See discussions, stats, and author profiles for this publication at: https://www.researchgate.net/publication/331481791 LABORATORY MANUAL FOR HARDNESS TEST Method · March 2019 CITATIONS READS 0 90,133 1 author: Ifeyinwa Obianyo African University of Science and Technology 26 PUBLICATIONS 120 CITATIONS SEE PROFILE Some of the authors of this publication are also working on these related projects: Sustainable and Affordable Building Materials View project Water Resources and Environmental Engineering View project All content following this page was uploaded by Ifeyinwa Obianyo on 03 March 2019. The user has requested enhancement of the downloaded file. LABORATORY MANUAL FOR HARDNESS TEST Department of Materials Science and Engineering, African University of Science and Technology, Abuja. A) ROCKWELL HARDNESS TEST (I) Aim: To determine the Rockwell hardness number of the given Specimen using “Rockwell Hardness tester”. (II) Apparatus: Rockwell hardness testing machine. Diamond cone indentor, ball indentor. Specimens (Hardened steel, Mild steel, Brass, Copper, Aluminium) (III) Theory: Hardness of a material is generally defined as Resistance to the permanent indentation under static and dynamic load. Hardness is the property of the material by which it offers resistance to scratch or indentation. It is the most important property, as the material is subjected to friction and scratch. When a material is required to use under direct static or dynamic loads, only indentation hardness test will be useful to find out resistance to indentation. This test is an indentation test used for smaller specimens and harder materials. In this test indentor is forced into the surface of a test piece in two operations, measuring the permanent increase in depth of an indentation from the depth increased from the depth reached under a datum load due to an additional load. Measurement of indentation is made after removing the additional load. Indentor used is the cone having an angle of 120 degrees made of black diamond. The principle of Rockwell hardness test has to do with the application of a standard load (Based on the type of material) through a standard indentor (cone or ball indentor) for a standard duration of time. The hardness number is directly obtained in the experiment. The Rockwell hardness is derived from the measurement of the depth of the impression EP = Depth of penetration due to Minor load of 98.07 N. Ea = Increase in depth of penetration due to Major load. E = Permanent increase of depth of indentation under minor load at 98.07 N even after removal of Major load. Suitable Application: Rockwell hardness test is generally used for larger sample geometries. It is a ‘quick test’ mainly used for metallic materials. It can also be used for advanced tests, such as the Jominy (end quench) test (HRC). (IV) Equipment Description: Figure 1: Rockwell hardness testing machine. (V) Procedure: a) Keep the loading and unloading lever at position “A” which is unloading position. b) Select suitable indentor & weights according to the scale. c) Place the specimen on testing table anvil. d) Turn the hand wheel to raise a job until it makes contact with indentor & continue turning till the longer pointer at the dial gauge makes 2 ½ rotations. Then it stops at zero continue turning slowly till the small pointer reaches the red spot at 3‟, this is automatic zero setting dial gauge. e) Turn the lever position “A” to “B” i.e. from unloading to the loading position. So that the total load will act. f) When the longer pointer of the dial gauge reaches steady position, take back the lever to the unloading position “A”. [Avoid sudden release at the lever] g) Now note down the reading in the last dial indicator by notifying the large pointer h) Turn back the hand wheel and remove the job. i) Similarly, repeat the step from ‘a-h’ for different trials and for different metals. (VI) Observation and Calculation: Type of specimen Hard Metals Type of Indentor Diamond cone Soft Metals Ball (1/16”) S/No Specimen 01 02 03 04 05 Hardened steel Mild steel Brass Copper Aluminium Scale C (Black graduations) B (Red graduations) Type of Indentor Diamond cone Ball (1/16’’) Ball (1/16’’) Ball (1/16’’) Ball (1/16’’) (VII) Precautions: The specimen should be cleaned properly. 