Breaking Strength and Elongation Properties of Polyester Woven Fabrics on the Basis of Filament Fineness Hatice Kübra Kaynak, PhD1, Osman Babaarslan, PhD2 1 Gaziantep University, Textile Engineering Department, Gaziantep TURKEY 2 Çukurova University, Textile Engineering Department, Adana TURKEY Correspondence to: Hatice Kubra Kaynak email: tuluce@gantep.edu.tr ABSTRACT Woven fabrics produced from microfilament yarns are superior to conventional filament fabrics in rain clothes, tents, parachutes, sails, wind-proof clothes, sleeping bags, filters, and surgical gowns due to their distinguishing properties such as good filtration, barrier effect against weather conditions, and light weight. Breaking strength and elongation are important and decisive parameters for these end uses since low strength properties shorten the useful life time as well disable the functionality of these products. In this study, breaking strength and elongation properties of microfilament woven fabrics are investigated in comparison to conventional filament fabrics. Three different weave types are used as 1/1 Plain, 3/2 Twill, and 4/1 Satin. Four different weft setts and five different filament finenesses are applied for every weave type. In doing so, 60 woven fabric samples are produced. Important influences of weft sett and filament fineness are observed on weft direction breaking strength. Analysis of variance (ANOVA) results are used to interpret the experimental data. by different constructional parameters [20]. The desired strength property of a woven fabric for a particular end use can be obtained by applying the appropriate fabric construction such as weave type and yarn sett. In addition, by changing these parameters, a strength property can be optimized and negative parameters can be offset. Many researchers studied the strength properties of polyester filament woven fabrics [12, 19, 21-26]. Apart from the previous studies, in this study the breaking strength and elongation properties of polyester filament woven fabrics are investigated on the basis of filament fineness and weft sett. For this aim, the effects of filament fineness on breaking strength and elongation are investigated for different weave types and different weft sett values. ANOVA are conducted to determine the statistical importance of weft sett and filament fineness on breaking strength and elongation properties for three different weave types. MATERIALS AND METHOD This study is focused on the effects of filament fineness and weft sett on breaking strength and elongation of 100% polyester filament woven fabrics. Polyester microfilament textured yarns of 110 dtex with 0.33, 0.57, and 0.76 dtex filament fineness and conventional polyester textured yarns of 110 dtex with 1.14 and 3.05 dtex filament fineness are chosen. These yarns are used only in the weft direction. For warp yarns, 83 dtex polyester yarn with 1.14 dtex filament fineness is used. Yarn tenacity and elongation of weft yarns are determined according to ISO 2062: 2009 [27] and given in Table I. INTRODUCTION Filament woven fabrics are used in many textiles such as; casual wear, rain clothes, tents, parachutes, sails, wind-proof clothes, sleeping bags, filters, and surgical gowns. Fabrics produced from microfilaments are superior to conventional filament fabrics due to properties such as good filtration, an effective barrier against weather conditions, and light weight. A microfilament can be defined as a filament finer than 1 dtex or 1 denier [1-8]. In the literature, there are some experimental studies which deal with the performance properties of microfilament woven fabrics [9-19]. Strength properties are decisive parameters for filament fabric end uses because low strength properties shorten the useful life time as well disables the functionality of these products. It must be considered that strength properties of woven fabrics is a complex phenomenon and can be affected Journal of Engineered Fibers and Fabrics Volume 10, Issue 4 – 2015 TABLE I. Strength and elongation properties of weft yarns. Weft yarn filament fineness, dtex 