Attention:Alfred Culbreth
American Premium Water Corp.
*** COD ACCOUNT ***
1615 South Congress Ave
Suite 103
Delray Beach , FL
USA
33445
Report Date: 2014/10/17
Report #: R3191444
Version: 1 - Final
CERTIFICATE OF ANALYSIS
MAXXAM JOB #: B4I1770
Received: 2014/10/02, 12:10
Sample Matrix: Water
# Samples Received: 2
Analyses
Alkalinity
Carbonate, Bicarbonate and Hydroxide
Chloride by Automated Colourimetry
Conductivity
Dissolved Organic Carbon (DOC) (1)
Fluoride
Hardness (calculated as CaCO3)
Metals Analysis by ICPMS (as received) (2)
Total Metals Analysis in Food by ICP
Ion Balance (% Difference)
Anion and Cation Sum
Total Ammonia-N
Nitrate (NO3) and Nitrite (NO2) in Water (3)
pH
Orthophosphate
Ash
Sat. pH and Langelier Index (@ 20C)
Sat. pH and Langelier Index (@ 4C)
Beta-Carotene
Calories
Carbohydrates
Cholesterol
Density
Fatty Acid Profile by GC/FID (4)
KJ
Moisture
Sulphate by Automated Colourimetry
Protein
Quantity
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Date
Extracted
N/A
N/A
N/A
N/A
N/A
2014/10/02
N/A
Date
Analyzed
2014/10/03
2014/10/03
2014/10/07
2014/10/03
2014/10/03
2014/10/03
2014/10/16
Laboratory Method
CAM SOP-00448
CAM SOP-00102
CAM SOP-00463
CAM SOP-00414
CAM SOP-00446
CAM SOP-00449
CAM SOP
00102/00408/00447
2014/10/16 2014/10/16 CAM SOP-00447
2014/10/06 2014/10/07 CAM SOP-00408
N/A
2014/10/16
N/A
2014/10/16
N/A
2014/10/07 CAM SOP-00441
N/A
2014/10/03 CAM SOP-00440
N/A
2014/10/03 CAM SOP-00413
N/A
2014/10/06 CAM SOP-00461
N/A
2014/10/03 CAM SOP-00713
N/A
2014/10/16
N/A
2014/10/16
2014/10/06 2014/10/07 CAM SOP-00709
N/A
2014/10/09 CAM WI-00708
N/A
2014/10/09 CAM WI-00708
2014/10/08 2014/10/08 CAM SOP-00700
N/A
2014/10/07 CAM SOP-00747
2014/10/07 2014/10/07 CAM SOP-00702
N/A
2014/10/09 CAM WI-00708
N/A
2014/10/03 CAM SOP-00715
N/A
2014/10/07 CAM SOP-00464
N/A
2014/10/07 CAM SOP-00711
Reference
SM 22 2320 B m
APHA 4500-CO2 D
EPA 325.2 m
SM 22 2510 m
SM 22 5310 B m
SM 22 4500-F C m
SM 2340 B
EPA 6020 m
AOAC 984.27 (mod.)
EPA GS I-2522-90 m
SM 22 4500-NO3I/NO2B
SM 4500H+ B
EPA 365.1 m
AOAC 923.03
AOAC 992.04 mod.
Calculation
Calculation
AOAC 976.26/994.10
AOAC 985.19
AOAC 996.06
Calculation
AOAC methodology
EPA 375.4 m
AOAC 992.15
Page 1 of 8
Maxxam Analytics International Corporation o/a Maxxam Analytics 6740 Campobello Road, Mississauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca
Attention:Alfred Culbreth
American Premium Water Corp.
*** COD ACCOUNT ***
1615 South Congress Ave
Suite 103
Delray Beach , FL
USA
33445
Report Date: 2014/10/17
Report #: R3191444
Version: 1 - Final
CERTIFICATE OF ANALYSIS
MAXXAM JOB #: B4I1770
Received: 2014/10/02, 12:10
Sample Matrix: Water
# Samples Received: 2
Analyses
Retinol
Sugar Profile (5)
Total Dietary Fibre
Vitamin A IU/100g
Vitamin A RE/100g
Total Dissolved Solids
Total Sugars (6)
Vitamin C (Ascorbic Acid)
Quantity
1
1
1
1
1
1
1
1
Date
Extracted
2014/10/06
2014/10/06
N/A
2014/09/30
N/A
N/A
2014/09/30
2014/10/06
Date
Analyzed
2014/10/07
2014/10/07
2014/10/08
2014/10/09
2014/10/09
2014/10/03
2014/10/07
2014/10/06
Laboratory Method
CAM SOP-00709
CAM SOP-00708
CAM SOP-00707
CAM SOP-00709
CAM SOP-00709
CAM SOP-00428
CAM SOP-00708
CAM SOP-00724
Reference
AOAC 992.04 992.06
AOAC 980.13
AOAC 991.43, 985.29
AOAC 992.04, 992.06
AOAC 992.04, 992.06
SM 22 2540C m
AOAC 980.13
CFIA-LCAQ-001-09
* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.
