemical and Biological Engineering Course Description Page CBE 255 – Introduction to Chemical Process Modeling Catalog Description Textbook(s) and/or other required material R. Pratap, Getting Started with MATLAB, Oxford University Press, 2009 Course objectives Students will: - Develop facility with using modern computational software for numerical problem solving Obtain an integrative overview of the entire chemical engineering curriculum Be exposed to key modeling concepts for courses later in the curriculum Acquire a set of tools that will be useful in later CBE courses Be exposed to problems in stoichiometry of chemical reactions, diffusion and heat transfer, process systems steady-state modeling and design, chemical kinetics in well-mixed reactors, staged separations, estimating parameters from data Class/laboratory schedule Meets twice weekly, in 50 minute lectures on Monday and Wednesday mornings. Computer lab 90 minutes, Monday, Tuesday, or Wednesday afternoons modified from CBE 2006 ABET Self-Study B-3 COE Chemical and Biological Engineering Course Description Page CBE 310 - Chemical Process Thermodynamics I Note: this is the new course number for the old CBE 211 (eliminated) Textbook(s) and/or other required material No textbook information "Thermo" 2000 by Jay Schieber and Juan de Pablo Course objectives Students will have: The student will learn the relationship between heat and work by understanding the significance of the first law of thermodynamics. The student will understand the limitations imposed by the second law of thermodynamics on the conversion of heat to work. The student will learn the definitions and relationships among the thermodynamic properties of pure materials, such as internal energy, enthalpy, and entropy. The student will learn how to obtain or to estimate the thermal and volumetric properties of real fluids. The student will understand the applications of energy balances in the analysis of batch, flow, and cyclical processes, including power cycles, refrigeration, and chemical reactors. Topics covered First law of thermodynamics. Volumetric properties and equations of state of pure fluids. Sensible and latent heat effects and heats of reaction. Second law of thermodynamics. Definition of entropy and the third law. Maxwell relations and other relations among properties. Correlations of the thermal and volumetric properties of real fluids. Flow processes. Power cycles. Turbines and jet engines. Refrigeration cycles, heat pumps, and liquefaction of gases. Class/laboratory schedule 3 50-minute lectures/week; Section 1: 9:55 MWF; Section 2: 11:00 MWF 50-minute discussion session; 2:25 M or 1:20 T modified from CBE 2006 ABET Self-Study B-4 COE Chemical and Biological Engineering Course Description Page CBE 311 - Thermodynamics of Mixtures Textbook(s) and/or other required material Elliott and Lira, Introductory Chemical Engineering Thermodynamics, Prentice-Hall, 1st ed, 1999. "Thermo 2000" by Jay Schieber and Juan de Pablo Course objectives Students will have: Ability to apply chemical thermodynamics to systems to determine phase and chemical equilibrium Familiarity with terminology, theory, and common models used to describe solutions and mixtures Topics covered Solution thermodynamics Ideal and Real mixtures Vapor-liquid equilibrium Liquid-liquid equilibrium Vapor-liquid-liquid equilibrium Solid-liquid equilibrium Equations of state Chemical reaction equilibrium Class/laboratory schedule 2 75-minute lectures, TR 8:00 weekly 50-minute discussion section, 1:20 or 2:25 Monday afternoon modified from CBE 2006 ABET Self-Study B-5 COE Chemical and Biological Engineering Course Description Page CBE 320 - Introductory Transport Phenomena Textbook(s) and/or other required material Bird, Stewart and Lightfoot, Transport Phenomena, 2nd ed. rev., Wiley, 2007. Course objectives The objectives of this course are for students to learn to: Set up shell balances for conservation of momentum, energy, and mass; understand and apply flux laws in balances; understand and apply interphase transport relationships; employ shell balance equations to obtain desired profiles for velocity, temperature and concentration; reduce and solve the appropriate equations of