0.33 0.57 0.76 1.14 3.05 Yarn tenacity, cN/Tex Yarn breaking elongation, % 55 4.2 4.0 3.7 3.8 3.8 23 25 19 22 18 http://www.jeffjournal.org Three different weave types of 1/1 Plain, 3/2 Twill, and 4/1 Satin are chosen for this study. For each weave type, four different weft sett values are applied considering the weaveability limitations. The highest and the lowest weft sett values for the weave types are determined by production trials. Warp sett is 77 warps/cm for plain weave samples and 85 warps/cm for twill and satin weave samples. In doing so, 60 woven fabric samples are produced. To obtain dimensional stability, a thermal fixation process is applied to samples at 195ºC with 25m/min process speed before the desizing process. Structural properties of sample fabrics after thermal fixation and desizing processes are determined according to ISO 7211-2: 1984, ISO 7211-3: 1984, ISO 3801: 1977, and ISO 5084: 1996 [28-31] and the results are given in Table II. TABLE II. Structural features of fabrics. Weft yarn Weft sett, filament wefts/cm fineness, P T S dtex 30 41 43 0.33 30 41 43 0.57 30 41 43 0.76 30 41 43 1.14 30 41 43 3.05 32 43 45 0.33 32 43 45 0.57 32 43 45 0.76 32 43 45 1.14 32 43 45 3.05 34 45 47 0.33 34 45 47 0.57 34 45 47 0.76 34 45 47 1.14 34 45 47 3.05 36 47 49 0.33 36 47 49 0.57 36 47 49 0.76 36 47 49 1.14 36 47 49 3.05 P:Plain, T:Twill, S:Satin Fabric weight, g/m² Fabric thickness, mm P T S P T S P T S P T S 114 113 111 112 117 117 116 115 116 118 121 120 118 120 119 123 121 120 122 121 130 129 126 128 125 133 132 130 130 128 137 135 132 133 131 141 138 136 136 134 130 130 128 129 129 133 133 132 131 132 136 136 134 132 133 138 140 138 139 136 0.24 0.24 0.23 0.23 0.25 0.22 0.22 0.22 0.23 0.24 0.22 0.22 0.21 0.22 0.24 0.21 0.22 0.21 0.22 0.23 0.22 0.22 0.22 0.22 0.22 0.22 0.22 0.22 0.22 0.22 0.23 0.22 0.22 0.22 0.22 0.23 0.23 0.22 0.22 0.23 0.22 0.22 0.22 0.22 0.23 0.23 0.22 0.22 0.22 0.23 0.23 0.22 0.23 0.23 0.23 0.23 0.23 0.23 0.22 0.23 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 14 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 In this study, the breaking strength and elongation properties of polyester filament woven fabrics are determined. All fabric samples are conditioned according to ISO 139 before testing and tests are performed under standard conditions of 20±2ºC and 65±4% humidity [32]. Breaking strength and elongation properties are determined according to ISO 13934-1 [33]. Design-Expert (8.0.7.1) statistical software is used to interpret the experimental data. A full factorial design with two replicates at each design point is constructed for these statistical analyses. A full factorial design is chosen in order to investigate the effect of a factor at different levels of the other factor. This provides higher confidence for the results. At the same time, a full factorial design enables determination of interactions between filament fineness and weft sett for this study. ANOVA is performed to determine the significant interactions between filament fineness, weft sett, and breaking strength and elongation for all weave types. Weft crimp, % Warp crimp, % RESULTS AND DISCUSSION Breaking Strength Filament fineness and weft sett are differentiated for only the weft direction. The breaking strength results are analyzed only for the weft direction. Weft direction breaking strength results are given in Figures 1, 2, and 3 for plain, twill, and satin weave types, respectively. Warp direction breaking strength results are given in Table III. FIGURE 1. Weft direction breaking strength of plain samples. Journal of Engineered Fibers and Fabrics Volume 10, Issue 4 – 2015 56 http://www.jeffjournal.org A consistent trend of having higher fabric breaking strength values for finer filaments is obvious from Figure 1 for all weft sett values. It is a known fact that yarn strength is the foremost parameter on fabric breaking strength. If the yarn strength values are observed from Table I, it is seen that 0.33 dtex and 0.57 dtex filament yarns have higher yarn strength values than that of other yarns. Therefore, the higher fabric breaking strength values are estimated for these yarns. On the other hand, 0.76 dtex, 1.14 dtex, and 3.05 dtex yarns have the same yarn strength value whereas higher fabric breaking strength values are obtained with finer filaments. 