(1) Dissolved Organic Carbon (DOC) present in the sample should be considered as non-purgeable DOC.
(2) Metals analysis was performed on the sample 'as received'.
(3) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures.
(4) "Note: Total fatty acids and individual fatty acids are expressed as the triglycerides. Summed fatty acid groups are expressed as the fatty acids"
(5) Glucose result reported represents a total of both the D- and L- isomers.
(6) The result reported for Total Sugars is a calculated value based on the sum of glucose, fructose, lactose, sucrose and maltose only.
Michael Black
Encryption Key
17 Oct 2014 12:35:32 -04:00
Please direct all questions regarding this Certificate of Analysis to your Project Manager.
Michael Black, CS Rep-Food Science and Safety Division
Email: MBlack@maxxam.ca
Phone# (905)817-5834
====================================================================
Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section 5.10.2 of ISO/IEC 17025:2005(E),
signing the reports. For Service Group specific validation please refer to the Validation Signature Page.
Total Cover Pages : 2
Page 2 of 8
Maxxam Analytics International Corporation o/a Maxxam Analytics 6740 Campobello Road, Mississauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca
Maxxam Job #: B4I1770
Report Date: 2014/10/17
American Premium Water Corp.
RESULTS OF ANALYSES OF WATER
Maxxam ID
XU6089
XU8017
Units
L'alpina Ilitre
-Natural
Spring WaterSTILL
L'alpina Ilitre
-Natural
Spring WaterSTILL
RDL
Anion Sum
me/L
N/A
2.83
N/A
Bicarb. Alkalinity (calc. as CaCO3)
mg/L
N/A
130
1.0
Carb. Alkalinity (calc. as CaCO3)
mg/L
N/A
ND
1.0
Cation Sum
me/L
N/A
2.83
N/A
Hardness (CaCO3)
mg/L
N/A
140
1.0
%
N/A
NC
N/A
Langelier Index (@ 20C)
N/A
N/A
-0.0550
N/A
Langelier Index (@ 4C)
N/A
N/A
-0.305
N/A
Saturation pH (@ 20C)
N/A
N/A
7.58
N/A
Saturation pH (@ 4C)
N/A
N/A
7.83
N/A
Ammonia-N
mg/L
N/A
ND
0.050
Conductivity
umho/cm
N/A
270
1.0
Dissolved Solids
mg/L
N/A
120
10
Fluoride (F-)
mg/L
N/A
0.13
0.10
Organic Carbon
mg/L
N/A
0.43
0.20
Orthophosphate (P)
mg/L
N/A
0.044
0.010
pH
N/A
7.53
N/A
Sulphate (SO4)
mg/L
N/A
4
1
Alkalinity (Total as CaCO3)
mg/L
N/A
130
1.0
Chloride (Cl)
mg/L
N/A
2
1
Nitrite (N)
mg/L
N/A
ND
0.010
Nitrate (N)
mg/L
N/A
ND
0.10
p-Alkalinity
mg/L
N/A
ND
1.0
Nitrate + Nitrite
mg/L
N/A
ND
0.10
Density
g/mL
0.99580
N/A
N/A
KJ
/100g
ND
N/A
1
Ash
g/100g
ND
N/A
0.1
Calories
/100g
ND
N/A
1
Protein
g/100g
ND
N/A
0.10
Fat (GC/FID)
g/100g
0.003
N/A
0.001
Saturated Fatty Acids
g/100g
0.002
N/A
0.001
cis-Monounsaturated Fatty Acids
g/100g
<0.001
N/A
0.001
Sampling Date
Calculated Parameters
Ion Balance (% Difference)
Inorganics
pH
Nutritional Parameters
RDL = Reportable Detection Limit
N/A = Not Applicable
ND = Not detected
Page 3 of 8
Maxxam Analytics International Corporation o/a Maxxam Analytics 6740 Campobello Road, Mississauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca
Maxxam Job #: B4I1770
Report Date: 2014/10/17
American Premium Water Corp.
RESULTS OF ANALYSES OF WATER
Maxxam ID
XU6089
XU8017
Units
L'alpina Ilitre
-Natural
Spring WaterSTILL
L'alpina Ilitre
-Natural
Spring WaterSTILL
RDL
cis-Polyunsaturated Fatty Acids
g/100g
<0.001
N/A
0.001
Trans-Fatty Acids
g/100g
<0.001
N/A
0.001
Carbohydrates
g/100g
ND
N/A
0.1
Omega-3 Polyunsaturated Fatty Acids
g/100g
<0.001
N/A
0.001
Omega-6 Polyunsaturated Fatty Acids
g/100g
<0.001
N/A
0.001
Total Dietary Fibre
g/100g
ND
N/A
0.1
Total Sugars
g/100g
ND
N/A
0.4
Fructose
g/100g
ND
N/A
0.1
Glucose
g/100g
ND
N/A
0.2
Sucrose
g/100g
ND
N/A
0.3
Maltose
g/100g
ND
N/A
0.4
Lactose
g/100g
ND
N/A
0.4
Sampling Date
Cholesterol
mg/100g
ND
N/A
1
Moisture
g/100g
100.0
N/A
0.1
Vitamin A
IU/100g
ND
N/A
50
Vitamin A
RE/100g
ND
N/A
10
Retinol
ug/100g
ND
N/A
10
Beta Carotene
ug/100g
ND
N/A
10
Vitamin C
mg/100g
ND
N/A
0.5
RDL = Reportable Detection Limit
N/A = Not Applicable
ND = Not detected
Page 4 of 8
Maxxam Analytics International Corporation o/a Maxxam Analytics 6740 Campobello Road, Mississauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca
Maxxam Job #: B4I1770
Report Date: 2014/10/17
American Premium Water Corp.
