SEMILAB’s PRODUCTS for the SEMICONDUCTOR INDUSTRY SEMILAB Semiconductor Physics Laboratory, Inc. Prielle Kornelia u. 2, H-1117 Budapest, Hungary Tel:36-1-382-4530 Fax: 36-1-382-4532 E-mail: semilab@semilab.hu Web site: www.semilab.com www.semilab.com Semicond - 1 Semiconductor Characterization Systems Wafer Mapping Tools Bulk Microdefect Analyzer Deep Level Spectrometer for high speed, high resolution whole wafer mapping of defects and/or contaminants for imaging of extended defects (from 20nm to several micron) for identification of electrically active point defects Resistivity Tester p/n Tester for non-contact determination of bulk resistivity for non-contact determination of conductivity type (p or n) of the material in blocks and feedstock material in wafers www.semilab.com Semicond - 2 Wafer Mapping Tools WT-2000 Wafer Tester monitoring defects and contamination both in the bulk and in the surface region of silicon wafers Applied measurement techniques: m-PCD for bulk Si Charge-PCD for bare wafers EpiTest for epi wafers SPV for bulk Si V-Q for oxide characterization Eddy current for resistivity mapping www.semilab.com Semicond - 3 In-line Monitoring Tool WT-3000 model for in-line contamination monitoring • SPC product wafer • Iron contamination mapping - 10x faster than SPV • Full wafer monitoring due to high mapping speed • Integrated minienvironment including FOUP loadport, robot and pre-aligner Fe Fe Fe www.semilab.com Semicond - 4 WT-2000 m-PCD Tool m-PCD (microwave photoconductive decay) technique for mapping crystal growth and process induced defects and heavy metal contamination in bulk silicon wafers APPLICATIONS CRYSTAL GROWTH DEFECTS Laser Microwave wafer I = I0 e-t/t Slip lines Oxygen striations OSF ring PROCESS INDUCED DEFECTS/Fe MAPPING Fe Fe Fe Contaminated vacuum chuck www.semilab.com Boat contamination Fe detection Semicond - 5 WT-2000 SPV Tool Surface Photovoltage (SPV) technique for mapping heavy metal contamination and crystal defects in the bulk silicon wafer IRON CONCENTRATION MAPPING F/VSPV 4 1 3 NFe = C ( 1 1 Lafter2 - 1 Lbefore2 ) Lifetime, ms 2 L Fe AND O2 MONITORING BY COMBINED m-PCD AND SPV TECHNIQUES Fe-B pair O2 prec. 0.1 0.01 1.E+11 1/a m-PCD SPV 1.E+13 1.E+15 1.E+17 Injection level, 1/cm3 F = C(L+1/a) VSPV oxygen SPV iron m-PCD Fe www.semilab.com Semicond - 6 WT-2000 Charge-PCD Semilab’s patented new surface passivation method applying controlled charge deposition on to the wafer surface during lifetime mapping provides a highly efficient, reproducible and homogeneous surface recombination elimination on bare wafers. Lifetime map measured with charging without charging Laser Microwave Charging wafer Charging 1 tmeas 1 1 1 + t +t =t bulk diff surf taverage=15.7 ms taverage=268 ms Surface /interface characterization Interface recombination velocity map of an oxidized wafer calculated from the lifetime map measured with and without charging on the same wafer www.semilab.com Semicond - 7 WT-2000 V-Q Tool Fast, non-contact measurement technique, that replace the traditional contact C-V measurements for qualifying the oxide/interface in silicon wafer Electrical oxide thickness Non-contact V-Q combines three non-contact methods: Charge Light/Kelvin probe ........... SPV, V Theoritical 0.5 Darkcorrected bright -0.5 100 • Corona discharge • Kelvin Probe • Illumination o 1 0 o 26 A 0 Charge, nC/cm2 100 Tox Vfb Dit Qm Vox Qeff Etunnel Vs Vsurf Vtunnel Electrical oxide thickness Flatband voltage Interface state density Mobile charge Oxide voltage Effective charge Tunelleing electric field Surface potential Surface voltage Tunnel voltage www.semilab.com 24 A Etunnel -11V -6.8V Semicond - 8 WT-2000 Epitest Improved m-PCD (microwave photoconductive decay) technique for the characterization of recombination processes in epi