0.76 dtex samples exhibit nearly 10% higher fabric breaking strength than 3.05 dtex samples. As the filament fineness decreases, the number of filaments in the yarn cross section increases. Thus, the total specific surface area of filaments in the yarn cross section increases as the filaments get finer. In other words, the 0.76 dtex sample has a higher total specific surface area than that of the 1.14 dtex sample and the 1.14 dtex sample has higher specific surface area than that of the 3.05 dtex samples. This situation causes a higher cohesion force for finer filaments in the fabric structure during tensioning. Consequently, this provides a probable reason for higher breaking strength values of finer filaments for different weft sett values. Besides, an increase is observed by increased weft sett values for all filament fineness types. This is a probable result of a higher number of yarns and interlacings in a unit cell. The phenomenon was observed in a former study done on polyester filament woven fabrics [22]. Nevertheless, for 0.76 dtex, 1.14 dtex, and 3.05 dtex samples which have the same yarn strength value, the higher fabric breaking strength values are seen for finer filaments. There is nearly a 6% fabric breaking strength difference between the 0.76 dtex and 3.05 dtex samples. Similarly as with plain samples, due to increased total specific surface area of filaments in the yarn cross section, a higher cohesion force for finer filaments occurs in the fabric structure during tensioning. Consequently, this provides a probable reason for higher fabric breaking strength caused by finer filaments in the yarn cross-section. On the other hand, a regular increase is seen in weft direction breaking strength with higher weft sett values due to a higher number of yarns and interlacings in the unit cell as observed in a similar manner with plain samples. FIGURE 3. Weft direction breaking strength of satin samples. It is seen from Figure 3 that, the higher breaking strength values are observed for samples with finer filaments for all weft sett values. As seen for plain and twill samples, the higher fabric breaking strength values are observed for 0.33 dtex and 0.57 dtex samples due to higher yarn strength. On the other hand, for 0.76 dtex, 1.14 dtex, and 3.05 dtex filament fineness values, the higher fabric breaking strength values are observed for finer filaments which have similar yarn breaking strength. 0.76 dtex samples exhibit nearly 5% higher fabric breaking strength than 3.05 dtex samples. This is believed to be caused by a higher total specific surface area and a higher cohesion force for finer filaments in the fabric structure during tensioning. Also, a considerable increase of fabric breaking strength is determined with higher weft sett due to a higher number of yarns and interlacings in the unit cell. FIGURE 2. Weft direction breaking strength of twill samples. Figure 2 exhibits the breaking strength of twill weave samples. Higher breaking strength values are seen for finer filaments. Similarly as with plain weave samples, a part of this increase is a result of a higher yarn strength value of the 0.33 and 0.57 dtex filament yarns. Journal of Engineered Fibers and Fabrics Volume 10, Issue 4 – 2015 57 http://www.jeffjournal.org TABLE III. Warp direction breaking strength (N). Plain Weft sett (wefts/cm) 3/2 Twill 0,33 0,57 0,76 1,14 3,05 1171,8 1201,3 1231,1 1223,5 1165,9 32 1211,9 1219,5 1217,1 1214,0 1192,0 34 1220,7 1191,4 1203,2 1178,9 1171,8 36 1150,0 1199,1 1177,4 1186,3 1193,1 Filament fineness, dtex 0,76 1,14 3,05 41 1372,6 1363,2 1380,6 1357,6 1374,2 43 1362,5 1372,4 1370,4 1377,5 1368,4 45 1359,8 1363,1 1368,2 1360,2 1361,0 47 1321,5 1375,8 1341,6 1376,7 1365,6 Weft sett (wefts/cm) 4/1 Satin Filament fineness, dtex 30 Weft sett (wefts/cm) Breaking Elongation Weft direction breaking elongation