Nanofabrication and Devices (in ECE and ME Departments) John Melngailis Department of Electrical and Computer Engineering & Institute for Research in Engineering and Applied Physics. University of Maryland, College Park Nanofabrication - electron beam lithography, (SEM with beam writing software, 20nm min. features) C.H. Yang - focused ion beam, milling, induced deposition, etching, and implantation, 5-10 nm minimum beam diameter, ~30nm features milled. K. Edinger, A. Stanishevsky, J. Orloff and J. Melngailis - deep reactive ion beam etching, D. DeVoe - aligner/bonder, R. Ghodssi - new Engineering & Applied Sciences Bldg. (6000 sq. ft. class 1000, clean room), ready May,04 Engineering and Applied Sciences Building Clean room floor plan 6000sq. ft. Class 1000 Space Cross section view of clean room and subfab FIB facilities Micrion FIB-2500 system with 50 kV Ga+ source and 5nm minimum beam diameter Nanofab 150 kV FIB system with alloy ion sources used for implantation of semiconductor devices FEI-620 30 kV Dual-Beam SEM/FIB with Ga+ ion source FIB patterning of diamond films Patterned CVD diamond microcrystal A. Stanishevsky, Univ. of Trenches focused-ionbeam milled in a diamond film. 30nm wide, 600nm deep Focused Ion Beam Milled Cross Section of Part of an Integrated Circuit FIB/SEM fabricated NanoProbes Klaus Edinger Ion Beam Shaving SNOM probe Electrochemical probe Electron Beam Induced Deposition Scanning Thermal Probe AFM / MFM Probe LIBRA Focused Ion Beam Milling Scanning Gas-Nozzle “Nano-jet” Focused Ion Beam Implantation Scanning Electric Field Probe Nanodevices-Electronic & optical • quantum (C. H. Yang, et. al.) • modeling: nanoMOSFET’s, carbon nanotubes (N. Goldsman & G. Pennington) • magnetic storage (R. Gomez, et al.) • FIB implanted JFET (A. DeMarco & J. Melngailis) • single photon tunneling (I. Smolyaninov & C. Davis) Nanoelectronics Research C.H. Yanga, M.J. Yangb, Andy Chenga, Philip Changa, and J.C. Culbertsonb aDepartment of Electrical and Computer Engineering,University bNaval Research Laboratory, Washington DC of Maryland, College Park, Maryland Fabricated 30 nm conducting InAs wires by L (I) MBE growth of heterojunctions, (II) electron beam lithography and (III) wet etching W le l Observed: 1D pure metal regime: W < le < l Ballistic regime: L < le < l Nanoelectronics Research C.H. Yanga, M.J. Yangb, Andy Chenga, Philip Changa, and J.C. Culbertsonb aDepartment of Electrical and Computer Engineering,University bNaval Research Laboratory, Washington DC of Maryland, College Park, Maryland Fabricated 100 nm diameter conducting InAs ring, and observed quantum interference due to wave-like electron transport. Left: AFM topography Below: Magnetoresistance Numerical Boltzmann/Schrodinger Equations: CAD .. of Quantum Effects in Nanoscale Semiconductors Neil Goldsman, ECE Dept. UMCP Flow Chart Band Diagram Quantum Domain Dispersion Relation of QM Well Numerical Boltzmann/Schrodinger Equations: CAD of Quantum Effects in Nanoscale Semiconductors .. Neil Goldsman, ECE Dept. UMCP Numerical Subthreshold Characteristics Current Vector(SHBTE) I-V Charactistics Current Vector(QM-SHBTE) Design and Theory of Carbon Nanotube Diodes by Gary Pennington and Neil Goldsman ECE Department University of Maryland •Results: Using the tube diameter dependence of the effective mass, band offset, dielectric constant, and hole concentration for an array of Y-junction multiwalled carbon nanotubes, we determined an theoretical analytical formula the junction current as a function of constituent tube diameters. Array of Y-junction carbon nanotubes -V Experiment: C. Papadopoulos et al., Phys. Rev. Lett 85, 3476 (2000). Demonstration of current-induced domain wall motion for