Uploaded by Jenny D

Activity - chromatography

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ACTIVITY
Colors that run
In this activity you will separate a mixture into its component parts
Materials
rectangular pieces of filter paper
250 mL beaker
water soluble black felt pen
1.0 mL of vinegar
water
Procedure
1. Use a felt tip pen to make a large dot about 3cm from one end of the
piece of filter paper. Let the spot dry completely. Add more ink to the
spot and let it dry again. Repeat this process a few more times.
2. Pour the vinegar into the beaker and add ware until the solutin is
about 2 cm deep.
3. Place the filer paper into the beaker so the end with the ink dot is
closest to the water. Make sure the dot is not in the water.
4. Observe the ink spot as the water is soaked up by the filter paper.
Questions
1. What colors appeared on the filter paper? Where do you think these
colors came from?
2. Suppose someone told you that the black ink was a mixture. Use
your observations to come up with a definition for the term mixture.
Questions
1. What type of mixture are you separating?
ACTIVITY
Colors that run
2. What role does the burner have in the distillation process? Could the
solution be distilled without the burner?
3. You notice that your sample begins to boil at 96.2C and liquid begins to
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drip into the collection flask. What is happening?
Why is it a good idea to remove the collection flask and replace it with another as
soon as the temperature of the solution begins to rise again?
The temperature rises steadily and the solution begins to boil again at 102.3C.
What is happening now?
The temperature continues to rise until it reaches 108C and the rest of the solution
boils. How many different liquids were contained in your sample? Explain.
As you complete the distillation, you notice a white, crystalline film lining the inside of
the flask that contained the original sample. What could this substance be? Why
didn’t you notice it in the original solution?
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