of plain, twill, and satin weave samples are seen in Figures 4, 5, and 6, respectively. Similarly as with breaking strength results, breaking elongation values are illustrated only for weft direction. Warp direction breaking elongation values are also given in Table V. 0,33 0,57 Filament fineness, dtex 0,76 1,14 3,05 43 1357,4 0,33 1358,4 0,57 1376,2 1353,1 1325,9 45 1369,6 1355,0 1351,7 1359,6 1360,7 47 1366,0 1349,0 1369,5 1368,7 1374,5 49 1330,4 1377,5 1372,9 1333,0 1352,6 FIGURE 4. Weft direction breaking elongation of plain samples. Figure 4 shows the weft direction breaking elongation of plain weave samples. There is no regular effect of filament fineness on fabric breaking elongation. In addition, 0.33 dtex and 0.57 dtex filament yarns have higher yarn breaking elongation values whereas an increase in fabric breaking elongation has not been determined for these samples. Besides, the warp direction breaking elongation values are considerably higher than those of the weft direction. This is a probable result of extremely high crimp values of warp direction in plain weave samples. In general, as the amount of original crimp increases, the extent of the crimp interchange region increases, thus increasing fabric elongation to failure [34]. On the other hand, a minor decrease of breaking elongation is observed for increasing weft sett values. Warp direction breaking strength results are seen in Table III. A consistent trend is not observed for warp direction breaking strength due to the fact that filament fineness and weft sett are differentiated for only weft direction. ANOVA results for breaking strength of samples are given in Table IV. According to ANOVA results, factors which have a P value below 0.05 are statistically significant on breaking strength with 95% confidence. Otherwise, P values above 0.05 indicates an insignificant factor. TABLE IV. P Values of ANOVA for breaking strength. Weave Type Plain Twill Satin Factors Filament fineness Weft sett Filament fineness Weft sett Filament fineness Weft sett Weft direction < 0.0001 < 0.0001 < 0.0001 < 0.0001 < 0.0001 < 0.0001 Warp direction 0.1582 0.0255 0.2471 0.1721 0.1899 0.4532 It is seen from Table IV that, in the weft direction, the filament fineness and weft sett have a statistically significant effect on breaking strength contrary to the warp direction. FIGURE 5. Weft direction breaking elongation of twill samples. Journal of Engineered Fibers and Fabrics Volume 10, Issue 4 – 2015 58 http://www.jeffjournal.org TABLE VI. P Values of ANOVA results for breaking elongation. Breaking elongation of twill weave samples are seen in Figure 5. A regular tendency of neither increase nor decrease is observed due to filament fineness for twill weave samples. On the other hand 0.33 dtex and 0.57 dtex samples which have higher yarn breaking elongation values, do not exhibit higher fabric breaking elongation values. In other words, the effect of yarn breaking elongation on fabric breaking elongation is not observed for twill weave samples. Besides, the weft sett has no effect on breaking elongation, contrary to plain samples. Weave Type Plain Twill Satin Plain 3/2 Twill Weft sett (wefts/cm) 41 43 45 47 0.33 33.5 33.1 34.0 36.9 4/1 Satin TABLE V. Warp direction breaking elongation (%). Weft sett (wefts/cm) 43 45 47 49 0.33 28.9 29.8 31.4 30.3 Filament fineness, dtex 0.57 0.76 1.14 36.6 36.6 37.0 37.6 37.2 37.0 37.4 38.3 37.7 39.9 37.9 39.0 Filament fineness, dtex 0.57 0.76 1.14 31.2 30.0 29.6 32.0 29.7 30.2 30.1 29.2 29.4 32.7 29.7 30.7 Filament fineness, dtex 0.57 0.76 1.14 28.7 30.4 28.3 28.3 28.4 29.1 29.3 30.5 28.7 30.0 30.6 28.5 Warp Direction 0.0376 0.5430 0.0035 0.3346 0.4039 0.1592 CONCLUSION For all weave types, filament fineness and weft sett have a considerable effect on weft direction breaking strength. Higher fabric breaking strength results are observed for higher weft sett and finer filaments in fabric structure. With respect to filament fineness, a part of this effect originates from higher yarn strength values of 0.33 dtex and 0.57 dtex filament yarns. Nevertheless, the effect of filament fineness on weft direction breaking strength is observed for other levels of filament fineness (0.76 dtex, 1.14 dtex and 3.05 dtex) which have the same yarn strength values. 