change to obtain desired profiles for velocity, temperature and concentration; reduce and solve appropriate macroscopic balances for conservation of momentum, energy and mass; utilize information obtained from solutions of the balance equations to obtain engineering quantities of interest; recognize and apply analogies among momentum, heat and mass transfer; Appreciate relevance of transport principles in diverse applications of chemical, biological, and materials science and engineering. Topics covered Mass, momentum and energy transport mechanisms Calculation of transport coefficients Dimensional analysis Momentum, energy and mass interphase transport Microscopic and macroscopic balances Solution to problems in viscous flow, energy and mass transport Elementary applications Class/laboratory schedule 3 50-minute lectures/week, MWF 8:50-9:40 Recitation section; M 1:20-3:15 or 3:30-5:25 modified from CBE 2006 ABET Self-Study B-6 COE Chemical and Biological Engineering Course Description Page CBE 324 - Transport Phenomena Laboratory Textbook(s) and/or other required material CBE 324 Lab Notes, available online or at Bob's Copy Shop each semester Course objectives Introduces engineering lab practice Develops engineering report preparation and writing skills Demonstrates the basic concepts of transport phenomena Illustrates the application of the macroscopic balances of mass, energy, and chemical species Topics covered Pressure-volume-temperature behavior of gases Viscosities of Newtonian liquids Velocity profiles for turbulent flow Friction factors for flow in circular tubes Efflux time for a tank with an exit pipe Thermal conductivity of solids Temperature profiles on solids Heat-transfer coefficients in circular tubes Heating liquids in tank storage Diffusivity in gases Concentration profiles in a stagnant film Class/laboratory schedule Sections meet weekly for one afternoon (T, W. R, or F) Lecture: 1:20-2:25 Laboratory: 2:25-5:25 modified from CBE 2006 ABET Self-Study B-7 COE Chemical and Biological Engineering Course Description Page CBE 326 - Momentum and Heat Transfer Operations Catalog Description 326 Momentum and Heat Transfer Operations. I, II; 3cr. Analysis of chemical engineering operations involving fluid flow and heat transfer. Flow of fluids through ducts and porous media; motion of particulate matter in fluids; general design and operation of fluid-flow equipment. Conductive, convective and radiative heat exchange with and without phase change; general design and operation of heat-exchange equipment. P:CBE 310 & 320 with grades of C or better. Graham, Klingenberg, Swaney. Course Prerequisite(s) CBE 211 CBE 320 with grades of C or better Prerequisite knowledge and/or skills Chemical Process Thermodynamics Transport Phenomena Textbook(s) and/or other required material McCabe, Smith, and Harriott, Unit Operations of Chemical Engineering, 7 th ed., McGraw-Hill, 2007. Bird, Stewart, and Lightfoot, Transport Phenomena, Wiley, 1960. Holman, Heat Transfer, 5th Edition, McGraw-Hill, 1981 Coulson, Richardson, Sinnott, Chemical Engineering, Vol 6, 2nd Edition, Pergamon Press, 1993 van Dyke, An Album of Fluid Motion, Parabolic Press, 1982 Course objectives Ability to apply thermodynamics and transport phenomena to analyze and design chemical process equipment. Familiarity with the theory and design equations describing common chemical engineering process equipment. Topics covered Dimensional Analysis and Scale-Up Mechanical Energy Balances Flow of Incompressible Newtonian and Non-Newtonian Fluids Flow of Compressible Fluids Flow Measurement Pumps, Compressors, Fans and Blowers Two Phase Flow Drag Coefficients and Settling Packed Beds, Fluidized Beds, and Filtration Cyclones and Centrifuges Agitation and Mixing Conduction in Solids Heat Transfer Coefficients modified from CBE 2006 ABET Self-Study B-8 Forced and Free Convection Boiling and Condensation Heat Exchangers Evaporators Radiation Class/laboratory schedule 3 50-minute lectures, 12:05 MWF 50-minute discussion session, 2:25 W or 1:20 R modified from CBE 2006 ABET Self-Study B-9 COE Chemical and Biological Engineering Course Description Page CBE 424 - Operations and Process Laboratory Catalog Description 424 Operations