1 RHN 2 Total load(P) Kg-F 150 100 3 Average RHN Readings must be taken carefully and correctly. (VIII) Result: Rockwell hardness Number of the given specimen is Hardened steel = Mild steel = Brass = Copper = Aluminium = (IX) Conclusion: (X) References: 1. Metals Handbook, 9th ed., Mechanical Testing, Vol. 8, 1990. 2. G. Dieter, Mechanical Metallurgy, S1 ed., Mc Graw Hill, 1986. 3. N. Dowling, Mechanical Behavior of Materials, Prentice Hall, 1993. B) BRINELL HARDNESS TEST (I) Aim: To determine the Brinell hardness number of the given Specimen using Brinell hardness tester. (II) Apparatus: Brinell hardness testing machine and Brinell Microscope. Ball Indentor of diameter 2.5mm and 5mm Specimens (Mild steel, Brass, Copper, Aluminum) (III) Theory: The Brinell Hardness Test is used to determine the Hardness Number of hard, moderately hard, and soft material E.g.: Brass, Bronze, Aluminum, Gold, and Copper. Very hard material and Brittle material cannot be tested by Brinell hardness tester. Brinell hardness number (BHN) is obtained by the ratio of the calculated load and the spherical area of the Indentation or Impression made on the specimen by the corresponding Indentor Ball. In Brinell hardness test, a steel ball of diameter (D) is forced under a load (F) on to a surface of the test specimen. Mean diameter (d) of indentation is measured after the removal of the load (P). The Brinell Hardness Number (BHN) is obtained by dividing the applied force P, in kg-F; by the curved surface area of the indentation, which is actually a segment of a sphere. Since the deformations caused by an indenter are of similar magnitude to those occurring at the ultimate tensile strength in a tension test, some empirical relationships have been established between hardness and engineering ultimate tensile strength of metals and alloys. For example, for steels UTS can be roughly estimated from Brinell hardness as follows: UTS (in MPa) = 3.45 x BHN Suitable Application: Brinell hardness test is used for materials with a coarse or inhomogeneous grain structure. It is used for larger samples. It is also suitable for forgings and castings where the structural elements are large. (IV) Equipment Description: Figure 2: Brinell hardness testing machine. (V) Procedure: a) Keep the loading and unloading lever at position “A” which is unloading position. b) Select suitable indentor & weights according to the scale. c) Place the specimen on testing table anvil. d) Turn the hand wheel to raise a job until it makes contact with indenter & continue turning till the longer pointer at the dial gauge makes 2 ½ rotations. Then it stops at zero continue turning slowly till the small pointer reaches the red spot at 3‟, this is automatic zero setting dial gauge. e) Turn the lever position “A” to “B” i.e. from unloading to the loading position. So that the total load will act. f) When the longer pointer of the dial gauge reaches steady position, take back the lever to the unloading position “A”. [Avoid sudden release at the lever] g) Remove the job from the platform and note down the diameter of the indentation using Brinell microscope. h) Using the appropriate formula calculate BHN. i) Similarly, repeat the step from ‘a-h’ for different trials and for different metals. (VI) Observation and Calculation: Type of Indentor Ball Indentor 2.5mm diameter Ball Indentor 5mm diameter S/ No Specimen 01 02 03 04 Mild steel Brass Copper Aluminium Total load(P) Kg-F 187.5 Total load(P) Kg-F 250 Suitable for Nonferrous soft metals, Soft iron, steel castings, Cast iron, malleable iron. Light alloys casting, forging alloys, die casting alloys. Indentor Diameter(D) in mm Diameter of Indentation(d) in mm 1 2 3 Average Diameter (mm) BHN Brinell hardness number (BHN) = Where, The Brinell hardness number is expressed as (value in N/mm2) D = Diameter of ball indentor in mm d= Diameter of Indentation in mm P= Load applied in Kgf Least Count of Brinell Microscope=0.01mm (VII) Precautions: The specimen should be well cleaned. Place the specimen properly. Reading must be taken carefully and correctly. Remove the load after applying. (VIII) Results: Brinell hardness number of the given specimen is Mild steel = Brass = Copper = Aluminium = (IX) Conclusion: Based on BHN for Mild Steel, the Relation between the tensile strength and Hardness Number is given as follows, Tensile Strength of Mild Steel = … K*BHN for MS Where K= constant (for types of steel from 3.4 to 3.9). (X) References: 1. Metals Handbook, 9th ed., Mechanical Testing, Vol. 8, 1990. 