structures. Lifetime map Light excitation Green laser 532nm Oxide or passivation Ssurface Epi layer Sinterface Fe concentration map Microwave tep i tsubstrate p+ or n+ substrate 13.8ms www.semilab.com 14.8ms 5 E9 1/cm3 3 E10 1/cm3 Semicond - 9 WT-2000 Resistivity Mapper Non-contact whole wafer resistivity mapping based on the eddy current technique for the determination of bulk resistivity distribution in silicon wafers Resistivity map Head height control Control electronics Single crystal 8” CZ wafer Multi-crystalline PV material High frequency coil www.semilab.com Semicond - 10 WT-2000 MCT Temperature Dependent Lifetime Monitoring minority carrier lifetime as a function of temperature in narrow band gap semiconductors (InSb, HgCdTe, etc.) Two measurement strategies: • whole wafer mapping at a preselected stabilized temperature between 85K and 300K • single point lifetime plot as a function of temperature between 85K and 300K Temperature dependent carrier lifetime measurements 0.16 HgCdTe InSb 0.14 0.5 sa m p le 1 sample#2 sample#4 sa m p le 2 0.4 0.12 0.3 0.10 0 .1 Lifetime [µs] Lifetime [µs] L ife tim e [µ s] 1 0.2 0.08 0.06 0.1 0.04 0 .0 1 50 100 150 T e m p e ra tu re [K ] 200 250 50 100 150 200 250 Temperature [K] 0.02 100 150 200 250 Temperature [K] www.semilab.com Semicond - 11 300 SIRM-300 Bulk Microdefect Analyzer Non-contact, non-destructive method based on reflection mode confocal microscopy for detection and analysis of bulk microdefects Dislocations Stacking fault laser beamsplitter detector Denuded zone determination Z scanning wafer X-Y scanning depth www.semilab.com Semicond - 12 Light Scattering Tomograph Micro- and Grown-in Defects Analyzer The BMDs scatter the incident light which is recorded by a CCD camera near to the cleaved edge of the sample •High Sensitivity - Detectable Particle Size down to 10 nm •High Depth Resolution - 0.5 μm •High Measurement Speed, 50 sec/2mm x 400 μm •Fully automatic operation including half wafer handling •Stabilized Laser Wavelength •Variable Laser Power Near surface analysis surface 5mm Cumulative BMD number 0 50 100 150 200 Depth [µm] 0 10 DNZ depth: 18.9µm y=0.2508x+18.896 20 R2 = 0.9969 30 40 Denuded zone determination 50 60 www.semilab.com Semicond - 13 DLS-83D Deep Level Spectrometer Detection and identification of trace level of impurities in concentrations down to 109 atoms/cm3 Radiation defects in n-type FZ silicon in p-type FZ silicon Cs-Sii-Cs Ps-Ci(1) Vac-Vac Ps-Ci(2) P-Vac Vac-Vac Vac-O CRYOSTATS IN DIFFERENT TEMPERATURE RANGES • Closed Cycle He-cryostat from 20K to 300K • LN2 cryostats from 77K to 450K: simple bath type LN2 cryostat automatic LN2 cryostat with controlled LN2 flow ? Ci Cs-Oi or C-O-V2 Vac-? Influence of annealing on Fe-B pairs Molybdenum SAMPLE HOLDER Fe-interstitial Fe-B pair with motor driven positioning www.semilab.com Semicond - 14 Epimet Fast, Repeatable Measurements Without Wafer Damage Epimet delivers the industry’s first realtime, non-contact method to measure epi layer resistivity profiles in production. Fast feedback and the availability of resistivity profile plots and wafer maps aid in troubleshooting for still higher control over epi processes. Resitivity profile measured by Epimet www.semilab.com Semicond - 15 Surface Charge Analyzer SiO2 + - Wd p-type silicon Depletion width, Wd(mm) The Surface Charge Analyzer allows real-time monitoring of contamination and damage in the critical semiconductor manufacturing processes, such as thermal oxidation, CVD film deposition, metallization, and etch processes. Photons (Light) Typical SCA Curve Onset on Inversion Inversion Midgap P-type Oxidized Wafer Nsc Qox Dit Accumulation Induced charge, Qind Wafer maps indicating backstreaming Source Avg Qox: 8E10q/cm2 www.semilab.com Load Avg Qox: 2E11q/cm2 Semicond - 16