and Process Laboratory. SS; 5cr. Experiments in unit operations, and supervised individual assignments selected from areas such as: fluid dynamics, analytical methods, reaction kinetics, plastics technology, and use of computers in data processing and simulation. P: CBE 324, 326, 426, & 430, or cons inst. Hill, Root, Swaney. Course Prerequisite(s) CBE 324 CBE 326 or 426 Textbook(s) and/or other required material Laboratory manual, to be purchased at Bob's Copy Shop at the start of the lab session Course objectives developing familiarity with a range of common chemical engineering equipment through experiments on pilot-scale apparatus acquiring or expanding abilities to take a novel project assignment, define an investigation, design and construct experimental apparatus, collect and analyze data, and present conclusions and recommendations in oral or written formats Topics covered Distillation (Formal) Chemical Reactors (Formal) Heat and Mass Transfer in a Spray Tower (Formal) Heat Exchangers (Formal) Fluid Flow - Pump and Flowmeters (Formal) Freeform experiments (4 Informals) Data analysis and report writing Class/laboratory schedule Course meets for 5 weeks, 5 days/week, 8 hours/day in Summer Sessions only. Assessment of student progress toward course objectives Written reports (8 x 10%) Oral report (10%) Mandatory report rewrite (10%) Person(s) who prepared this description Thatcher W. Root modified from CBE 2006 ABET Self-Study B-10 COE Chemical and Biological Engineering Course Description Page CBE 426 - Mass Transfer Operations Catalog Description 426 Mass Transfer Operations. I, II; 3cr. Analysis of chemical engineering operations involving mass transfer. Differential and stagewise separation processes; simultaneous heat and mass transfer; mass transfer accompanied by chemical reaction; general design and operation of mass-transfer equipment. P:CBE 311 & 320 with grades of C or better. Murphy, Yin. Course Prerequisite(s) CBE 311 CBE 320 with grades of C or better Prerequisite knowledge and/or skills Phase equilibrium Material and energy balances Equation of continuity Fick's law Textbook(s) and/or other required material McCage, Smith, and Harriott, Unit Operations of Chemical Engineering, 7 th ed., McGraw-Hill, 2005. Mass Transfer: Fundamentals and Applications A.L. Hines and R. N. Maddox Course objectives Develop familiarity with major chemical process separations units. Apply appropriate criteria for selecting among alternative separation technologies. Complete design calculations for equilibrium staged separation processes (e.g., distillation, absorption). Complete design calculations for differential contactors. Apply mass transfer fundamentals to calculate rates of mass transfer for practical situations and to identify rate-limiting processes. Topics covered Selection of separation technology Phase equilibrium review Single-component absorption - graphical methods Binary distillation - graphical methods Liquid-liquid extraction - graphical methods Multicomponent absorption Multicomponent distillation Review of Fick's law Equation of continuity - applications Mass transfer coefficients Interphase mass transfer Differential contactors Adsorption modified from CBE 2006 ABET Self-Study B-11 Simultaneous heat and mass transfer Membrane processes Class/laboratory schedule 3 50-minute lectures, 9:55 MWF 50-minute discussion session, 1:20 M or T Person(s) who prepared this description Regina M. Murphy modified from CBE 2006 ABET Self-Study B-12 COE Chemical and Biological Engineering Course Description Page CBE 430 - Chemical Kinetics and Reactor Design Catalog Description 430 Chemical Kinetics and Reactor Design. I, II; 3 cr. Analysis and interpretation of kinetic data and catalytic phenomena; application of basic engineering principles to chemical reactor design. P: CBE 311 & 320 or cons inst. Dumesic, Hill, Mavrikakis, Rawlings, Root. Course Prerequisite(s) CBE 311 CBE 320 Prerequisite knowledge and/or skills Ordinary differential equations Thermodynamics of open systems and chemical reactions Elementary chemical kinetics Transport phenomena Ability to use spreadsheets, equation solvers, and computer languages to analyze, manipulate, and plot data in a variety