novel magnetic device applications Mechanism: s-d exchange interaction L. Gan, S.H. Chung, K. Aschenbach, M.Dreyer and R.D. Gomez, IEEE Transactions on Magnetics 36, 3047, 2000. Ballistic Nanocontact Magnetic Random Access Memory R.D. Gomez, et al., Laboratory for Physical Sciences, College Park MD R.D. Gomez, Department of Electrical andMD Computer Engineering and University of Maryland, College Park, Demonstration of Fabrication and Characterization of Single Domain Magnet Arrays Topography of interacting NiFe island arrays H. Koo and R.D. Gomez, IEEE Transactions on Magnetics 37. Ballistic Nanocontact Magnetic Random Access Memory R.D. Gomez, Department of Electrical and Computer Engineering Single-Photon Tunneling I.I. Smolyaninov, C.Davis et.al. ECE Dept. to PMT fiber 3BCMU gold film pinhole pr ism 632 nm light Schematic view of our experimental setup. Small smart systems &MEMS • Don Devoe- mechanical resonators… • Reza Ghodssi- III-V MEMS, MEMS_VLSI integration • Elisabeth Smela- polymer mEMS High-Q Piezoelectric Nanomechanical Filter Arrays • Functional filter banks based on nano-scale piezoelectric NEMS structures: – orders-of-magnitude size reduction compared to SAW devices – direct integration with VLSI (ZnO) and high-speed electronics (AlAs) – low power operation • Applications in miniature RF communications, spectrum 105 HTS analyzers, etc. 104 Thin Crystal piezo NEMS. Thin Film 103 Q Dielectric Planar DielectricLumped 102 Element 10 1 10-10 10-8 10-6 10-4 Volume (cm3) 10-2 1 10+2 Piezoelectric resonator scaling Input Signal Top Pt Bottom Pt Output Signal ~~ 34 34m m Deep Deep Trench in Si PZT SiO22 L=200nm gap=L/10 L=30nm gap=20nm f=60MHz f=3GHz Mechanical & thermal devices • Hugh Bruck - funcionally graded materials • Klaus Edinger - scanning thermal nanoprobe *>150. 0° C Functionally Graded Smart Thin Film 5 mm 145.0 140.0 Mf >Troom Ms <Troom ATC 1200 SPUTTERING MACHINE 135.0 130.0 Functionally Graded Smart Thin Film 125.0 *<123. 7° C Out-of-plane Displacement “Microbubble” 1 mm 150.0 Infrared Temperature Field Microdevice Performance Characterization “Micropump” Fabrication of Functionally Graded Thin Films Hugh Bruck ME Dept Force Modulation Microscopy Atomic Force Microscopy 1 m Nano Indenter XP Dimension 3000 SPM Nanoscale Material Property and Stress Characterization Film-substrate interface Before Actuation 400 oC T After Actuation s = 100 MPa t Digital Image Correlation U-DISPLACEMENT 100 nm 100 nm z Finite Element Analysis Ms = 43 oC, Mf = 23 oC V-DISPLACEMENT 150 nm 150 nm Nanoscale Structure and Deformation Characterization T = 44 oC r Ms = 3 oC, Mf = -17 oC Microscale Modeling of Device Performance Scanning Thermal Probe Klaus Edinger LIBRA Me3 MeCp Pt precursor deposits a Pt/carbon mixture Filament diameter ~ 30 nm Tip end radius < 20 nm Height: 2-5 m Nanofabricated Scanning Thermal Probe Klaus Edinger, LIBRA LIBRA •Passive mode: the resistance of the wire in contact with the sample is measured, using a low current temperature mapping •Active mode: the wire is heated by applied an AC-current mapping of thermal conductivity and diffusivity. • Free-standing 20-50 nm Pt “wire” grown by electron beam induced deposition from an organometallic precursor gas on an AFM type cantilever. • Low thermal mass; high sensitivity; high spatial resolution Topographic image (left): Only the metal leads are visible. The two buried resistors are indicated by the dotted line. Temperature image (right): The two buried resistors (heating current ~2mA) are visible. Summary • nanofabrication capabilities (e-beam/SEM, focused ion beam, MEMS, new EAS Building with clean room) • nanodevices: electrical & optical • nanoMEMS • mechanical and thermal devices