2. G. Dieter, Mechanical Metallurgy, S1 ed., Mc Graw Hill, 1986. 3. N. Dowling, Mechanical Behavior of Materials, Prentice Hall, 1993. C) VICKERS HARDNESS TEST (I) Aim: To determine the hardness of the given Specimen using Vickers hardness test. (II) Apparatus: Vickers Hardness Testing Machine. Diamond cone indentor, Specimen. (III) Theory: Very Hard materials (e.g. Mild steel, case hardened steel, etc,) can be tested by the Vickers’ method. If the moderately hard materials like Brass, Copper and Aluminum are tested in this machine, the indentor makes a deep impression. Hence, a proper indentation cannot be made on the specimen and correct value of the hardness cannot be obtained for these materials by V. H. Test. VHN = Load Sloping or pyramidal area of the indentation This test is similar to the Brinell hardness test similar relationship and eliminates most of the errors. The produced impression is projected onto a focusing screen and the diagonals of the impression are measured by means of the measuring equipment. Due to small impressions, it is very suitable for testing polished and hardened material surfaces. This test is rapid and accurate. The required load as calculated by P/D2 ratio is applied on the specimen for a standard time of 8-10 seconds and BHN is calculated by the ratio of load and the spherical area of indentation. The diameter of the indentation is measured on the focusing screen of the machine. Suitable Application: Vickers hardness test is used for hardness testing of all solid materials, including metallic materials. It is suitable for a wide range of applications. It can also be used for a sub-group of hardness testing of welds. (IV) Equipment Description: Figure 3: Vickers Hardness Testing Machine. (V) Procedure: a) Clean the surface at the specimen b) Fix the indentor in the hardness tester and switch on the power supply. c) Place the specimen with a cleaned surface facing the indentor on the anvil at work table. d) Focus the workpiece surface for clean visibility by rotating the hand wheel at the work table upwards and downwards. e) Select the load specified (P) push button available on the right side at the hardness tester. f) Actuate the electric push button (Green Button) at the front for loading, the loading lever starts moving up words and reaches the study position. g) Now release the loading lever slowly and bring it to the downward position. h) For major reading adjust the display at the indentation made by the indentor to coincide with the micrometre on the display screen. i) For major (minor) reading adjust the movable side at the micrometre and note down the total reading. j) The measurement is to be made for two opposite corners of the diagonal indentation denoted as (l). k) Repeat the above procedure for different material. (VI) Observation and Calculation: Type of indentor = Diamond cone S/No Specimen Load applied in Kg-F Length of Indentation in mm(l) 1 2 3 Average length in mm Vickers Hardness Number (VHN) = Where, P= Load applied in Kg l= Average length of the diagonal L in mm Least count of microscope=0.001mm 1st scale each division =0.1mm 2nd scale each division =0.01 3rd scale each division =0.001mm (VII) Precautions: The specimen should be well cleaned. Place the specimen properly. Reading must be taken carefully and correctly. (VIII) Results: Vickers hardness Number of the given specimen is Mild steel = Hardened mild steel = (IX) Conclusion: (X) References: 1. Metals Handbook, 9th ed., Mechanical Testing, Vol. 8, 1990. 2. G. Dieter, Mechanical Metallurgy, S1 ed., Mc Graw Hill, 1986. 3. N. Dowling, Mechanical Behavior of Materials, Prentice Hall, 1993. Compiler: Ifeyinwa Ijeoma Obianyo PhD Candidate, Department of Materials Science and Engineering, African University of Science and Technology, Abuja. Date: 03/03/2019 View publication stats