of formats Textbook(s) and/or other required material J. Rawlings and J. Ekerdt, Chemical Reactor Analysis and Design Fundamentals, 1st ed., Nob Hill, 2004. C. G. Hill, Jr., Introduction to Chemical Engineering Kinetics and Reactor Design, Wiley, 1977 Course objectives To develop the ability to analyze kinetic data and determine rate laws To obtain the ability to apply ideal reactor models To provide meaningful experience in solving mass and energy balances for chemical reactors To develop the ability to analyze the performance of reactors in which multiple reactions are occurring To develop the ability to analyze nonideal flow conditions in reactors and to develop the skill to utilize simple models to characterize the performance of such reactors To obtain the ability to analyze data for heterogeneous catalytic reactions and to employ the results of such analyses in designing simple reactors To develop the ability to analyze situations in which heterogeneous reactions are limited by diffusion or mass transfer processes Topics covered Review of thermodynamics and basic concepts Analysis of kinetic data Theoretical foundations of chemical kinetics (reaction mechanisms, collision theory, transition state theory, explosions) Analysis of complex reaction networks Design of ideal isothermal reactors Selectivity and optimization Temperature and energy effects modified from CBE 2006 ABET Self-Study B-13 Nonideal reactors/residence time considerations Adsorption and heterogeneous catalysis Role of mass transfer phenomena in catalytic reactions Class/laboratory schedule Class meets MWF, from 8:50-9:40 a.m. Discussion period M or T 2:25 Person(s) who prepared this description James B. Rawlings modified from CBE 2006 ABET Self-Study B-14 COE Chemical and Biological Engineering Course Description Page CBE 440 - Chemical Engineering Materials Catalog Description 440 Chemical Engineering Materials. I, II; 3cr. Structure and properties of metallic and nonmetallic materials of construction; interrelations between chemical bonding, structure, and behavior of materials. P: Chem 345. Dumesic, Kuech, Root. Course Prerequisite(s) Chem 345 Textbook(s) and/or other required material White, Physical Properties of Materials, 2nd ed., CRC Press, 2012. Ralls, Courtney, and Wulff, Introduction to Materials Science and Engineering, Wiley & Sons, 1976 Course objectives Provide a survey of materials properties Establish the connection of microscopic and chemical principles with macroscopic and physical properties Study the structure and properties of metallic and nonmetallic materials of construction Understand the interactions between chemical bonding, structure, and behavior of materials Topics covered Elements, compounds, and bonding Solid structure, crystallography, X-ray diffraction Phase equilibria and transformations Electrical, thermal, and magnetic properties Metals, inorganic materials, polymers, and composites Structural imperfections: defects, dislocations, grain boundaries Mechanical properties: deformation, strength and fracture, creep and relaxation Interfacial phenomena: surface tension, contact angles, wetting, lubrication Optical properties: index of refraction, fiber optics, lasers Materials processing techniques, materials safety data sheets (MSDS), ASTM tests Class/laboratory schedule 2 75-minute lectures, TR 8:00-9:15 Person(s) who prepared this description Thatcher W. Root modified from CBE 2006 ABET Self-Study B-15 COE Chemical and Biological Engineering Course Description Page CBE 450 - Process Design Catalog Description 450 Process Design. I, II; 3cr. Analysis and design of chemical processing systems and equipment. P:CBE 326, 426 & 430 or cons inst. Swaney, Nealey, Murphy. Course Prerequisite(s) CBE 326 CBE 426 CBE 430 Prerequisite knowledge and/or skills Momentum and heat transfer operations Mass transfer operations and separation processes Chemical reaction kinetics and reactor design Textbook(s) and/or other required material Ulrich and Vasudeva, Chemical Engineering Process Design and Economics: A Practical Guide, 2nd ed., Process Publishing, 2004. Recommended: Towler and Sinnott, Chemical Engineering Design, Second Edition: Principles, Practice and Economics of Plant