Gaertner Ellipsometer Operation Procedure 1. Initial Settings 1.1. Turn the system key counter-clockwise to horizontal position and the yellow LED will lit. (laser will take about 5 minutes to warmup for more stable result) 1.2. 1.3. 1.4. 1.5. Turn on the computer, the red alignment laser will be on. Login to the computer with AD password GEMP (Gaertner EllipsoMeter Program) will automatically launch. After GEMP finish loading, click the ellipsometer icon in the top menu. 1.6. After Measurement and Calculation Window launch, press F9 or click on “Adjust Sample Table” button to launch the alignment window. Prepared by Edmond Chow 217-244-9556 Checked by Paul DiPippo 1 Version 3.0 Version 3.1 March 27, 2020 April 1, 2020 Gaertner Ellipsometer Operation Procedure 2. Sample Loading 2.1. Place your sample on the sample table and center the target area near the red alignment laser spot. 2.2. Adjust the knob at the sample table to center the cross. (front knob for Y-plane and right knob for X-plane adjustment). 2.3. After centering the cross, adjust the vertical adjustment wheel at the back to peak up the signal bar, until it turn green. Click OK to after alignment. 2.4. If you don’t see any signal, check if the laser key is on, and if your sample is flat, contact staff if you need help, do NOT turn the knob more than 2 full turns. 3. Film Model Selection and Measurement (single layer film on Si or GaAs) 3.1. Load model file from the software base on the material of you film, if the material is not available, contact Edmond to create the material for you. 3.2. Enter the approximate thickness of film in A. 3.3. Click “Print Measured Data” and then click “Measure & Calculate” Prepared by Edmond Chow 217-244-9556 Checked by Paul DiPippo 1 Version 3.0 Version 3.1 March 27, 2020 April 1, 2020 Gaertner Ellipsometer Operation Procedure 3.4. The result will show the thickness of the film measured from three wavelength: 405nm, 632.nm and 830nm. The thickness measured from three wavelength should be within 20A, otherwise, the initial approximate thickness you enter is likely to be incorrect. 3.5. If you need to move the same sample to different location or measure different samples, you will need to repeat alignment procedure 2.2-2.4 with some fine adjustment. 4. Sample Unloading and shutdown 4.1. Remove your sample. 4.2. Close the program 4.3. Shutdown computer (NOT logout) 4.4. Turn the key clockwise to vertical direction. 5. Application note: 5.1. Our ellipsometer can only measure single layer film on semiconductor, if you have multiple layer film on some other material substrate, please put a dummy Si sample during you film deposition, so that you can use that for the ellipsometer measurement. 5.2. The best refractive index measurement thickness on Si substrate for 633nm SiO2, PMMA, ~140nm, Si3N4, HfO2 TiO2 ~90nm Prepared by Edmond Chow 217-244-9556 Checked by Paul DiPippo 1 Version 3.0 Version 3.1 March 27, 2020 April 1, 2020