0.76 dtex samples have 5-10% higher fabric breaking strength values than those of 3.05 dtex samples for all samples. This is a probable result of a higher cohesion force between filaments due to higher total specific surface area of finer filaments in the yarn cross section. It is an important result to manage this increase in fabric breaking strength with only changes in filament fineness, keeping other parameters constant [35]. With respect to statistical analysis, weft sett and filament fineness have a significant effect on weft direction breaking strength for all weave types. Besides, the contribution of weft sett on breaking strength is higher than that of filament fineness according to statistical analyses. Breaking elongation of satin weave samples are seen in Figure 6. There is no obvious effect of weft sett and filament fineness on fabric breaking elongation. In addition, the effect of yarn breaking elongation on fabric breaking elongation is not observed, similar to plain and twill samples. 0.33 40.0 38.4 39.5 38.8 Filament fineness Weft sett Filament fineness Weft sett Filament fineness Weft sett Weft Direction 0.0688 0.0468 0.0012 0.6803 0.0006 0.6528 It is seen from Table VI that the effects of weft sett and filament fineness on fabric breaking elongation is generally found to be statistically insignificant. FIGURE 6. Weft direction breaking elongation of satin samples. Weft sett (wefts/cm) 30 32 34 36 Factors 3.05 40.5 40.4 38.5 39.4 The filament fineness and weft sett have no considerable effect on fabric breaking elongation. Also, yarn breaking elongation does not have a significant effect on fabric breaking elongation. There is a considerable difference between weft and warp direction breaking elongation values of plain weave types due to extremely higher crimp values of warp direction than weft direction in plain weave samples. 3.05 31.8 31.6 32.6 31.9 3.05 30.2 30.3 30.7 30.3 ANOVA results for breaking elongation are given in Table VI. Journal of Engineered Fibers and Fabrics Volume 10, Issue 4 – 2015 59 http://www.jeffjournal.org REFERENCES [1] Leadbetter, P.; Dervan, S.; “The microfiber step change”, Journal of the Society of Dyers and Colourists, Vol.108, 1992, p.369–371. [2] Bianchi, R.; Maglione, R.; “Manufacturing of fine denier filaments”, Polyester: 50 Years of Achievement, Tomorrow's Ideas and Profits. England: Dewsbury, 1993. [3] Purane, S.V.; Panigrahi, N.R.; “Microfibers, microfilaments and their applications”, AUTEX Research Journal, Vol.7, 2007, p.148-158. [4] Basu, A.; “Microfibers: Properties, processing and use”, Asian Textile Journal, Vol.10, 2001, p.43-52. [5] Mukhopadhyay, S.; “Microfibers – An Overview”, Indian Journal of Fibre and Textile Research, Vol.27, 2002, p.307-314. [6] Falkai, B.V.; “Production and properties of microfibers and microfilaments”, The Indian Textile Journal, Vol.2, 1991, p.62-70. [7] Rupp, J.; Yonenaga, A.; “Microfibers-The new manmade fiber image”, International Textile Bulletin, Vol.4, 2000, p.12-24. [8] Kaynak, H.K.; Babaarslan, O.; “Polyester microfilament woven fabrics”, Woven Fabrics, Croatia, 2012, p.155-178. [9] Kaynak, H.K.; Babaarslan, O.; “Effects of microfilament fineness on woven fabric properties”, Electronic Journal of Textile Technology,Vol.3, 2011, p.30-39. [10] Babaarslan, O.; Kaynak, H.K.; “A study on air permeability of windproof polyester microfilament fabrics”, ICONTEX 2011International Congress of Innovative Textiles, Turkey, 2011. [11] Babaarslan, O.; Kaynak, H.K.; “Air permeability of windproof polyester microfilament fabrics at different pressure drop values”, The Fiber Society 2012 Spring Conference Fiber Research for Tomorrow’s Applications, Switzerland, 2012. [12] Al-ansary, M.A.R.; “The Influence of number of filaments on physical and mechanical characteristics of polyester woven fabrics”, Life Science Journal,Vol.9, 2012, p.79-83. [13] Schacher, L.; Adolphe, D.C.; Drean, J.Y.; “Comparison between thermal insulation and thermal properties of classical and microfibres polyester fabrics”, International Journal of Clothing Science and Technology, Vol.12, 2000, p.84-95. Journal of Engineered Fibers and Fabrics Volume 10, Issue 4 – 2015 [14] Islam, M.N.; Lappan, U.; Simon, F.; Voit, B.; “Hydrophobic modification of PET microfilament fabric by low pressure plasma treatment”, Melliand International, Vol.10, 2004, p.211-215. [15] Pociute, M.; Lehmann, B.; Vitkauskas, A.; “Wetting behaviour of surgical polyester woven fabrics”, Materials Science, Vol.9, 2003, p.410-413. [16] Laourine, E.; Cherif, C.; “Characterisation of barrier properties of woven fabrics for surgical protective textiles”, AUTEX Research Journal, Vol.11, 2011, p.31-36. [17] Aibibu, D.; Lehmann, B.; Offermann, P.; “Barrier effect of woven fabrics used for surgical gowns”, AUTEX Research Journal, Vol.3, 2003, p.186-193. [18] Ezaz Shahabi, N.; Asghari Mooneghi, S.; Saharkhiz, S.; Hosseini Varkiyani, S.M.; “Investigating the effect of weight reduction treatment on Poisson’s ratio of microfiber polyester woven fabric”, Journal of Textile Institute, Vol.103, 2011, p.292-297. [19] Nassif, G.A.A.; “Effect of weave structure and weft density on the physical and mechanical properties of micropolyester woven fabrics”, Life Science Journal, Vol.9, 2012, p.13261331. [20] Tortora, P.G.; Collier, B.J.; Understanding textiles, 1997, New Jersey. [21] Petrulis, D.; “Construction, investigation, and application of mathematical models for tensile properties of industrial polyester woven fabrics”, Tekstil, Vol.56, 2007, p.670674. [22] Gürkan Ünal, P.; Taşkın, C.; “The effect of weave and densities on tensile strength of 100% polyester fabrics”, Journal of Textiles and Apparel, Vol.2, 2007, p.115-118. [23] Bilişik, K.; Demiryürek, O.; “Analysis and offaxis tensile characterization of air-entangled textured polyester woven fabrics depending on unit cell interlacing frequency”, Fibers and Polymers, Vol.11, 2010, p.805-811. [24] Bilişik, K.; Demiryürek, O.; “Analysis and tensile characterization of air entangled textured polyester woven fabrics depending on interlacement and yarn sett”, Fibers and Polymers, Vol.12, 2011, p.390-398. [25] Salem, E.H.; Johnson, R.H.; Mohamed, M.H.; “Tensile properties of textured polyester woven fabrics: Theoretical model for plain weave fabric”, Textile Research Journal, Vol.64, 1995, p.185-196. 60 http://www.jeffjournal.org [26] Kumpikaite, E.; “Influence of fabric Structure on the character of fabric breakage”, Fibres and Textiles in Eastern Europe, Vol.68, 2008, p.44-46. [27] ISO 2062:2009 - Textiles - Yarns from packages - Determination of single-end breaking force and elongation at break using constant rate of extension (CRE) tester. [28] ISO 7211-2:1984 - Textiles - Woven fabrics Construction - Methods of analysis - Part 2: Determination of number of threads per unit length. [29] ISO 7211-3:1984 - Textiles - Woven fabrics Construction - Methods of analysis - Part 3: Determination of crimp of yarn in fabric. [30] ISO 3801:1977 - Textiles - Woven fabrics Determination of mass per unit length and mass per unit area. [31] ISO 5084:1996 - Textiles - Determination of thickness of textiles and textile products. [32] ISO 139:2005 - Textiles - Standard atmospheres for conditioning and testing. [33] ISO 13934-1: Determination of maximum force and elongation at maximum force using the strip method by CRE (Constant rate of extension). [34] Realff, M.L.; “Identifying local deformation phenomenon during woven fabric uniaxial tensile loading”, Textile Research Journal, Vol.64, 1994, p.135-141. [35] Kaynak, H.K.; “Investigation of The Performance Properties of Fabrics Woven with Microfilament Yarns”, 2013, Çukurova University, PhD Thesis. AUTHORS’ ADDRESSES Hatice Kübra Kaynak, PhD Gaziantep University Textile Engineering Department 27310 Gaziantep TURKEY Osman Babaarslan, PhD Çukurova University Textile Engineering Department 01330 Adana TURKEY Journal of Engineered Fibers and Fabrics Volume 10, Issue 4 – 2015 61 http://www.jeffjournal.org