and Process Design, Butterworth-Heinemann, 2012. Extensive supplementary reference list Course objectives Development of system design skills for chemical processes Experience solving a complex engineering design problem Ability to perform economic evaluation of chemical processes and capital projects, and economic optimization of designs Familiarity with professional conventions and formats for representing engineering results Integrated application of chemical engineering knowledge acquired in prior courses Topics covered Economic Analysis Process Synthesis Shortcut and computer-aided design methods Optimization Risk and safety Design project Class/laboratory schedule 2 50-minute lectures, 9:55 TR 3 hour discussion/lab session, 1:20-4:20 T, W, R, or F Person(s) who prepared this description Thatcher W. Root Ross E. Swaney modified from CBE 2006 ABET Self-Study B-16 COE Chemical and Biological Engineering Course Description Page CBE 470 - Process Dynamics and Control Catalog Description 470 Process Dynamics and Control. I, II; 3cr. A systematic introduction to dynamic behavior and automatic control of industrial processes; lab includes instrumentation, measurement and control of process variables by using conventional hardware and real-time digital computers. P: CBE 326 & ECE 376; CBE 430 or con reg. Graham, Swaney, Rawlings. Course Prerequisite(s) CBE 326 CBE 430 ECE 376 Prerequisite knowledge and/or skills A working knowledge of computer programming is also assumed. Textbook(s) and/or other required material "Process Dynamics, Modeling and Control" by B.A. Ogunnaike and W.H. Ray, Oxford Press, 1994. Laboratory Manual Course objectives Objective 1: Introduce undergraduate chemical engineers to dynamics and control of chemical processes. Individual outcomes include: a. Ability to identify, formulate, and solve linear chemical process dynamics problems. b. Ability to use techniques, skills, and modern engineering tools necessary for the practice of chemical engineering. Computational tools especially are emphasized in this course. c. Ability to design and conduct laboratory experiments, as well as to analyze and interpret data, in particular to determine the efficacy of control designs. d. Ability to design a control system to meet desired needs for a given process. e. Capacity for continuing development in understanding and expertise in process dynamics and control. Objective 2: The course is evenly divided between modeling and analysis of chemical process dynamic behavior, and design and analysis methods for automatic control. Individual outcomes include: a. Understanding of professional and ethical responsibility, including knowledge of contemporary issues, particularly those of safety and environmental impact that are directly affected by control system design. b. Ability to function on multi-disciplinary teams, and ability to communicate effectively, through laboratory experience, teamwork, and laboratory project reports. modified from CBE 2006 ABET Self-Study B-17 Topics covered Linear system dynamics Block diagrams, feedback control Process identification Stability: Routh criterion, root locus, Bode, Nyquist Tuning: Xiegler-Nichols, Cohen&Coon Cascade control Feedforward control Multivariable control: linear systems, feedback, interaction, loop pairing, interaction compensation Time delay compensation Discrete time systems Ratio control, overides, selectors, adaptive control Model-based control Class/laboratory schedule 2 50-minute lectures, 11:00 TR 50 minute discussion, 3 hour laboratory; 1:20-5:25 M, T, W, or R Person(s) who prepared this description Michael D. Graham Thatcher W. Root modified from CBE 2006 ABET Self-Study B-18 COE Chemical and Biological Engineering Course Description Page CBE 540 - Polymer Science and Technology Catalog Description 540 Polymer Science and Technology. I, II; 3cr. Synthesis, properties, and fabrication of plastic materials of industrial importance. P: Chem 345; CBE 326 & 430, or con reg; Stat 324; or cons inst. dePablo, Nealey. Course Prerequisite(s) CBE 326 CBE 430 Chem 345 Textbook(s) and/or other required material Young and Lovell, Introduction to Polymers, 3rd ed., CRC/Taylor Francis, 2011. Young, R. A., and Lovell, P. A., "Introduction to Polymers," Second Edition, Chapman and Hall, 1991. Course objectives To acquire fundamental chemical and physical information on the synthesis, production and characterization of polymer materials To appreciate the breadth of polymer properties and applications, and to learn in depth about polymers in a particular application area Topics covered Polymerization and reactions of polymers - condensation, addition, copolymerization, novel reactions Structure and properties of polymers - polymer solution thermodynamics, measurement of molecular weight and size, morphology and order in crystalline & amorphous polymers, polymer flow and rheology, laboratory equipment and demonstration Polymer processing and fabrication - film and molding technology, fiber technology, laboratory equipment and demonstration Commercial polymers (production and applications) - olefins, dienes, vinyl and vinylidene polymers and copolymers, heterochain polymers, fluorocarbon polymers, specialty polymers, laboratory equipment and demonstration Class/laboratory schedule Monday, Wednesday, Friday 11:00-11:50 Person(s) who prepared this description W. Harmon Ray modified from CBE 2006 ABET Self-Study B-19 Catalog Description 541 Plastics and High Polymer Laboratory. I, II; 1-3 cr (P-A). Experiments on polymerization, fabrication, and testing of plastics. P: CBE 540 or con reg; or Chem 664 or con reg. Bray, dePablo, Klingenberg, Nealey. Course Prerequisite(s) ▪ See catalog description. Course objectives Our recently modernized polymer lab gives students access to one of the best educational facilities of this type in the country. Here they are trained in modern methods of polymer characterization. The course emphasizes polymer synthesis, characterization and structure-property relationships. It consists of several weeks of training on each of the instruments followed by group research projects. Topics covered ▪ Differential scanning calorimeter ▪ High-precision solution calorimeter ▪ Thermal gravimetric analyzer ▪ Dynamic mechanical analyzer ▪ Gel permeation chromatograph ▪ Controlled stress rheometer ▪ Capillary viscometer ▪ X-ray spectro-photometer with an area detector modified from CBE 2006 ABET Self-Study B-20 Catalog Description 544 Processing of Electronic Materials. (Crosslisted with E C E, M S & E 544.) Irr; 3cr. Physics and chemistry principles underlying microelectronic materials processing. Effects of processing on materials and structures important in microelectronic and opto-electronic devices. P:CBE 440, MS&E 351, ECE 335; or cons inst. Kuech. Course Prerequisite(s) ▪ See catalog description above. Prerequisite knowledge and/or skills ▪ Introductory Materials Science ▪ Introductory Physics and Chemistry Textbook(s) and/or other required material ▪ Process Engineering Analysis in Semiconductor Device ruFabrication, S. Middleman and A.K. Hochberg, McGraw-Hill. ▪ Selected literature and textbook selections Course objectives This course addresses the basic chemical and physical techniques used in the modern processing of materials at the micro and nanoscales particularly in the microelectronics industry. Simple device concepts are developed and used to relate the influence of the process technology to the device fabrication and materials characteristics. The relation between the properties of a deposited thin film and the deposition process is developed. The underlying physical and chemical features common to many of these processes is emphasized. While focusing on techniques used for the development of both Si and compound semiconductor-based technologies, the use and extension of these processing techniques to other types of materials is developed. Topics covered ▪ Introduction to materials ▪ Physical deposition ▪ Ion beam modification of materials ▪ Lithography ▪ Chemical vapor deposition ▪ Dielectric formation ▪ Reaction-diffusion based processing ▪ Etching processes ▪ Epitaxial growth ▪ Plasma processes ▪ Packaging materials. modified from CBE 2006 ABET Self-Study B-21 Class/laboratory schedule 3 50-minute lectures, MWF 9:45-10:45 modified from CBE 2006 ABET Self-Study B-22 CBE 575 – Instrumental Methods Information to follow. modified from CBE 2006 ABET Self-Study B-23