ELEMENTS BY ATOMIC SPECTROSCOPY (WATER)
Maxxam ID
XU6089
XU8017
Units
L'alpina Ilitre
-Natural
Spring WaterSTILL
L'alpina Ilitre
-Natural
Spring WaterSTILL
Aluminum (Al)
ug/L
N/A
5.8
5.0
Antimony (Sb)
ug/L
N/A
ND
0.50
Arsenic (As)
ug/L
N/A
ND
1.0
Barium (Ba)
ug/L
N/A
16
2.0
Beryllium (Be)
ug/L
N/A
ND
0.50
Bismuth (Bi)
ug/L
N/A
ND
1.0
Boron (B)
ug/L
N/A
ND
10
Cadmium (Cd)
ug/L
N/A
ND
0.10
Calcium (Ca)
ug/L
N/A
44000
200
Chromium (Cr)
ug/L
N/A
ND
5.0
Cobalt (Co)
ug/L
N/A
ND
0.50
Copper (Cu)
ug/L
N/A
ND
1.0
Iron (Fe)
ug/L
N/A
ND
100
Lead (Pb)
ug/L
N/A
ND
0.50
Lithium (Li)
ug/L
N/A
ND
5.0
Magnesium (Mg)
ug/L
N/A
6300
50
Manganese (Mn)
ug/L
N/A
ND
2.0
Molybdenum (Mo)
ug/L
N/A
ND
0.50
Nickel (Ni)
ug/L
N/A
ND
1.0
Phosphorus (P)
ug/L
N/A
ND
100
Potassium (K)
ug/L
N/A
760
200
Selenium (Se)
ug/L
N/A
ND
2.0
Silicon (Si)
ug/L
N/A
6000
50
Silver (Ag)
ug/L
N/A
ND
0.10
Sodium (Na)
ug/L
N/A
2300
100
Strontium (Sr)
ug/L
N/A
78
1.0
Tellurium (Te)
ug/L
N/A
ND
1.0
Thallium (Tl)
ug/L
N/A
ND
0.050
Tin (Sn)
ug/L
N/A
ND
1.0
Titanium (Ti)
ug/L
N/A
ND
5.0
Tungsten (W)
ug/L
N/A
ND
1.0
Uranium (U)
ug/L
N/A
0.38
0.10
Vanadium (V)
ug/L
N/A
ND
0.50
Zinc (Zn)
ug/L
N/A
ND
5.0
Sampling Date
RDL
Metals
RDL = Reportable Detection Limit
N/A = Not Applicable
ND = Not detected
Page 5 of 8
Maxxam Analytics International Corporation o/a Maxxam Analytics 6740 Campobello Road, Mississauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca
Maxxam Job #: B4I1770
Report Date: 2014/10/17
American Premium Water Corp.
ELEMENTS BY ATOMIC SPECTROSCOPY (WATER)
Maxxam ID
XU6089
XU8017
Units
L'alpina Ilitre
-Natural
Spring WaterSTILL
L'alpina Ilitre
-Natural
Spring WaterSTILL
RDL
Zirconium (Zr)
ug/L
N/A
ND
1.0
Calcium (Ca)
ug/g
66
N/A
20
Iron (Fe)
ug/g
ND
N/A
2
Potassium (K)
ug/g
ND
N/A
100
Sodium (Na)
ug/g
ND
N/A
50
Sampling Date
RDL = Reportable Detection Limit
N/A = Not Applicable
ND = Not detected
Page 6 of 8
Maxxam Analytics International Corporation o/a Maxxam Analytics 6740 Campobello Road, Mississauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca
Maxxam Job #: B4I1770
Report Date: 2014/10/17
American Premium Water Corp.
GENERAL COMMENTS
RESULTS OF ANALYSES OF WATER
Fatty Acid Profile by GC/FID: Fatty acids were detected in the method blank at a level marginally above the detection limit. Sample results have not
been blank corrected. Those results at or near the detection limit may be biased high.
Results relate only to the items tested.
Page 7 of 8
Maxxam Analytics International Corporation o/a Maxxam Analytics 6740 Campobello Road, Mississauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca
Maxxam Job #: B4I1770
Report Date: 2014/10/17
American Premium Water Corp.
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s).
Cristina Carriere, Scientific Services
Helen Weidinger, Scientific Specialist
Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section 5.10.2 of ISO/IEC
17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.
Page 8 of 8
Maxxam Analytics International Corporation o/a Maxxam Analytics 6740 Campobello Road, Mississauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca